CN102832087B - Steel core wire replaces the tungsten filament manufacture craft of molybdenum filament - Google Patents
Steel core wire replaces the tungsten filament manufacture craft of molybdenum filament Download PDFInfo
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- CN102832087B CN102832087B CN201210267622.1A CN201210267622A CN102832087B CN 102832087 B CN102832087 B CN 102832087B CN 201210267622 A CN201210267622 A CN 201210267622A CN 102832087 B CN102832087 B CN 102832087B
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- filament
- steel core
- core wire
- molybdenum
- tungsten
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- Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)
Abstract
The invention discloses the tungsten filament manufacture craft that a kind of steel core wire replaces molybdenum filament, comprise single-filament triple-helix lamp filament coiling, steel core wire after sodium hydroxide solution electrolytic cleaning is deoiled, then cleans through running water, then dries, and then arranges silk take-up; First spiral adopts steel core wire to be heart yearn, with tungsten filament, second, third spiral of molybdenum filament continuous coiling; A high-temperature shaping, after cooling, falls steel core silk with nitric acid, dissolving with hydrochloric acid, but insoluble tungsten filament, molybdenum filament, clean up; Secondary high-temperature is shaped, and dissolves molybdenum filament, to obtain final product.The present invention utilizes ordinary metallic material steel core wire to instead of tungsten and molybdenum material, has saved rare metal resources, has reduced cost.
Description
Technical field
The present invention relates to filament field, is exactly the tungsten filament manufacture craft that a kind of steel core wire replaces molybdenum filament.
Background technology
Tungsten filament is used as except the reinforcement of the exothermic material of high temperature furnace, the heater of electron tube and composite material etc. except a small amount of, and the overwhelming majority is all for the electrode of the filament and gaseous discharge lamp that make various incandescent lamp and tungsten halogen lamp.
Illuminator lamp wire material is generally tungsten and molybdenum material in the world at present.Along with industrial expansion, raw-material resource is more and more in short supply, and national tungsten Mineral Resource declines rapidly, new tungsten can be replaced for the material of illuminator lamp silk in the urgent need to having.
Summary of the invention
The object of this invention is to provide the tungsten filament manufacture craft that a kind of steel core wire replaces molybdenum filament.
Above-mentioned purpose is realized by following scheme:
Steel core wire replaces the tungsten filament manufacture craft of molybdenum filament, comprises single-filament triple-helix lamp filament coiling, it is characterized in that comprising the following steps:
(1), steel core wire after sodium hydroxide solution electrolytic cleaning is deoiled, then cleans through running water, then dries, then row's silk take-up;
(2), the first spiral adopts steel core wire to be heart yearn, with tungsten filament, molybdenum filament continuous coiling second spiral, triple helical;
(3), a high-temperature shaping, setting temperature is 1140-1200 DEG C, and the time is 8-10 minute;
(4), after cooling, fall steel core wire, but insoluble tungsten filament, molybdenum filament with the solubilize of nitric acid, hydrochloric acid composition, clean up;
(6), secondary high-temperature sizing, setting temperature is 1350-1400 DEG C, and the time is 10-12 minute, then melt fall molybdenum filament, obtain filament.
The concentration of described sodium hydroxide solution is 8-12%.
Described steel core wire replaces the tungsten filament manufacture craft of molybdenum filament, it is characterized in that: the filament after secondary high-temperature sizing, adds after boiling 5-8 minute in boiled 8-12% sodium hydrate aqueous solution, more repeatedly use tap water; And then boil 5-8 minute pass fire again after opening with poach such as distillation poach, clean repeatedly with running water, finally enter oven for drying with after absolute ethyl alcohol dehydration.
Beneficial effect of the present invention is: the present invention utilizes ordinary metallic material steel core wire to instead of tungsten and molybdenum material, has saved rare metal resources, has reduced cost.
Embodiment
Steel core wire replaces the tungsten filament manufacture craft of molybdenum filament, comprises single-filament triple-helix lamp filament coiling, comprises the following steps:
(1), steel core wire after 10% sodium hydroxide solution electrolytic cleaning is deoiled, then cleans through running water, then dries, then row's silk take-up;
(2), the first spiral adopts φ 0.08mm steel core wire to be heart yearn, with tungsten filament, molybdenum filament continuous coiling second spiral, triple helical;
(3), a high-temperature shaping, setting temperature is 1160 DEG C, and the time is 10 minutes;
(4), after cooling, fall steel core wire, but insoluble tungsten filament, molybdenum filament with the solubilize of nitric acid, hydrochloric acid composition, clean up;
(6), secondary high-temperature sizing, setting temperature is 1350 DEG C, and the time is 10 minutes, then melt fall molybdenum filament, obtain filament.Filament after secondary high-temperature sizing, adds after boiling 8 minutes in 10% boiled sodium hydrate aqueous solution, more repeatedly uses tap water; And then boil 5 minutes pass fire again after opening with poach such as distillation poach, clean repeatedly with running water, finally enter oven for drying with after absolute ethyl alcohol dehydration.
Claims (3)
1. steel core wire replaces the tungsten filament manufacture craft of molybdenum filament, comprises single-filament triple-helix lamp filament coiling, it is characterized in that comprising the following steps:
(1), steel core wire after sodium hydroxide solution electrolytic cleaning is deoiled, then cleans through running water, then dries, then row's silk take-up;
(2), the first spiral adopts steel core wire to be heart yearn, with tungsten filament, molybdenum filament continuous coiling second spiral, triple helical;
(3), a high-temperature shaping, setting temperature is 1140-1200 DEG C, and the time is 8-10 minute;
(4), after cooling, fall steel core wire, but insoluble tungsten filament, molybdenum filament with the solubilize of nitric acid, hydrochloric acid composition, clean up;
(6), secondary high-temperature sizing, setting temperature is 1350-1400 DEG C, and the time is 10-12 minute, then melt fall molybdenum filament, obtain filament.
2. steel core wire according to claim 1 replaces the tungsten filament manufacture craft of molybdenum filament, it is characterized in that: the concentration of described sodium hydroxide solution is 8-12%.
3. steel core wire according to claim 1 replaces the tungsten filament manufacture craft of molybdenum filament, it is characterized in that: the filament after secondary high-temperature sizing, adds after boiling 5-8 minute in boiled 8-12% sodium hydrate aqueous solution, more repeatedly use tap water; And then with distillation poach, boil again after waiting poach to open and close fire in 5-8 minute, clean repeatedly with running water, finally enter oven for drying with after absolute ethyl alcohol dehydration.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210267622.1A CN102832087B (en) | 2012-07-30 | 2012-07-30 | Steel core wire replaces the tungsten filament manufacture craft of molybdenum filament |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210267622.1A CN102832087B (en) | 2012-07-30 | 2012-07-30 | Steel core wire replaces the tungsten filament manufacture craft of molybdenum filament |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102832087A CN102832087A (en) | 2012-12-19 |
| CN102832087B true CN102832087B (en) | 2016-03-09 |
Family
ID=47335172
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210267622.1A Expired - Fee Related CN102832087B (en) | 2012-07-30 | 2012-07-30 | Steel core wire replaces the tungsten filament manufacture craft of molybdenum filament |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102832087B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104576299A (en) * | 2013-10-18 | 2015-04-29 | 丹阳市中远车灯有限公司 | Halogen lamp producing technique |
| CN104409566A (en) * | 2014-11-06 | 2015-03-11 | 云南师范大学 | Two-electrode electrochemical preparation method of copper zinc tin sulfide thin film material |
| CN107086170A (en) * | 2017-03-22 | 2017-08-22 | 合肥仁德电子科技有限公司 | A kind of street lamp filament manufacture craft |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5491973A (en) * | 1977-12-28 | 1979-07-20 | Mitsubishi Electric Corp | Production of filament coil for lamp bulb |
| DE3123442A1 (en) * | 1981-06-12 | 1982-12-30 | Patent-Treuhand-Gesellschaft für elektrische Glühlampen mbH, 8000 München | BULB FOR AN ELECTRIC LAMP AND METHOD FOR THE PRODUCTION THEREOF |
| JPS55161330A (en) * | 1979-06-05 | 1980-12-15 | Mitsubishi Electric Corp | Manufacture of filament coil for bulb |
| CN201417744Y (en) * | 2009-06-19 | 2010-03-03 | 启东市汇利照明有限公司 | Florescent lamp filament |
| CN102082067B (en) * | 2010-12-08 | 2012-10-03 | 安徽霍山县华光节能科技有限公司 | Coreless winding method of coiled-coil filament |
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2012
- 2012-07-30 CN CN201210267622.1A patent/CN102832087B/en not_active Expired - Fee Related
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| Publication number | Publication date |
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| CN102832087A (en) | 2012-12-19 |
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Effective date of registration: 20160127 Address after: 237200 weft eight road, Mount Holyoke Economic Development Zone, Lu'an, Anhui Applicant after: Anhui Ocean Lighting Electric Co.,Ltd. Address before: 237200, Lu'an Mount Holyoke Economic Development Zone, Anhui Province, by the three South Road and weft eight road junction Applicant before: ANHUI HUOSHAN COUNTY WANXIN ELECTRONIC TECHNOLOGY Co.,Ltd. |
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Granted publication date: 20160309 Termination date: 20210730 |