CN102800374B - Continuous operation feeding device and method - Google Patents

Continuous operation feeding device and method Download PDF

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Publication number
CN102800374B
CN102800374B CN201210320815.9A CN201210320815A CN102800374B CN 102800374 B CN102800374 B CN 102800374B CN 201210320815 A CN201210320815 A CN 201210320815A CN 102800374 B CN102800374 B CN 102800374B
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pressure
valve
pressure vessel
auxiliary
pressurer system
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CN102800374A (en
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郝少昌
马景陶
赵兴宇
邓长生
王阳
周湘文
梁彤翔
郭文利
唐春和
刘兵
唐亚平
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Tsinghua University
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Tsinghua University
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E30/00Energy generation of nuclear origin
    • Y02E30/30Nuclear fission reactors

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Abstract

The invention provides a continuous operation feeding device and method, wherein, the continuous operation feeding device comprises a main pressure vessel (1), an auxiliary pressure vessel (2), a pressure measuring device, a pressure control system, a pipeline, a feed valve (3) and a discharging valve (4); the pressure control system is respectively connected with the main pressure vessel (1) and the auxiliary pressure vessel (2); the feed valve (3) is connected with the auxiliary pressure vessel (2); the discharging valve (4) is connected with the main pressure vessel (1); the main pressure vessel (1) is positioned below the auxiliary pressure vessel (2); and the main pressure vessel (1) is connected with the auxiliary pressure vessel (2) through the pipeline and a connection valve (8). The continuous operation feeding device can achieve mass continuous production on the premise of criticality safety, the whole device occupies small space, the continuous operation feeding device is simple and convenient to operate, and the core production cannot be influenced during the continuous feeding operation process.

Description

A kind of operation charging gear and method continuously
Technical field
The present invention relates to nuclear material preparing technical field, relate in particular to a kind of sol-gal process that is applicable to and prepare continuous operation charging gear and the method in the uranium dioxide core core technique of high temperature gas cooled reactor spheric fuel element.
Background technology
Sol-gal process is prepared ceramic microsphere process application in the uranium dioxide core core of preparation high temperature gas cooled reactor spheric fuel element.This uranium dioxide fuel core core requires 500 microns of left and right of diameter, and dimensional discrepancy is little.
Sol-gal process is prepared uranium dioxide core core and is mainly contained following steps:
1, dissolve, by triuranium octoxide (U 3o 8) powder is dissolved in nitric acid, is configured to the uranyl nitrate solution of certain uranium atom concentration;
2, boil glue, in uranyl nitrate solution, add urea by certain metering ratio, evaporation and concentration certain hour at a certain temperature, adds after cooling thickening agent to adjust viscosity, obtains glue;
3, disperse granulation, the glue of getting ready is moved in head tank, promoting glue with certain pressure flows along pipeline, glue is finally admitted to the vibrating nozzle with certain frequency vibration, from flowing out, vibrating nozzle disperses to become the drop that has certain size, this step needs the accurate flow of controlling, because the difference of flow directly causes the deviation of drop size;
4, gelling balling-up, drop forms afterwards first through air zone, rely on the surface tension of self to form spherical, spherical droplets is again by ammonia district, drop and ammonia generation gelling reaction make surperficial precuring and have certain intensity, enter afterwards ammoniacal liquor district and carry out further gelling reaction and become gel ball;
5, ageing, when gel ball has just formed, gelling reaction only completes at gel ball near surface, gel ball internal-response needs regular hour and temperature, therefore need that gel ball is placed in to ammoniacal liquor and add thermal aging 1~3 hour, gel ball is reacted completely, become the spheric grain that has uniformly some strength;
6, washing, uranyl nitrtate reacts with ammoniacal liquor and generates ammonium diuranate and ammonium nitrate, and ammonium diuranate is required composition, and ammonium nitrate is objectionable constituent, easily in subsequent technique, causes little ball fractured, therefore ammonium nitrate must be removed, method is washing repeatedly.Washing needs 3~5 times, and first pass uses 1%~2% weak aqua ammonia, and several all over using deionized water subsequently, each washing lotion need to be tested its concentration of nitric acid, guarantees that nitrate radical content is enough low;
7, dry, the bead after washing is dry by vacuum rotating seasoning, need to control temperature, vacuum tightness and rotational speed, to ensure that dry run fully completes and can not cause the destruction of bead;
8, roasting, dried bead need to be at roasting kiln roasting, and to slough the organic components in bead, the principal ingredient of bead becomes orange oxide simultaneously;
9, reduction, roasting ball, in reduction furnace, is reduced to uranium dioxide under hydrogen atmosphere, need to ensure suitable reduction temperature and sufficient reductive agent and sufficient recovery time;
10, sintering, the bead after reduction, under hydrogen atmosphere, 1400~1600 degrees Celsius of lower sintering 3~5 hours, becomes uranium dioxide core core;
11, screening and sorting, through screening and sorting step, can obtain size homogeneous, the uranium dioxide core core that sphericity meets the demands.
In the above-mentioned step of preparing uranium dioxide core core, it is preparation technology's key that step 3 is disperseed granulation, is also that technique realizes quantity-produced bottleneck in enormous quantities.Because the adhesive liquid quantity of preparing core core need to meet criticality safety, the stored adhesive liquid quantity of each container must be lower than critical mass, or head tank is safe by geometry.But the head tank of safe by geometry is flat or longilineal, volume will certainly cause space hold too large after strengthening, and therefore answer the volume of limiting pressure tank, but this has limited productive capacity.For meeting continuous need of production, also to meet criticality safety, it is impracticable using single head tank.
Summary of the invention
(1) technical matters that will solve
The technical problem to be solved in the present invention is to provide one and meets quantity-produced glue charging gear in enormous quantities and method, and it can expand in batches and realize continuously and producing under the principle of criticality safety.
(2) technical scheme
For reaching above-mentioned purpose, continuous operation charging gear of the present invention, comprise principal pressure container 1, auxiliary pressure vessel 2, device for pressure measurement, control pressurer system, pipeline, inlet valve 3 and outlet valve 4, wherein control pressurer system is connected with principal pressure container 1, auxiliary pressure vessel 2 respectively, inlet valve 3 is connected with auxiliary pressure vessel 2, outlet valve 4 is connected with principal pressure container 1, and principal pressure container 1 is positioned at auxiliary pressure vessel 2 belows, between them, is connected with connection valve 8 by pipeline.
Described device for pressure measurement comprises the first device for pressure measurement P1 that measures principal pressure container 1 internal pressure and the second device for pressure measurement P2 that measures auxiliary pressure vessel 2 internal pressures, described control pressurer system comprises the first control pressurer system a and the second control pressurer system b, between principal pressure container 1 and the first control pressurer system a, be connected by the first pipeline, between auxiliary pressure vessel 2 and the second control pressurer system b, be connected by the second pipeline and auxiliary pressure control valve 6, between the first pipeline and the second pipeline, connect by coupling cock 7.The tie point of the second pipeline and the first pipeline, between auxiliary pressure control valve 6 and auxiliary pressure vessel 2.
This moves continuously charging gear and also comprises pneumatic manifold and pressurized air main valve 5, and pressurized air main valve 5 is positioned on pneumatic manifold, after pneumatic manifold branch, is connected respectively with the first control pressurer system a and the second control pressurer system b.
The first device for pressure measurement P1 and the second device for pressure measurement P2 are tensimeter or pressure unit.
The method that described continuous operation charging gear moves feed continuously comprises initial step and continuous-feeding step.
Described initial step comprises:
Glue is added to auxiliary pressure vessel 2 by peripherals from inlet valve 3;
Open connection valve 8, make glue rely on gravity to enter principal pressure container 1, close afterwards inlet valve 3 and connection valve 8;
Open pressurized air main valve 5, regulate the first control pressurer system a, make the first pressure A that the first device for pressure measurement P1 records reach setting value, open outlet valve 4.
Described continuous-feeding step comprises:
In the time that in principal pressure container 1, glue consumption is extremely a certain amount of, open inlet valve 3, follow-up glue is added to auxiliary pressure vessel 2, after adding, close inlet valve 3;
Open auxiliary pressure control valve 6, and regulate the second control pressurer system b, control the second pressure B of auxiliary pressure vessel 2, make it approach the first pressure A, wherein the second pressure B is recorded by the second device for pressure measurement P2;
Close auxiliary pressure control valve 6 and open coupling cock 7, opening afterwards connection valve 8, making glue flow into principal pressure container 1;
After transfer, close connection valve 8, coupling cock 7 and auxiliary pressure control valve 6.
(3) beneficial effect
The device and method that the present invention adopts technique scheme to provide, can realize continuous-feeding operation by two interconnective pressure vessels, and wherein pressure vessel is all safe by geometry.First in auxiliary pressure vessel, add glue, glue relies on gravity to enter principal pressure container, provides pressure to make glue flow out and produce from discharge port by control pressurer system; Glue in principal pressure container consumes when a certain amount of, in the situation that not affecting principal pressure container air pressure, according to certain method and program, follow-up glue is supplemented into principal pressure container via auxiliary pressure vessel.So just under the prerequisite of criticality safety, realized production continuously in enormous quantities, whole equipment occupation space is little, easy and simple to handle, and in continuous-feeding operating process, does not affect the production of core core.
Brief description of the drawings
Fig. 1 is the structural drawing of continuous operation charging gear of the present invention.
In figure, 1: principal pressure container; 2: auxiliary pressure vessel; 3: inlet valve; 4: outlet valve; 5: pressurized air main valve; 6: auxiliary pressure control valve; 7: coupling cock; 8: connection valve; A: the first control pressurer system; B: the second control pressurer system; P1: the first device for pressure measurement; P2: the second device for pressure measurement.
Embodiment
Below in conjunction with drawings and Examples, the present invention being moved to charging gear is continuously described in further detail.Following examples are used for illustrating the present invention, but are not used for limiting the scope of the invention.
In description of the invention, it should be noted that, term " " center ", " longitudinally ", " laterally ", " on ", D score, " front ", " afterwards ", " left side ", " right side ", " vertically ", " level ", " top ", " end " " interior ", orientation or the position relationship of instructions such as " outward " are based on orientation shown in the drawings or position relationship, only the present invention for convenience of description and simplified characterization, instead of device or the element of instruction or hint indication must have specific orientation, with specific orientation structure and operation, therefore can not be interpreted as limitation of the present invention.In addition, term " first ", " second ", " the 3rd " be only for describing object, and can not be interpreted as instruction or hint relative importance.
In description of the invention, it should be noted that, unless otherwise clearly defined and limited, term " installation ", " being connected ", " connection " should be interpreted broadly, and for example, can be to be fixedly connected with, and can be also to removably connect, or connect integratedly; Can be mechanical connection, can be also electrical connection; Can be to be directly connected, also can indirectly be connected by intermediary, can be the connection of two element internals.For the ordinary skill in the art, can concrete condition understand above-mentioned term concrete meaning in the present invention.
In addition,, in description of the invention, except as otherwise noted, the implication of " multiple " is two or more.
Continuous operation charging gear of the present invention, comprise principal pressure container 1, auxiliary pressure vessel 2, device for pressure measurement, control pressurer system, pipeline, inlet valve 3 and outlet valve 4, wherein control pressurer system is connected with principal pressure container 1, auxiliary pressure vessel 2 respectively, inlet valve 3 is connected with auxiliary pressure vessel 2, outlet valve 4 is connected with principal pressure container 1, principal pressure container 1 is positioned at auxiliary pressure vessel 2 belows, between them, is connected with connection valve 8 by pipeline.
Described device for pressure measurement comprises the first device for pressure measurement P1 that measures principal pressure container 1 internal pressure and the second device for pressure measurement P2 that measures auxiliary pressure vessel 2 internal pressures, described control pressurer system comprises the first control pressurer system a and the second control pressurer system b, between principal pressure container 1 and the first control pressurer system a, be connected by the first pipeline, between auxiliary pressure vessel 2 and the second control pressurer system b, be connected by the second pipeline and auxiliary pressure control valve 6, between the first pipeline and the second pipeline, connect by coupling cock 7.The tie point of the second pipeline and the first pipeline, between auxiliary pressure control valve 6 and auxiliary pressure vessel 2.
This moves continuously charging gear and also comprises pneumatic manifold and pressurized air main valve 5, and pressurized air main valve 5 is positioned on pneumatic manifold, after pneumatic manifold branch, is connected respectively with the first control pressurer system a and the second control pressurer system b.
Wherein, principal pressure container 1, auxiliary pressure vessel 2 are for depositing glue, and its shape is flattened cylindrical body, for example flat head tank.Described coupling cock 7 is for the UNICOM of principal pressure container 1 and auxiliary pressure vessel 2 pressure, the material that described connection valve 8 is controlled principal pressure container 1 and auxiliary pressure vessel 2 shifts, described pressurized air main valve 5 is provided by the pressurized air being provided by peripherals, described auxiliary pressure control valve 6 is controlled the pressurized air of auxiliary pressure vessel 2, and described the first control pressurer system a and the second control pressurer system b control respectively the interior pressure of principal pressure container 1 and auxiliary pressure vessel 2.
Preferably, the first device for pressure measurement P1 and the second device for pressure measurement P2 are tensimeter or pressure unit.Working pressure table can read the pressure in principal pressure container 1 and auxiliary pressure vessel 2 intuitively, and working pressure transmitter can be converted to electric signal by pressure and feed back to controller, and the pressure in principal pressure container 1 and auxiliary pressure vessel 2 is monitored in real time.
The method that described continuous operation charging gear moves feed continuously comprises initial step and continuous-feeding step.
Described initial step comprises:
Glue is added to auxiliary pressure vessel 2 by peripherals from inlet valve 3;
Open connection valve 8, make glue rely on gravity to enter principal pressure container 1, close afterwards inlet valve 3 and connection valve 8;
Open pressurized air main valve 5, regulate the first control pressurer system a, make the first pressure A that the first device for pressure measurement P1 records reach setting value, open outlet valve 4.
Described continuous-feeding step comprises:
In the time that in principal pressure container 1, glue consumption is extremely a certain amount of, open inlet valve 3, follow-up glue is added to auxiliary pressure vessel 2, after adding, close inlet valve 3;
Open auxiliary pressure control valve 6, and regulate the second control pressurer system b, control the second pressure B of auxiliary pressure vessel 2, make it approach the first pressure A, wherein the second pressure B is recorded by the second device for pressure measurement P2;
Close auxiliary pressure control valve 6 and open coupling cock 7, opening afterwards connection valve 8, making glue flow into principal pressure container 1;
After transfer, close connection valve 8, coupling cock 7 and auxiliary pressure control valve 6.
Above embodiment is only for illustrating the present invention, and be not limitation of the present invention, the those of ordinary skill in relevant technologies field, without departing from the spirit and scope of the present invention, can also make a variety of changes and modification, therefore all technical schemes that are equal to also belong to category of the present invention.

Claims (6)

1. one kind is moved charging gear continuously, it is characterized in that: this moves continuously charging gear and comprises principal pressure container (1), auxiliary pressure vessel (2), device for pressure measurement, control pressurer system, pipeline, inlet valve (3) and outlet valve (4), wherein control pressurer system respectively with principal pressure container (1), auxiliary pressure vessel (2) connects, inlet valve (3) is connected with auxiliary pressure vessel (2), outlet valve (4) is connected with principal pressure container (1), principal pressure container (1) is positioned at auxiliary pressure vessel (2) below, between them, be connected with connection valve (8) by pipeline,
Wherein, described device for pressure measurement comprises the first device for pressure measurement (P1) of measuring principal pressure container (1) internal pressure and the second device for pressure measurement (P2) of measuring auxiliary pressure vessel (2) internal pressure, described control pressurer system comprises the first control pressurer system (a) and the second control pressurer system (b), between principal pressure container (1) and the first control pressurer system (a), be connected by the first pipeline, between auxiliary pressure vessel (2) and the second control pressurer system (b), be connected by the second pipeline and auxiliary pressure control valve (6), between the first pipeline and the second pipeline, connect by coupling cock (7).
2. continuous operation charging gear according to claim 1, it is characterized in that: this moves continuously charging gear and also comprises pneumatic manifold and pressurized air main valve (5), pressurized air main valve (5) is positioned on pneumatic manifold, after pneumatic manifold branch, be connected with the first control pressurer system (a) and the second control pressurer system (b) respectively.
3. continuous operation charging gear according to claim 1, is characterized in that: the first device for pressure measurement (P1) and the second device for pressure measurement (P2) are tensimeter or pressure unit.
4. continuous operation charging gear according to claim 1, is characterized in that: the tie point of the second pipeline and the first pipeline, is positioned between auxiliary pressure control valve (6) and auxiliary pressure vessel (2).
5. the continuous operation charging gear described in employing claim 2-4 any one moves the method for feed continuously, it is characterized in that: described method comprises initial step and continuous-feeding step;
Wherein, described initial step comprises:
Glue is added to auxiliary pressure vessel (2) by peripherals from inlet valve (3);
Open connection valve (8), make glue rely on gravity to enter principal pressure container (1), close afterwards inlet valve (3) and connection valve (8);
Open pressurized air main valve (5), regulate the first control pressurer system (a), make the first pressure A that the first device for pressure measurement (P1) records reach setting value, open outlet valve (4).
6. method according to claim 5, is characterized in that: described continuous-feeding step comprises:
In the time that in principal pressure container (1), glue consumption is extremely a certain amount of, open inlet valve (3), follow-up glue is added to auxiliary pressure vessel (2), after adding, close inlet valve (3);
Open auxiliary pressure control valve (6), and regulate the second control pressurer system (b), control the second pressure B of auxiliary pressure vessel (2), make it approach the first pressure A, wherein the second pressure B is recorded by the second device for pressure measurement (P2);
Close auxiliary pressure control valve (6) and open coupling cock (7), opening afterwards connection valve (8), making glue flow into principal pressure container (1);
After transfer, close connection valve (8), coupling cock (7) and auxiliary pressure control valve (6).
CN201210320815.9A 2012-08-31 2012-08-31 Continuous operation feeding device and method Active CN102800374B (en)

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Publication number Priority date Publication date Assignee Title
CN109012493B (en) * 2018-08-16 2021-03-05 宋波 Pressure-reducing operation type fuel rod application device
CN110860256B (en) * 2019-12-24 2024-06-07 青岛理工大学 Pressure vessel feeding device

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