CN102745732B - Barium chloride reactor - Google Patents

Barium chloride reactor Download PDF

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Publication number
CN102745732B
CN102745732B CN201110109283.XA CN201110109283A CN102745732B CN 102745732 B CN102745732 B CN 102745732B CN 201110109283 A CN201110109283 A CN 201110109283A CN 102745732 B CN102745732 B CN 102745732B
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CN
China
Prior art keywords
pipe
reactor body
reactor
hydrochloric acid
feed
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201110109283.XA
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Chinese (zh)
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CN102745732A (en
Inventor
褚明武
曹刚
牟龙云
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SHANDONG ZHONGCHENG BARIUM SLAT CO Ltd
Original Assignee
SHANDONG ZHONGCHENG BARIUM SLAT CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SHANDONG ZHONGCHENG BARIUM SLAT CO Ltd filed Critical SHANDONG ZHONGCHENG BARIUM SLAT CO Ltd
Priority to CN201110109283.XA priority Critical patent/CN102745732B/en
Publication of CN102745732A publication Critical patent/CN102745732A/en
Application granted granted Critical
Publication of CN102745732B publication Critical patent/CN102745732B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)

Abstract

The invention relates to a barium chloride reactor, characterized in that the barium chloride reactor comprises a reactor body, a feeding pipe, a gas discharge pipe, an anger, a motor, a residue discharge pipe, a hydrochloric acid feeding pipe, a finished liquid outlet and a star-shaped valve, wherein the reactor body is obliquely mounted, one side with lower horizontal position of the bottom of the reactor body is provided with the finished liquid outlet, one side with higher horizontal position of the bottom of the reactor body is provided with the residue discharge pipe, the anger is arranged in the reactor body, the anger is connected with the motor, the top end of the reactor body is provided with the feeding pipe and the gas discharge pipe, and the side wall of the reactor body is provided with the hydrochloric acid feeding pipe. The barium chloride reactor disclosed herein overcomes most problems, realizes the continuous production of barium chloride, simultaneously raises the purity of carbon dioxide, is convenient for recovering carbon dioxide, that is, the resource is saved, and the environment is protected.

Description

Bariumchloride reactor
Technical field
The present invention relates to a kind of bariumchloride reactor, belong to field of chemical equipment.
Background technology
In in the past traditional bariumchloride reaction process, all use reactor, hydrochloric acid and barium carbonate are added in reactor, again finished fluid is released after having reacted, so virtually just limit reaction process for interrupted reaction, so namely, consume the energy, lavish labor on again, production efficiency is low simultaneously, to realizing automatically controlling and streamlined operation very unfavorable, also be difficult to accomplish scale production, and produce with reactor, long reaction time, interruptedization is produced, make to reclaim the carbonic acid gas produced in reaction process very difficult, some carbonic acid gas must be discharged in air, this just causes the pollution to environment, also result in the waste of raw material simultaneously, and use reactor to produce bariumchloride, the electric energy that the whipping device of reactor consumes also is very large.
Summary of the invention
According to the deficiencies in the prior art, technical problem to be solved by this invention is: provide a kind of bariumchloride reactor, realize the continuous prodution of bariumchloride, is convenient to reclaim carbonic acid gas, without the need to the whipping device of complexity.
The technical solution adopted for the present invention to solve the technical problems is: provide a kind of bariumchloride reactor, it is characterized in that comprising: reactor body, feed-pipe, gas discharge pipe, screw feeder, motor, scum pipe, hydrochloric acid feed-pipe, finished fluid outlet and star valve, reactor body is that tilting is installed, the side that reactor body horizontal position sets low is provided with finished fluid outlet, higher side, reactor body bottom level position is provided with scum pipe, in reactor body, screw feeder is installed, screw feeder connects motor, reactor body top is provided with feed-pipe and gas discharge pipe, reactor body sidewall is provided with hydrochloric acid feed-pipe.
Described feed-pipe is provided with star valve.
Described scum pipe is provided with star valve.
Described motor is arranged on and exports relative side with finished fluid.
Described hydrochloric acid feed-pipe is arranged on the side near motor.Such setting ensure that the charging of hydrochloric acid and the discharge of waste residue are in the other direction, this ensure that the denseest hydrochloric acid fully contacts with the barium carbonate of least easily reaction, shorten the time that reaction is used.
During use, Ba carbonate solid enters from feed-pipe, controlled by planet valve, barium carbonate after entering reacts with the hydrochloric acid entered through persalt feed-pipe, because reactor body is tilted-putted, first solid carbonic acid calcium used and hydrochloric acid can arrive the lower position reaction of level attitude, this reactive site exports near finished fluid, by the stirring of screw feeder, barium carbonate and hydrochloric acid are fully reacted, after the finished fluid reacted has been saved bit by bit many, when arriving finished fluid outlet, finished fluid can flow out automatically, unreacted completely barium carbonate transports through screw feeder, tilt upward away, the hydrochloric acid entered from hydrochloric acid feed-pipe at the same time flows down in the other direction with barium carbonate, continue to react with the barium carbonate for having reacted, residue after reaction, be transported to scum pipe by screw feeder to discharge, scum pipe is controlled by planet valve.
The invention has the beneficial effects as follows:
(1) this equipment overcomes most of problem, achieves the continuous prodution of bariumchloride, simultaneously improves the purity of carbonic acid gas, is more convenient to the recovery of carbonic acid gas, has namely saved resource, protects environment again simultaneously;
(2) by hydrochloric acid charging and the reciprocal setting of waste sludge discharge, make the reaction of barium carbonate more abundant, substantially reduce the reaction times;
(3) production of bariumchloride achieves serialization, the Automated condtrol of equipment is more prone to, is easy to the production of large-scale;
(4) deduct complicated whipping device in this equipment, saved a large amount of electric energy, while reducing production cost, also a saving the energy.
Accompanying drawing explanation
Fig. 1 is structural representation of the present invention;
In figure, 1 is reactor body; 2 is feed-pipe; 3 is gas discharge pipe; 4 is screw feeder; 5 is motor; 6 is scum pipe; 7 is hydrochloric acid feed-pipe; 8 is finished fluid outlet; 9 is star valve.
Embodiment
Below in conjunction with accompanying drawing, embodiments of the invention are described further:
As described in Figure 1, the present invention includes: reactor body 1, feed-pipe 2, gas discharge pipe 3, screw feeder 4, motor 5, scum pipe 6, hydrochloric acid feed-pipe 7, finished fluid outlet 8 and star valve 9, reactor body 1 is tilting installation, the side that reactor body 1 horizontal position sets low is provided with finished fluid outlet 8, higher side, reactor body 1 bottom level position is provided with scum pipe 6, screw feeder 4 is installed in reactor body 1, screw feeder 4 connects motor 5, reactor body 1 top is provided with feed-pipe 2 and gas discharge pipe 3, and reactor body 1 sidewall is provided with hydrochloric acid feed-pipe 7.
Feed-pipe 2 is provided with star valve 9.
Scum pipe 6 is provided with star valve 9.
Motor 5 is arranged on and exports 8 relative sides with finished fluid.
Hydrochloric acid feed-pipe 7 is arranged on the side near motor 5.Such setting ensure that the charging of hydrochloric acid and the discharge of waste residue are in the other direction, this ensure that the denseest hydrochloric acid fully contacts with the barium carbonate of least easily reaction, shorten the time that reaction is used.
During use, Ba carbonate solid enters from feed-pipe 2, 9 are controlled by planet valve, barium carbonate after entering reacts with the hydrochloric acid entered through persalt feed-pipe 7, because reactor body 1 is tilted-putted, first solid carbonic acid calcium used and hydrochloric acid can arrive the lower position reaction of level attitude, this reactive site is near finished fluid outlet 8, by the stirring of screw feeder 4, barium carbonate and hydrochloric acid are fully reacted, after the finished fluid reacted has been saved bit by bit many, when arrival finished fluid exports 8, finished fluid can flow out automatically, unreacted completely barium carbonate transports through screw feeder 4, tilt upward away, the hydrochloric acid entered from hydrochloric acid feed-pipe 7 at the same time flows down in the other direction with barium carbonate, continue to react with the barium carbonate for having reacted, residue after reaction, be transported to scum pipe 6 by screw feeder 4 to discharge, scum pipe 6 controls 9 by planet valve.

Claims (2)

1. a bariumchloride reactor, it is characterized in that comprising: reactor body (1), feed-pipe (2), gas discharge pipe (3), screw feeder (4), motor (5), scum pipe (6), hydrochloric acid feed-pipe (7), finished fluid outlet (8) and star valve (9), reactor body (1) is tilting installation, the side that reactor body (1) horizontal position sets low is provided with finished fluid outlet (8), higher side, reactor body (1) bottom level position is provided with scum pipe (6), screw feeder (4) is installed in reactor body (1), screw feeder (4) connects motor (5), reactor body (1) top is provided with feed-pipe (2) and gas discharge pipe (3), reactor body (1) sidewall is provided with hydrochloric acid feed-pipe (7),
Described feed-pipe (2) is provided with star valve (9);
Described scum pipe (6) is provided with star valve (9);
Described motor (5) is arranged on and exports (8) relative side with finished fluid.
2. bariumchloride reactor according to claim 1, is characterized in that described hydrochloric acid feed-pipe (7) is arranged on the side near motor (5).
CN201110109283.XA 2011-04-22 2011-04-22 Barium chloride reactor Expired - Fee Related CN102745732B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201110109283.XA CN102745732B (en) 2011-04-22 2011-04-22 Barium chloride reactor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201110109283.XA CN102745732B (en) 2011-04-22 2011-04-22 Barium chloride reactor

Publications (2)

Publication Number Publication Date
CN102745732A CN102745732A (en) 2012-10-24
CN102745732B true CN102745732B (en) 2015-07-15

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Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103288117B (en) * 2013-06-18 2016-02-03 滨州坤宝化工有限责任公司 A kind of High Purity Hydrogen barium oxide produce in the treatment process of waste water and equipment

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101654274A (en) * 2009-09-15 2010-02-24 赖成文 Barium chloride production technology
CN101941729A (en) * 2009-07-07 2011-01-12 付远征 Technology for preparing barium sulfate by witherite
CN201990500U (en) * 2011-04-22 2011-09-28 山东众诚钡盐股份有限公司 Barium chloride reactor

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101941729A (en) * 2009-07-07 2011-01-12 付远征 Technology for preparing barium sulfate by witherite
CN101654274A (en) * 2009-09-15 2010-02-24 赖成文 Barium chloride production technology
CN201990500U (en) * 2011-04-22 2011-09-28 山东众诚钡盐股份有限公司 Barium chloride reactor

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Granted publication date: 20150715

Termination date: 20160422