CN102794144A - Condensation air exhaust type vanadium liquid automatic preparation system - Google Patents
Condensation air exhaust type vanadium liquid automatic preparation system Download PDFInfo
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- CN102794144A CN102794144A CN2012103303191A CN201210330319A CN102794144A CN 102794144 A CN102794144 A CN 102794144A CN 2012103303191 A CN2012103303191 A CN 2012103303191A CN 201210330319 A CN201210330319 A CN 201210330319A CN 102794144 A CN102794144 A CN 102794144A
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
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Abstract
The invention relates to a condensation air exhaust type vanadium liquid automatic preparation system which comprises a reaction kettle, a hot oil circulating system, a cold oil circulating system and an air exhaust type condensation gas recycling system, wherein the hot oil circulating system supplies heat to the vanadium liquid in the reaction kettle; the cold oil circulating system cools the vanadium liquid in the reaction kettle; the air exhaust type condensation gas recycling system is connected with an exhaust port on the reaction kettle; the hot oil in the hot oil circulating system passes through the reaction kettle and then flows back to a hot oil storage device; the cold oil in the cold oil circulating system passes through the reaction kettle and then flows back to a cold oil storage device; and the air exhaust type condensation gas recycling system comprises a condensation device, a waste gas neutralizing and recycling device and an air exhaust device, wherein the condensation device and/or the waste gas neutralizing and recycling device are/is communicated with the air exhaust device. The condensation air exhaust type vanadium liquid automatic preparation system provided by the invention can effectively recycle and dispose the harmful gas discharged by the reaction kettle; and moreover, the hot oil circulating system and the cold oil circulating system can more effectively guarantee the reaction temperature in the reaction kettle.
Description
[technical field]
The present invention relates to a kind of vanadium liquid preparing system, be specifically related to a kind of condensation bleeder vanadium liquid automatic preparation system.
[background technology]
The inventor finds that in practice agitated reactor can produce great amount of high-temperature, corrosivity pernicious gas (especially on agitated reactor, adopt batch charger fast in agitated reactor during a large amount of feeding intake and in the raw material reaction process) in the process of preparation vanadium liquid; These high temperature, corrosive gas will directly be discharged from agitated reactor under the situation of any processing, can bring very big influence to environment like this.And in the prior art, the agitated reactor heating arrangement that is used to produce vanadium liquid is employed in the inner heater of installing of agitated reactor; Be installed in the cavity of agitated reactor after the sealing of this heater, in raw material is introduced into agitated reactor after, open heater the raw material in the agitated reactor heated; Because said heater is installed in the agitated reactor cavity a bit; During heating, heat diffuses to whole cavity by this point, can make that so interior each regional temperature of agitated reactor cavity is inhomogeneous; Prepare whole heats in the process thereby influence vanadium liquid, influence the performance of vanadium liquid.
[summary of the invention]
In order to solve the technical problem that exists in the prior art; The invention provides a kind of condensation bleeder vanadium liquid automatic preparation system, said condensation bleeder vanadium liquid automatic preparation system comprises the agitated reactor that is used to prepare vanadium liquid, be used for to vanadium liquid in the agitated reactor carry out the Circulation and Hot Oil Spray system of heat supply, the cold oil circulatory system that is used for vanadium liquid in the agitated reactor is cooled off with agitated reactor on the bleeder condensed gas recovery system that is connected of the exhaust outlet that is provided with;
Wherein, the pyrogenicity oil storage device that refluxes again after through the agitated reactor circulation of the deep fat in the said Circulation and Hot Oil Spray system, the cold oil in the said cold oil circulatory system refrigeration oil storage device that refluxes again after through the agitated reactor circulation;
Said bleeder condensed gas recovery system comprises: with retracting device and air extractor, be communicated with air extractor with retracting device in said condensing unit and/or the waste gas in condensing unit that is connected with the exhaust outlet of agitated reactor and/or the waste gas.
According to optimal technical scheme of the present invention: said bleeder condensed gas recovery system also comprises condensation water tank, and said condensation water tank one end is connected the other end with the output of said condensing unit and inserts said agitated reactor, is connected with the filler of said agitated reactor.
According to optimal technical scheme of the present invention: the condensing unit that is connected with exhaust outlet in the said bleeder condensed gas recovery system is a condensing tower, in the condensing tower set inside cooling line is arranged, and said cooling line forms a circulation, and is communicated with cooling-water machine.
According to optimal technical scheme of the present invention: be provided with alkaline matter in the said waste gas He in the retracting device.
According to optimal technical scheme of the present invention: said air extractor is an air exhauster.
According to optimal technical scheme of the present invention: said Circulation and Hot Oil Spray system comprises deep fat storage device, deep fat heater; Wherein, Said deep fat storage device and said deep fat heater form operation cycle; Through said deep fat heater the oil in the said deep fat storage device is heated to design temperature, said deep fat storage device and agitated reactor form operation cycle, make the stream of hot oil in the said deep fat storage device in the outer chamber of said agitated reactor, be back to the deep fat storage device again.
According to optimal technical scheme of the present invention: be provided with pipeline in the said deep fat heater, this pipeline one end is connected with cooling water pipe, and the other end is connected with drainpipe.
According to optimal technical scheme of the present invention: the said cold oil circulatory system comprises the cold oil storage device; Said cold oil storage device self has a circulatory system; Said in addition cold oil storage device and agitated reactor form operation cycle, cold oil in the said cold oil storage device is flowed through be back to the cold oil storage device again in the outer chamber of said agitated reactor.
According to optimal technical scheme of the present invention: be provided with oily temperature cooling circuit in the said cold oil storage device, said oil temperature cooling circuit is connected with cooling-water machine.
According to optimal technical scheme of the present invention: the oil temperature of the cold oil of storage is at normal temperature or below the normal temperature in the said cold oil storage device.
The present invention designs ingenious; Condensation bleeder vanadium liquid automatic preparation system is satisfying under a large amount of, efficient, automatic situation about in vanadium liquid agitated reactor, feeding intake; Can effectively reclaim and dispose a large amount of high temperature, the corrosivity pernicious gas of discharging in the agitated reactor; And the Circulation and Hot Oil Spray system and the cold oil circulatory system can more effectively be guaranteed the reaction temperature in the agitated reactor.
[description of drawings]
Fig. 1 condensation bleeder of the present invention vanadium liquid automatic preparation system structural representation.
[specific embodiment]
Below in conjunction with accompanying drawing condensation bleeder vanadium liquid automatic preparation system of the present invention is elaborated:
See also Fig. 1 condensation bleeder of the present invention vanadium liquid automatic preparation system structural representation; Shown in figure; The invention provides a kind of condensation bleeder vanadium liquid automatic preparation system, said condensation bleeder vanadium liquid automatic preparation system comprises the agitated reactor 101 that is used to prepare vanadium liquid, be used for to vanadium liquid in the agitated reactor 101 carry out the Circulation and Hot Oil Spray system of heat supply, the cold oil circulatory system that is used for vanadium liquid in the agitated reactor 101 are cooled off with agitated reactor 101 on the bleeder condensed gas recovery system that is connected of the exhaust outlet 107 that is provided with;
Wherein, the pyrogenicity oil storage device 102 that refluxes again after through agitated reactor 101 circulations of the deep fat in the said Circulation and Hot Oil Spray system, the cold oil in the said cold oil circulatory system refrigeration oil storage device 103 that refluxes again after through agitated reactor 101 circulations;
Said bleeder condensed gas recovery system comprises: in the condensing unit 104 that is connected with the exhaust outlet 107 of agitated reactor 101, the waste gas and/or retracting device 105 and air extractor 106, be communicated with air extractor 106 with retracting device 105 in said condensing unit 104 and/or the waste gas.
Concrete; In Fig. 1, can show; Said Circulation and Hot Oil Spray system comprises deep fat storage device 102, deep fat heater 112; Wherein, deep fat storage device 102 is that deep fat jar, said deep fat heater 112 are oily temperature machine, between said deep fat storage device 102 and said deep fat heater 112, forms operation cycle through pipeline; Through said deep fat heater 112 oil in the said deep fat storage device 102 is heated to design temperature; Generally said temperature will add 140 ℃ to 180 ℃ of thermics, and said deep fat storage device 102 forms operation cycle with agitated reactor 101, and (agitated reactor 101 comprises the inner chamber body 117 that preparation vanadium liquid is used through the outer chamber 113 of said agitated reactor 101 to make said deep fat storage device 102 interior stream of hot oil; Outside this inner chamber body 117 and between the shell of agitated reactor 101, be provided with outer chamber 113; This outer chamber 113 is wrapped in the inner chamber body 117 of said agitated reactor 101) in be back to deep fat storage device 102 again, like this, flow into the outer chamber 113 of said agitated reactor 101 through deep fat; Can make the oil temperature in the inner chamber body 117 of sidewall conduction like agitated reactor 101 of agitated reactor 101; Effect is played in the heating of vanadium liquid, insulation, and the pipeline in " operation cycle between deep fat storage device 102 and the said deep fat heater 112 " in the said in the present invention Circulation and Hot Oil Spray system and " the deep fat storage device 102 flow through agitated reactor 101 be back to the operation cycle of deep fat storage device 102 again " has overlapping shared problem, only need can satisfy the use needs through the open and close of the valve that is provided with on the pipeline in the time of adjusting; Certainly, also can adopt pipeline independently to satisfy the needs of different closed circuits in practice.
Be provided with the pipeline (not shown) in the said deep fat heater 112 in the Circulation and Hot Oil Spray system (oily temperature machine); This pipeline one end is connected with cooling water pipe 114; The other end is connected with drainpipe 115, injects cold water through cooling water pipe 114 and can make cold water through the pipeline that is arranged in the deep fat heater 112 (oily temperature machine) deep fat heater 112 (oily temperature machine) played cooling effect.
In the present invention; The said cold oil circulatory system comprises cold oil storage device 103; Said cold oil storage device 103 self has a circulatory system; Said in addition cold oil storage device 103 forms operation cycle with agitated reactor 101; Cold oil in the said cold oil storage device 103 are flowed through be back to cold oil storage device 103 again in the outer chamber 113 (agitated reactor 101 comprises the inner chamber body 117 that preparation vanadium liquid is used, and outside this inner chamber body 117 and between the shell of agitated reactor 101, is provided with outer chamber 113, and this outer chamber 113 is wrapped in the inner chamber body 117 of said agitated reactor 101) of said agitated reactor 101; In technical scheme of the present invention, the shared oil-in 118 and oil-out 119 of the said Circulation and Hot Oil Spray system and the said cold oil circulatory system.
In technical scheme of the present invention; Be provided with oily temperature cooling circuit 116 in the said cold oil storage device 103; Said oil temperature cooling circuit 116 is connected with cooling-water machine 109; Can in oil temperature cooling circuit 116, inject cooling water through cooling-water machine 109, realize that with this said cooling-water machine 109 is connected with drainpipe 115 with cooling water pipe 114 respectively to the control and the adjusting of oil temperature in the cold oil storage device 103; In technical scheme of the present invention, the oil temperature of the cold oil of storage is at normal temperature or below the normal temperature in the said cold oil storage device 103.
In technical scheme of the present invention; Also comprise bleeder condensed gas recovery system, said bleeder condensed gas recovery system comprises: in the condensing unit 104 that is connected with the exhaust outlet 107 of agitated reactor 101, the waste gas and retracting device 105 and air extractor 106, be communicated with air extractor 106 with retracting device 105 in said condensing unit 104 and/or the waste gas; Said bleeder condensed gas recovery system also comprises condensation water tank 110; Said condensation water tank 110 1 ends are connected the other end with the output of said condensing unit 104 and insert said agitated reactor 101, are connected with the filler 111 of said agitated reactor 101, in the present invention; The condensing unit 104 that is connected with exhaust outlet 107 in the said bleeder condensed gas recovery system is condensing tower; In the condensing tower set inside cooling line 108 is arranged, said cooling line 108 forms a circulation, and is communicated with cooling-water machine 109; Be provided with alkaline matter in the said waste gas He in the retracting device 105, said air extractor 106 is an air exhauster.
The course of work of said bleeder condensed gas recovery system is following; When agitated reactor 101 in when work; Because the various raw materials of preparation vanadium liquid react and can produce a large amount of sour gas in the agitated reactor 101, at this moment said bleeder condensed gas recovery system startup work, the air extractor 106 (air exhauster) in the system is opened and is used to take out the sour gas in agitated reactor 101 inner chamber body; All sour gas are along with the exhaust outlet that is provided with on the agitated reactor 101 107 is discharged; The sour gas of high temperature is known from experience along with exhaust outlet 107 and blast pipe get into condensing unit 104 (condensing tower), and the sour gas of high temperature is known from experience and condensing unit 104 in, realized cooling, the gas after the cooling can inflow exhaust gas in and retracting device 105; Be provided with alkaline matter in the said waste gas He in the retracting device 105, above-mentioned sour gas can effectively neutralize.Be provided with forniciform cool cycles pipeline in the said condensing unit 104 (condensing tower); This cool cycles pipeline is connected with cooling-water machine 109; Inject cold water in the cool cycles pipeline that can in condensing unit 104 (condensing tower), be provided with through cooling-water machine 109; Also can be through the cool cycles pipeline to entering into the high-temperature acidic gas cooling in the condensing unit 104 (condensing tower); At this moment, the outer wall of cool cycles pipeline can condense has water droplet, and the water droplet of gathering can be dropped in the bottom of condensing unit 104 (condensing tower); This ponding can flow into the water tank that is connected with condensing unit 104 (condensing tower) again and compile, and through the reaction needed of water tank according to agitated reactor 101 filler 111 of ponding through agitated reactor 101 is injected in the agitated reactor 101 again.
The present invention designs ingenious; Condensation bleeder vanadium liquid automatic preparation system is satisfying under a large amount of, efficient, automatic situation about in vanadium liquid agitated reactor 101, feeding intake through batch charger 120; Can effectively reclaim and dispose a large amount of high temperature, the corrosivity pernicious gas of discharging in the agitated reactor 101; And the Circulation and Hot Oil Spray system and the cold oil circulatory system can more effectively be guaranteed the reaction temperature in the agitated reactor 101.
Above content is to combine concrete optimal technical scheme to the further explain that the present invention did, and can not assert that practical implementation of the present invention is confined to these explanations.For the those of ordinary skill of technical field under the present invention, under the prerequisite that does not break away from the present invention's design, can also make some simple deduction or replace, all should be regarded as belonging to protection scope of the present invention.
Claims (10)
1. condensation bleeder vanadium liquid automatic preparation system is characterized in that: said condensation bleeder vanadium liquid automatic preparation system comprises the agitated reactor (101) that is used to prepare vanadium liquid, be used for the interior vanadium liquid of agitated reactor (101) is carried out the Circulation and Hot Oil Spray system of heat supply, the cold oil circulatory system that is used for the interior vanadium liquid of agitated reactor (101) is cooled off and goes up the bleeder condensed gas recovery system that the exhaust outlet (107) that is provided with is connected with agitated reactor (101);
Wherein, the pyrogenicity oil storage device (102) that refluxes again after through agitated reactor (101) circulation of the deep fat in the said Circulation and Hot Oil Spray system, the cold oil in the said cold oil circulatory system refrigeration oil storage device (103) that refluxes again after through agitated reactor (101) circulation;
Said bleeder condensed gas recovery system comprises: in condensing unit (104) that is connected with the exhaust outlet (107) of agitated reactor (101) and/or the waste gas and retracting device (105) and air extractor (106), in said condensing unit (104) and/or the waste gas and retracting device (105) be communicated with air extractor (106).
2. according to the said condensation bleeder of claim 1 vanadium liquid automatic preparation system; It is characterized in that: said bleeder condensed gas recovery system also comprises condensation water tank (110); Said condensation water tank (110) one ends are connected the other end with the output of said condensing unit (104) and insert said agitated reactor (101), are connected with the filler (111) of said agitated reactor (101).
3. according to the said condensation bleeder of claim 2 vanadium liquid automatic preparation system, it is characterized in that:
The condensing unit (104) that is connected with exhaust outlet (107) in the said bleeder condensed gas recovery system is a condensing tower; In the condensing tower set inside cooling line (108) is arranged; Said cooling line (108) forms a circulation, and is communicated with cooling-water machine (109).
4. according to the said condensation bleeder of claim 3 vanadium liquid automatic preparation system, it is characterized in that: be provided with alkaline matter in the said waste gas and in the retracting device (105).
5. according to the said condensation bleeder of claim 4 vanadium liquid automatic preparation system, it is characterized in that: said air extractor (106) is an air exhauster.
6. according to the said condensation bleeder of claim 1 vanadium liquid automatic preparation system; It is characterized in that: said Circulation and Hot Oil Spray system comprises deep fat storage device (102), deep fat heater (112); Wherein, Said deep fat storage device (102) forms operation cycle with said deep fat heater (112); Through said deep fat heater (112) oil in the said deep fat storage device (102) is heated to design temperature; Said deep fat storage device (102) forms operation cycle with agitated reactor (101), makes the stream of hot oil in the said deep fat storage device (102) in the outer chamber (113) of said agitated reactor (101), be back to deep fat storage device (102) again.
7. according to the said condensation bleeder of claim 6 vanadium liquid automatic preparation system, it is characterized in that: be provided with pipeline in the said deep fat heater (112), this pipeline one end is connected with cooling water pipe (114), and the other end is connected with drainpipe (115).
8. according to the said condensation bleeder of claim 1 vanadium liquid automatic preparation system; It is characterized in that: the said cold oil circulatory system comprises cold oil storage device (103); Said cold oil storage device (103) self has a circulatory system; Said in addition cold oil storage device (103) and agitated reactor (101) form operation cycle, cold oil in the said cold oil storage device (103) is flowed through be back to cold oil storage device (103) again in the outer chamber (113) of said agitated reactor (101).
9. said according to Claim 8 condensation bleeder vanadium liquid automatic preparation system is characterized in that: be provided with oily temperature cooling circuit (116) in the said cold oil storage device (103), said oil temperature cooling circuit (116) is connected with cooling-water machine (109).
10. according to the said condensation bleeder of claim 9 vanadium liquid automatic preparation system, it is characterized in that: the oil temperature of the cold oil of storage is at normal temperature or below the normal temperature in the said cold oil storage device (103).
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012103303191A CN102794144A (en) | 2012-09-07 | 2012-09-07 | Condensation air exhaust type vanadium liquid automatic preparation system |
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| Application Number | Priority Date | Filing Date | Title |
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| CN2012103303191A CN102794144A (en) | 2012-09-07 | 2012-09-07 | Condensation air exhaust type vanadium liquid automatic preparation system |
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| CN102794144A true CN102794144A (en) | 2012-11-28 |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101480599A (en) * | 2008-12-30 | 2009-07-15 | 吕德斌 | Technique for heating and cooling material in reactor by heat carrier through jacket |
| CN201276517Y (en) * | 2008-09-17 | 2009-07-22 | 桂林正东化工机械设备有限公司 | Glue production apparatus |
| US20110071330A1 (en) * | 2009-09-22 | 2011-03-24 | Fina Technology, Inc. | Offgas Stream Direct Contact Condenser |
| CN201990623U (en) * | 2011-03-01 | 2011-09-28 | 福建兴宇树脂有限公司 | Exhaust gas recycling device for polyurethane resin reactions |
| CN202410657U (en) * | 2011-12-02 | 2012-09-05 | 深圳市金钒能源科技有限公司 | Reaction kettle for preparing vanadium liquid and heating and cooling structure of reaction kettle |
-
2012
- 2012-09-07 CN CN2012103303191A patent/CN102794144A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN201276517Y (en) * | 2008-09-17 | 2009-07-22 | 桂林正东化工机械设备有限公司 | Glue production apparatus |
| CN101480599A (en) * | 2008-12-30 | 2009-07-15 | 吕德斌 | Technique for heating and cooling material in reactor by heat carrier through jacket |
| US20110071330A1 (en) * | 2009-09-22 | 2011-03-24 | Fina Technology, Inc. | Offgas Stream Direct Contact Condenser |
| CN201990623U (en) * | 2011-03-01 | 2011-09-28 | 福建兴宇树脂有限公司 | Exhaust gas recycling device for polyurethane resin reactions |
| CN202410657U (en) * | 2011-12-02 | 2012-09-05 | 深圳市金钒能源科技有限公司 | Reaction kettle for preparing vanadium liquid and heating and cooling structure of reaction kettle |
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Application publication date: 20121128 |