CN102755443A - Black-bone chicken and longan blood-nourishing oral liquid and preparation method thereof - Google Patents
Black-bone chicken and longan blood-nourishing oral liquid and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a preparation method of a black-bone chicken and longan blood-nourishing oral liquid. The method comprises the following steps of: (1) weighing black-bone chicken powder, longan pulp, barbary wolfberry fruit, Chinese date, potassium sorbate and stevioside; (2) adding an ethanol aqueous solution into the black-bone chicken powder, soaking, extracting, filtering, standing a filtrate, recovering ethanol from a supernatant, and concentrating into an extract; (3) adding water into longan pulp, barbary wolfberry fruit and Chinese date for decocting, filtering, and concentrating a filtrate into an extract; and (4) combining the extracts obtained in the steps (2) and (3), adding stevioside and potassium sorbate, adding water for adjusting the pH, filtering, and sterilizing a filtrate to obtain a black-bone chicken and longan blood-nourishing oral liquid. The oral liquid prepared with the method plays a role in relieving pregnancy reactions such as vomit, anorexia, monophagia, picky eating, diarrhea and the like of a pregnant woman and symptoms such as malnutrition, delicate constitution and the like, plays a role in treating a hepatic disease in pregnancy, anemia of pregnancy, swelling in pregnancy and slow growth and development of a fetus in utero, and can be used for nourishing liver and kidney, supplementing qi, nourishing blood and improving human immunity.
Description
Technical field
The present invention relates to a kind of tonifying liver medicine that nourishes blood, particularly relate to a kind of Gallus Domesticus Arillus Longan blood nourishing oral liquid and preparation method thereof.
Background technology
" women is this with blood ", blood transmits oxygen and various nutritional labeling in the health cyclic process, directly nourish the vital organs of the human body, helps to regulate the female incretion balance.The women is at surprised, pregnancy period, puerperal, the easy loss QI and blood of postoperative, if insufficiency of vital energy and blood influences menstruation, sleep interior, influences dark and gloomy, the jaundice of skin outside, and the people more is old for one's age.Discover among per 5 women 1 anemia is just arranged.In time benefiting qi and nourishing blood is all very important to each women.
Gallus Domesticus: having another name called Gallus Domesticus, is the distinctive medicinal rare bird of China.Modern medicine study, Gallus Domesticus include abundant melanin, protein, and 18 seed amino acids such as vitamin B group and 18 kinds of trace element, wherein the content of nicotinic acid, vitamin E, phosphorus, ferrum, potassium, sodium all is higher than common Carnis Gallus domesticus, and cholesterol and fat content are but very low.Total serum protein of Gallus Domesticus and globular protein content are all apparently higher than common chicken.Contain aminoacid in the blackbone Chicken and be higher than common chicken, and it is also high a lot of than common chicken to contain ferrum element, is the high tonic of nutritive value, is claimed that by people Gallus Domesticus is " dotey who has deceived the heart "; So Gallus Domesticus is a tonify deficiency labor, the first-class good merchantable brand of the body that takes care of health.Edible Gallus Domesticus can be improved physiological function, slow down aging, strengthening the tendons and bones.To preventing and treating osteoporosis, rickets, women's iron deficiency anemia etc. obvious effect is arranged.Compendium of Material Medica thinks that Gallus Domesticus has tonify deficiency labor thin and weak, and system is quenched one's thirst, and beneficial puerpera controls married woman's metrorrhagia leukorrhagia and some deficient all sick functions.
Fructus Jujubae: use the history in existing more than 2000 year as Chinese medicine, be mainly used in the just treatment of cards such as sugar, blood deficiency and yellow complexion, women's hysteria of deficiency of QI in middle-JIAO, weakness of the spleen and stomach, fatigue and asthenia, lack of appetite.
Pharmacological research is found in recent years, contains multiple bioactive substance in the Fructus Jujubae, like jujube polysaccharide, flavonoid, saponins, triterpenes, alkaloids, cyclic adenosine monophosphate (cAMP), cyclic guanosine monophosphate (cGMP) etc., human body is had the plurality kinds of health care effect of curing the disease.
Fructus Lycii: as Chinese medicine, it has the kidney invigorating and essence nourishing, nourishing the liver to improve visual acuity, blood-enriching tranquillizing, promoting the production of body fluid to quench thirst, the effect of nourishing the lung to arrest cough.Be used for the treating the liver kidney yin and lose, soreness of the waist and knees, dizziness, dizzy, the many tears of blurred vision, cough due to consumptive disease is quenched one's thirst, diseases such as seminal emission.
Arillus Longan: calm the nerves, control insomnia, forgetful, palpitation with fear.Ancients praise highly the nutritive value of Arillus Longan very much, have many herbal medicines all to introduce the nourishing and the health-care effect of these article.As far back as Han dynasty period, Arillus Longan is just as medicinal.So " Mingyi Bielu " is referred to as " Fructus Alpiniae Oxyphyllae ", says its function the heart nourishing and intellengence improving also.Nourishing and body-strengthening is arranged, heart tonifying and tranquilizing, the tonifying YANG of nourishing blood, strengthening the spleen appetizing, the effect of moistening skin beautifying.The sugar content of Arillus Longan is very high, and contains the glucose that can directly be absorbed by human body, and weak anemia is worn with age, weakness due to chronic disease, and often eat a little Arillus Longan has tonification very much; Women puerperal, Arillus Longan also is that food mended in important accent.Arillus Longan has benefiting QI and nourishing blood, and the effect of spleen invigorating reinforcing the heart is so there is the title of " superb work in the fruit ".The Shennong's Herbal record: Arillus Longan has the effect of treatment " the five internal organs pathogen, peace will anorexia ", claims " it is clever to obey strong soul for a long time, and it is not old to make light of one's life by commiting suicide, being proficient in the law of natural movement ".
The Arillus Longan sweet in the mouth is warm in nature, and GUIXIN, spleen channel are applicable to syndrome of deficiency of both heart and spleen and deficiency of both QI and blood patient.The traditional Chinese medical science is thought heart governing blood and vessels and mind, and is relevant with spirit, consciousness thinking activities.Spleen is the source of generating QI and blood day after tomorrow, and the nutrition of whole body is provided.If people's excessive thinking, impairment caused by overstrain heart spleen can cause symptoms such as severe palpitation, insomnia forgetfulness, spiritlessness and weakness.Heart spleen two warps are gone in the nourishing of the sweet temperature of Arillus Longan, and merit be apt to invigorating the heart and spleen, and sweet good to eat, do not grow greasyly, do not stop up gas, and reality is the good merchantable brand of reinforcing the heart spleen invigorating.Weakness due to chronic disease or old asthenia person often have the card of insufficiency of vital energy and blood, and show as pale or sallow complexion, fatigue and weakness, and diseases such as shortness of breath and palpitation, Arillus Longan is the reinforcing the heart spleen both, and replenishing QI and blood is sweet gentle again, and better curative effect is arranged.
Modern medicine study confirms that Arillus Longan contains protein, fat, saccharide, organic acid, crude fibre and multivitamin and mineral etc.Arillus Longan can suppress lipid peroxidation and improve activities of antioxidant enzymes, points out it that certain anti-aging effects is arranged.Arillus Longan has the human body immunity improving function, suppresses tumor cell, blood fat reducing, coronary blood flow increasing, effects such as enhancing body quality.
Although above-mentioned substance has pair human body that good effect is arranged, it is not too convenient to take.
Summary of the invention
The objective of the invention is to overcome the deficiency of prior art, a kind of Gallus Domesticus Arillus Longan blood nourishing oral liquid is provided.
Second purpose of the present invention provides a kind of method for preparing of Gallus Domesticus Arillus Longan blood nourishing oral liquid.
Technical scheme of the present invention is summarized as follows:
A kind of method for preparing of Gallus Domesticus Arillus Longan blood nourishing oral liquid comprises the steps:
(1) takes by weighing by mass percentage: Gallus Domesticus powder 20%～50%, Arillus Longan 5%～10%, Fructus Lycii 20%～40%, Fructus Jujubae 20%～40%; Potassium sorbate 0.01%～0.1%; Steviol glycosides 0.01%～0.1%;
(2) in mass ratio be the ratio of 1:5～15, it is 30%～70% ethanol water that said Gallus Domesticus powder is added volumetric concentration, and dipping extracted 12～36 hours; Filter; Collect filtrating, extract merging filtrate 1～3 time; Left standstill 30～60 hours, supernatant reclaims ethanol and is concentrated in the time of 60 ℃ relative density is 0.95～0.99 extractum;
(3) with said Arillus Longan, Fructus Lycii and Fructus Jujubae add 3～8 quality decocting doubly and boiled 20～60 minutes, filter, and collect filtrating, decoct merging filtrate and to be concentrated in the time of 60 ℃ relative density be 1.00～1.10 extractum 1～3 time;
(4) extractum with step (2) and (3) acquisition merges, and adds steviol glycosides and potassium sorbate, mixing, and 1.0～1.5 times water of the extractum quality after adding merges, adding citron acid for adjusting pH is 4.0～5.0, stirs 20～40 minutes; Filter, the body of will filtrating is packed in the Packaging Bottle; Damp and hot 100～120 ℃ of sterilizations of sterilization cabinet 30～60 minutes obtain a kind of Gallus Domesticus Arillus Longan blood nourishing oral liquid.
Step (1) is preferably: take by weighing by mass percentage: Gallus Domesticus powder 30%～40%, Arillus Longan 6%～8%, Fructus Lycii 25%～35%, Fructus Jujubae 25%～35%; Potassium sorbate 0.05%～0.1%; Steviol glycosides 0.03%～0.07%.
Step (2) is preferably: in mass ratio is the ratio of 1:8～11, and it is 40%～55% ethanol water that said Gallus Domesticus powder is added volumetric concentration, and dipping extracted 18～28 hours; Filter; Collect filtrating, extract merging filtrate 1～3 time; Left standstill 40～50 hours, supernatant reclaims ethanol and is concentrated in the time of 60 ℃ relative density is 0.95～0.99 extractum.
Step (2) is preferably: in mass ratio is the ratio of 1:9～10, and it is 40%～50% ethanol water that said Gallus Domesticus powder is added volumetric concentration, and dipping extracted 24 hours; Filter; Collect filtrating, extract merging filtrate 2 times; Left standstill 45～48 hours, supernatant reclaims ethanol and is concentrated in the time of 60 ℃ relative density is 0.97～0.98 extractum.
Step (3) is preferably: with said Arillus Longan, Fructus Lycii and Fructus Jujubae add 6 quality decocting doubly and boiled 40 minutes, filter, and collect filtrating, decoct merging filtrate and to be concentrated in the time of 60 ℃ relative density be 1.05 extractum 2 times.
Step (4) is preferably: the extractum of step (2) and (3) acquisition merged, adds steviol glycosides and potassium sorbate, and mixing, 1.3 times water of the extractum quality after adding merges, adding citron acid for adjusting pH is 4.3～4.7, stirs 30 minutes; Filter, the body of will filtrating is packed in the Packaging Bottle; The damp and hot 110 ℃ of sterilizations of sterilization cabinet 30 minutes promptly get.
The quality standard of Gallus Domesticus powder is: moisture: smaller or equal to 8.0%, the volatility alkaline matter: the sulphuric acid volumetric solution that consumes 0.005mol/L must not surpass 20.0ml; Nitrogen content: more than or equal to 6.0%.
A kind of Gallus Domesticus Arillus Longan blood nourishing oral liquid of method for preparing.
The experiment proof; Oral liquid of the present invention to pregnancy women because of vomiting, anorexia, partial eclipse, select gestation reaction such as food, diarrhoea; The malnutrition in various degree that causes, disease such as have a delicate constitution have mitigation; To pregnant hepatopathy, anemia during pregnancy, pregnancy general edema and fetal in utero growth promoter slowly four kinds of commonly encountered diseases therapeutical effect is arranged, through case, take oral liquid of the present invention and observe four kinds of diseases; Abnormal liver function, anemia, edema, fetal in utero growth promoter symptom slowly all alleviate, the disappearance that has.Oral liquid nourishing the liver and kidney of the present invention, benefiting QI and nourishing blood improve body immunity.
The specific embodiment
Below in conjunction with specific embodiment the present invention is further described.
Below the quality standard of the used Gallus Domesticus powder of each embodiment be: moisture: smaller or equal to 8.0%, the volatility alkaline matter: the sulphuric acid volumetric solution that consumes 0.005mol/L must not surpass 20.0ml; Nitrogen content: more than or equal to 6.0%.
What Gallus Domesticus powder adopted is each manufacturers produce, and the Gallus Domesticus powder that the quality standard of Gallus Domesticus powder is satisfied in assurance gets final product.
Embodiment 1
A kind of method for preparing of Gallus Domesticus Arillus Longan blood nourishing oral liquid comprises the steps:
(1) takes by weighing by mass percentage: Gallus Domesticus powder 35%, Arillus Longan 7%, Fructus Lycii 30%, Fructus Jujubae 27.9%; Potassium sorbate 0.07%; Steviol glycosides 0.03%;
(2) in mass ratio be the ratio of 1:9, it is 40% ethanol water that said Gallus Domesticus powder is added volumetric concentration, and dipping extracted 24 hours; Filter, collect filtrating, extract 2 times; Merging filtrate left standstill 48 hours, and supernatant reclaims ethanol and is concentrated in the time of 60 ℃ relative density is 0.97 extractum;
(3) with Arillus Longan, Fructus Lycii and Fructus Jujubae add 6 quality decocting doubly and boiled 40 minutes, filter, and collect filtrating, decoct merging filtrate and to be concentrated in the time of 60 ℃ relative density be 1.05 extractum 2 times;
(4) extractum with step (2) and (3) acquisition merges, and adds steviol glycosides and potassium sorbate, mixing, and 1.3 times water of the extractum quality after adding merges, adding citron acid for adjusting pH is 4.3, stirs 30 minutes; Filter, the body of will filtrating is packed in the Packaging Bottle; The damp and hot 110 ℃ of sterilizations of sterilization cabinet 30 minutes promptly get.
Embodiment 2
A kind of method for preparing of Gallus Domesticus Arillus Longan blood nourishing oral liquid comprises the steps:
(1) takes by weighing by mass percentage: Gallus Domesticus powder 30%, Arillus Longan 6%, Fructus Lycii 35%, Fructus Jujubae 28.88%; Potassium sorbate 0.05%; Steviol glycosides 0.07%;
(2) in mass ratio be the ratio of 1:10, it is 50% ethanol water that said Gallus Domesticus powder is added volumetric concentration, and dipping extracted 24 hours; Filter, collect filtrating, extract 2 times; Merging filtrate left standstill 45 hours, and supernatant reclaims ethanol and is concentrated in the time of 60 ℃ relative density is 0.98 extractum;
(3) with Arillus Longan, Fructus Lycii and Fructus Jujubae add 6 quality decocting doubly and boiled 40 minutes, filter, and collect filtrating, decoct merging filtrate and to be concentrated in the time of 60 ℃ relative density be 1.05 extractum 2 times;
(4) extractum with step (2) and (3) acquisition merges, and adds steviol glycosides and potassium sorbate, mixing, and 1.3 times water of the extractum quality after adding merges, adding citron acid for adjusting pH is 4.5, stirs 30 minutes; Filter, the body of will filtrating is packed in the Packaging Bottle; The damp and hot 110 ℃ of sterilizations of sterilization cabinet 30 minutes promptly get.
Embodiment 3
A kind of method for preparing of Gallus Domesticus Arillus Longan blood nourishing oral liquid comprises the steps:
(1) takes by weighing by mass percentage: Gallus Domesticus powder 40%, Arillus Longan 8%, Fructus Lycii 26.87%, Fructus Jujubae 25%; Potassium sorbate 0.1%; Steviol glycosides 0.03%;
(2) in mass ratio be the ratio of 1:11, it is 40% ethanol water that said Gallus Domesticus powder is added volumetric concentration, and dipping extracted 28 hours; Filter, collect filtrating, extract 3 times; Merging filtrate left standstill 40 hours, and supernatant reclaims ethanol and is concentrated in the time of 60 ℃ relative density is 0.96 extractum;
(3) with Arillus Longan, Fructus Lycii and Fructus Jujubae add 6 quality decocting doubly and boiled 40 minutes, filter, and collect filtrating, decoct merging filtrate and to be concentrated in the time of 60 ℃ relative density be 1.05 extractum 2 times;
(4) extractum with step (2) and (3) acquisition merges, and adds steviol glycosides and potassium sorbate, mixing, and 1.3 times water of the extractum quality after adding merges, adding citron acid for adjusting pH is 4.7, stirs 30 minutes; Filter, the body of will filtrating is packed in the Packaging Bottle; The damp and hot 110 ℃ of sterilizations of sterilization cabinet 30 minutes promptly get.
Embodiment 4
A kind of method for preparing of Gallus Domesticus Arillus Longan blood nourishing oral liquid comprises the steps:
(1) takes by weighing by mass percentage: Gallus Domesticus powder 31.9%, Arillus Longan 8%, Fructus Lycii 25%, Fructus Jujubae 35%; Potassium sorbate 0.05%; Steviol glycosides 0.05%;
(2) in mass ratio be the ratio of 1:8, it is 55% ethanol water that said Gallus Domesticus powder is added volumetric concentration, and dipping extracted 18 hours, filtered, and collected filtrating, leaves standstill 50 hours, and supernatant reclaims ethanol and is concentrated in the time of 60 ℃ relative density is 0.99 extractum;
(3) with said Arillus Longan, Fructus Lycii and Fructus Jujubae add 3 quality decocting doubly and boiled 60 minutes, filter, and collect filtrating, are concentrated in the time of 60 ℃ relative density and are 1.00 extractum;
(4) extractum that step (2) and (3) is obtained merges, and adds steviol glycosides and potassium sorbate, and mixing adds the 1.0 quality water doubly of the extractum quality after merging, and adding the citron acid for adjusting pH is 5.0, stirs 20 minutes; Filter, the body of will filtrating is packed in the Packaging Bottle; The damp and hot 110 ℃ of sterilizations of sterilization cabinet 60 minutes promptly get.
Embodiment 5
A kind of method for preparing of Gallus Domesticus Arillus Longan blood nourishing oral liquid comprises the steps:
(1) takes by weighing by mass percentage: Gallus Domesticus powder 20%, Arillus Longan 10%, Fructus Lycii 40%, Fructus Jujubae 29.89%; Potassium sorbate 0.1%; Steviol glycosides 0.01%;
(2) in mass ratio be the ratio of 1:9, it is 50% ethanol water that said Gallus Domesticus powder is added volumetric concentration, and dipping extracted 20 hours; Filter, collect filtrating, extract 2 times; Merging filtrate left standstill 45 hours, and supernatant reclaims ethanol and is concentrated in the time of 60 ℃ relative density is 0.95 extractum;
(3) with Arillus Longan, Fructus Lycii and Fructus Jujubae add 4 quality decocting doubly and boiled 50 minutes, filter, and collect filtrating, decoct merging filtrate and to be concentrated in the time of 60 ℃ relative density be 1.05 extractum 2 times;
(4) extractum with step (2) and (3) acquisition merges, and adds steviol glycosides and potassium sorbate, mixing, and 1.2 times water of the extractum quality after adding merges, adding citron acid for adjusting pH is 4.5, stirs 30 minutes; Filter, the body of will filtrating is packed in the Packaging Bottle; The damp and hot 110 ℃ of sterilizations of sterilization cabinet 45 minutes promptly get.
Embodiment 6
A kind of method for preparing of Gallus Domesticus Arillus Longan blood nourishing oral liquid comprises the steps:
(1) takes by weighing by mass percentage: Gallus Domesticus powder 50%, Arillus Longan 9.8%, Fructus Lycii 20%, Fructus Jujubae 20%; Potassium sorbate 0.1%; Steviol glycosides 0.1%;
(2) in mass ratio be the ratio of 1:5, it is 70% ethanol water that said Gallus Domesticus powder is added volumetric concentration, and dipping extracted 12 hours; Filter, collect filtrating, extract 3 times; Merging filtrate left standstill 30 hours, and supernatant reclaims ethanol and is concentrated in the time of 60 ℃ relative density is 0.99 extractum;
(3) with Arillus Longan, Fructus Lycii and Fructus Jujubae add 5 quality decocting doubly and boiled 40 minutes, filter, and collect filtrating, decoct merging filtrate and to be concentrated in the time of 60 ℃ relative density be 1.10 extractum 3 times;
(4) extractum with step (2) and (3) acquisition merges, and adds steviol glycosides and potassium sorbate, mixing, and 1.4 times water of the extractum quality after adding merges, adding citron acid for adjusting pH is 4.2, stirs 40 minutes; Filter, the body of will filtrating is packed in the Packaging Bottle; The damp and hot 120 ℃ of sterilizations of sterilization cabinet 30 minutes promptly get.
Embodiment 7
A kind of method for preparing of Gallus Domesticus Arillus Longan blood nourishing oral liquid comprises the steps:
(1) takes by weighing by mass percentage: Gallus Domesticus powder 24.94%, Arillus Longan 5%, Fructus Lycii 30%, Fructus Jujubae 40%; Potassium sorbate 0.01%; Steviol glycosides 0.05%;
(2) in mass ratio be the ratio of 1:15, it is 30% ethanol water that said Gallus Domesticus powder is added volumetric concentration, and dipping extracted 36 hours, filtered, and collected filtrating, leaves standstill 60 hours, and supernatant reclaims ethanol and is concentrated in the time of 60 ℃ relative density is 0.95 extractum;
(3) with Arillus Longan, Fructus Lycii and Fructus Jujubae add 8 quality decocting doubly and boiled 20 minutes, filter, and collect filtrating, decoct merging filtrate and to be concentrated in the time of 60 ℃ relative density be 1.05 extractum 2 times;
(4) extractum with step (2) and (3) acquisition merges, and adds steviol glycosides and potassium sorbate, mixing, and 1.5 times water of the extractum quality after adding merges, adding citron acid for adjusting pH is 4.0, stirs 30 minutes; The body of will filtrating is packed in the Packaging Bottle; The damp and hot 100 ℃ of sterilizations of sterilization cabinet 60 minutes promptly get.
The product inspection method of each embodiment preparation:
[inspection] pH value should be 4.0-5.0
Relative density should be 0.98-1.10
[assay] precision is measured these article 40ml, measures according to N2 method (an appendix IX of Chinese Pharmacopoeia version in 2010 L first method), promptly gets.
The every 1ml of these article nitrogenous (N) must not measure and is less than 0.6mg.
Clinical efficacy (Tianjin obstetrics and gynecology hospital: doctor Hu, doctor Liu)
Hospital finds in the clinical practice of decades; Pregnancy women because of vomiting, anorexia, partial eclipse, select gestation reaction such as food, diarrhoea; All in various degree the appearance malnutrition, disease such as have a delicate constitution; Clinically be reflected as that anemia, edema, embryo growth and development are bad more, visceral dysfunction etc., had a strong impact on the healthy of anemia of pregnant woman, also directly influenced the fetus normal growth and grown.So pregnant hepatopathy, anemia during pregnancy, pregnancy general edema and fetal in utero growth promoter four kinds of commonly encountered diseases totally five ten routine cases have slowly been selected by hospital, observe with product of the present invention.Through finding after the medication in nearly three months that abnormal liver function, anemia, edema, fetal in utero growth promoter symptom slowly all alleviate, the disappearance that has.Below be clinical data:
A kind of Gallus Domesticus Arillus Longan blood nourishing oral liquid of each embodiment preparation, every bottled amount 10ml.
Table 1-1 gestation hepatopathy
Table 1-2
Annotate: according to the assay of clinical disease, total case 5 examples, produce effects 5 examples, obvious effective rate is 100%.
Table 2 anemia during pregnancy
Annotate: according to the assay of clinical disease, total case 7 examples, produce effects 7 examples, obvious effective rate is 100%.
Table 3-1 fetal in utero retarded growth
Table 3-2
Annotate: according to the assay of clinical disease, total effective rate is 100%, produce effects 5 examples wherein, and obvious effective rate is 83%; Effective 1 example, effective percentage are 17%.
Table 4-1 pregnancy general edema
Table 4-2
Annotate: according to the assay of clinical disease, total effective rate is 100%, produce effects 15 examples wherein, and obvious effective rate is 71.4%; Effective 6 examples, effective percentage are 28.6%.
Above-mentioned observation on Clinical Application proves that the present invention has the effect of good nutritious tonifying, its ability QI replenishing and blood tonifying, nourishing heart spleen, flat invigorating the liver and kidney.For pregnancy women; Can adjust gastrointestinal function, stimulating appetite, improvement sleep especially; Thereby promoted the normal growth promoter of fetus to cause a series of clinical symptoms owing to the many malnutrition of pregnant women and body are empty; The nutrition increase of these article of taking back, system are strengthened, and the whole health level of anemia of pregnant woman all improves.
Claims (8)
1. the method for preparing of a Gallus Domesticus Arillus Longan blood nourishing oral liquid is characterized in that comprising the steps:
(1) takes by weighing by mass percentage: Gallus Domesticus powder 20%～50%, Arillus Longan 5%～10%, Fructus Lycii 20%～40%, Fructus Jujubae 20%～40%; Potassium sorbate 0.01%～0.1%; Steviol glycosides 0.01%～0.1%;
(2) in mass ratio be the ratio of 1:5～15, it is 30%～70% ethanol water that said Gallus Domesticus powder is added volumetric concentration, and dipping extracted 12～36 hours; Filter; Collect filtrating, extract merging filtrate 1～3 time; Left standstill 30～60 hours, supernatant reclaims ethanol and is concentrated in the time of 60 ℃ relative density is 0.95～0.99 extractum;
(3) with said Arillus Longan, Fructus Lycii and Fructus Jujubae add 3～8 quality decocting doubly and boiled 20～60 minutes, filter, and collect filtrating, decoct merging filtrate and to be concentrated in the time of 60 ℃ relative density be 1.00～1.10 extractum 1～3 time;
(4) extractum with step (2) and (3) acquisition merges, and adds steviol glycosides and potassium sorbate, mixing, and 1.0～1.5 times water of the extractum quality after adding merges, adding citron acid for adjusting pH is 4.0～5.0, stirs 20～40 minutes; Filter, the body of will filtrating is packed in the Packaging Bottle; Damp and hot 100～120 ℃ of sterilizations of sterilization cabinet 30～60 minutes obtain a kind of Gallus Domesticus Arillus Longan blood nourishing oral liquid.
2. the method for preparing of a kind of Gallus Domesticus Arillus Longan blood nourishing oral liquid according to claim 1 is characterized in that said step (1) is: take by weighing by mass percentage: Gallus Domesticus powder 30%～40%, Arillus Longan 6%～8%, Fructus Lycii 25%～35%, Fructus Jujubae 25%～35%; Potassium sorbate 0.05%～0.1%; Steviol glycosides 0.03%～0.07%.
3. the method for preparing of a kind of Gallus Domesticus Arillus Longan blood nourishing oral liquid according to claim 1, it is characterized in that said step (2) is: in mass ratio is the ratio of 1:8～11, it is 40%～55% ethanol water that said Gallus Domesticus powder is added volumetric concentration; Dipping extracted 18～28 hours, filtered, and collected filtrating; Extract 1～3 time; Merging filtrate left standstill 40～50 hours, and supernatant reclaims ethanol and is concentrated in the time of 60 ℃ relative density is 0.95～0.99 extractum.
4. the method for preparing of a kind of Gallus Domesticus Arillus Longan blood nourishing oral liquid according to claim 3, it is characterized in that said step (2) is: in mass ratio is the ratio of 1:9～10, it is 40%～50% ethanol water that said Gallus Domesticus powder is added volumetric concentration; Dipping extracted 24 hours, filtered, and collected filtrating; Extract 2 times; Merging filtrate left standstill 45～48 hours, and supernatant reclaims ethanol and is concentrated in the time of 60 ℃ relative density is 0.97～0.98 extractum.
5. the method for preparing of a kind of Gallus Domesticus Arillus Longan blood nourishing oral liquid according to claim 1; It is characterized in that said step (3) is: with said Arillus Longan, Fructus Lycii and Fructus Jujubae add 6 quality decocting doubly and boiled 40 minutes; Filter; Collect filtrating, decoct 2 times, merging filtrate and to be concentrated in the time of 60 ℃ relative density be 1.05 extractum.
6. the method for preparing of a kind of Gallus Domesticus Arillus Longan blood nourishing oral liquid according to claim 1; It is characterized in that said step (4) is: the extractum of step (2) and (3) acquisition is merged; Add steviol glycosides and potassium sorbate, mixing, 1.3 times water of the extractum quality after adding merges; Adding the citron acid for adjusting pH is 4.3～4.7, stirs 30 minutes; Filter, the body of will filtrating is packed in the Packaging Bottle; The damp and hot 110 ℃ of sterilizations of sterilization cabinet 30 minutes promptly get.
7. according to the method for preparing of the described a kind of Gallus Domesticus Arillus Longan blood nourishing oral liquid of one of claim 1～6; The quality standard that it is characterized in that said Gallus Domesticus powder is: moisture: smaller or equal to 8.0%, the volatility alkaline matter: the sulphuric acid volumetric solution that consumes 0.005mol/L must not surpass 20.0ml; Nitrogen content: more than or equal to 6.0%.
8. a kind of Gallus Domesticus Arillus Longan blood nourishing oral liquid of the method for one of claim 1～7 preparation.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012102730902A CN102755443A (en) | 2012-08-02 | 2012-08-02 | Black-bone chicken and longan blood-nourishing oral liquid and preparation method thereof |
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| CN2012102730902A CN102755443A (en) | 2012-08-02 | 2012-08-02 | Black-bone chicken and longan blood-nourishing oral liquid and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109674058A (en) * | 2019-02-28 | 2019-04-26 | 江西普正制药有限公司 | A kind of Cortex Eucommiae Gallus domesticlus brisson preparation and preparation method thereof |
| CN110074341A (en) * | 2019-04-26 | 2019-08-02 | 普正药业集团股份有限公司 | A kind of Gallus domesticlus brisson Orally taken product and preparation method thereof |
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| CN101322520A (en) * | 2008-07-23 | 2008-12-17 | 内蒙古伊利实业集团股份有限公司 | Freezing beverage containing red date, longan and medlar juice and preparation thereof |
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| CN101322520A (en) * | 2008-07-23 | 2008-12-17 | 内蒙古伊利实业集团股份有限公司 | Freezing beverage containing red date, longan and medlar juice and preparation thereof |
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| 国家食品药品监督管理局 中国新闻社编辑: "《国家中药品种选编》", 31 January 2005 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109674058A (en) * | 2019-02-28 | 2019-04-26 | 江西普正制药有限公司 | A kind of Cortex Eucommiae Gallus domesticlus brisson preparation and preparation method thereof |
| CN110074341A (en) * | 2019-04-26 | 2019-08-02 | 普正药业集团股份有限公司 | A kind of Gallus domesticlus brisson Orally taken product and preparation method thereof |
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Application publication date: 20121031 |