CN102720920A - Vacuum insulation board core material and manufacture method of vacuum insulation board core material - Google Patents

Vacuum insulation board core material and manufacture method of vacuum insulation board core material Download PDF

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Publication number
CN102720920A
CN102720920A CN201210187543XA CN201210187543A CN102720920A CN 102720920 A CN102720920 A CN 102720920A CN 201210187543X A CN201210187543X A CN 201210187543XA CN 201210187543 A CN201210187543 A CN 201210187543A CN 102720920 A CN102720920 A CN 102720920A
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CN
China
Prior art keywords
glass fibre
fibre cotton
core material
core
produced
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201210187543XA
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Chinese (zh)
Inventor
翟传伟
李壮贤
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Qingdao Creek New Environmental Materials Co Ltd
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Qingdao Creek New Environmental Materials Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Qingdao Creek New Environmental Materials Co Ltd filed Critical Qingdao Creek New Environmental Materials Co Ltd
Priority to CN201210187543XA priority Critical patent/CN102720920A/en
Publication of CN102720920A publication Critical patent/CN102720920A/en
Pending legal-status Critical Current

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Abstract

The invention relates to a vacuum insulation board core material and a manufacture method of the vacuum insulation board core material. The vacuum insulation board core material is manufactured by mixing glass fiber cotton which has the diameter being 3.5 to 5mum and the length being 5 to 20mm and is produced by a centrifugal method, with glass fiber cotton which has the diameter being 1.5 to 2.5 mum and the length being 1 to 5mm and is produced by a flame method, the glass fiber cotton produced by the flame method accounts for 70 percent, and the glass fiber cotton produced by the centrifugal method accounts for 30 percent. The manufacture method of the insulation board core material comprises the following steps of glass fiber cotton mixing, pulp forming through water addition and stirring, dehydration forming, surface flattening, vacuum dehydration, drying, cooling and cutting.

Description

Core material of vacuum heat insulation plate and preparation method thereof
Technical field
The present invention relates to a kind of core material of vacuum heat insulation plate and preparation method thereof, be specifically a kind of be the method that raw material is made insulated panel core material with the glass fibre cotton.
Background technique
At present, vacuum heat-insulating plate has applied in the every field, and it satisfies with the characteristic of energy-conservation, low-carbon (LC), environmental protection, safety
Customer requirement.Can know with practical operation through investigation, vacuum heat-insulating plate inside core select for use with making method to tool each item property
Can the influence very big, core-as select porous media material for use, like aerogel, little { L polyurethane, SiO 2 powder, asbestos fiber, glass fibre etc.The against vacuum insulated panel core material must possess following four specific characters: 1, under the high vacuum negative pressure state, vacuum heat-insulating plate is had supporting effect, prevent that vacuum heat-insulating plate from shrinking, caving in; 2, to reduce heat conducting generation as much as possible, prolong heat conducting path; 3, must possess open-celled structure, gas can be discharged with prestissimo under negative pressure state; 4, material need possess and prevents thermal-radiating performance.
At present because of different types of vacuum heat-insulating plate application is different, the selection of its core is difference to some extent also, requires to hinder good in thermal property for household electrical appliances insulation, building exterior wall heat preserving etc.; Thermal conductivity is low; The thermal conductivity of the exhausted plate of present most of vacuum is all between 0.01-0.02W/m.K, and core material of vacuum heat insulation plate is bulky, and thickness is generally between lcm-5cm; After being used for household electrical appliances insulations, building exterior wall heat preserving, space capable of using and the insulation life-span of having reduced household electrical appliances, building are short.So, hope that the attenuation of vacuum insulation plate thickness, thermal conductivity reduce to household electrical appliances and building exterior wall heat preserving, reduce the cost of production of vacuum heat-insulating plate simultaneously, these are real to be the current problem that needs research.
Summary of the invention
Goal of the invention: the objective of the invention is in order to overcome the deficiency of existing technology, low core material of vacuum heat insulation plate such as a kind of cost that is used for household electrical appliances insulation, building exterior wall heat preserving etc. and preparation method thereof is provided.
Technological scheme: in order to solve the problems of the technologies described above; The invention provides---planting by diameter is 3.5-5um; Length is that glass fibre cotton and the diameter that 5-20mm centrifuge method is produced is 1.5-2.5um; Length is that the glass fibre cotton that 1-5mm flame method is produced is mixed and made into: the glass fibre cotton that said flame method is produced accounts for 70wt%, and the glass fibre cotton that said centrifuge method is produced accounts for 30wt%.
Because what adopt during centrifuge method is produced all is discarded cullet, cost of material is low, the diameter 35 that produces simultaneously-
5um, the glass fibre cotton of length 5-20mm use the relative cost of manufacturing mechanism low, so the glass fibre cotton cost that obtains is low, thereby adopt diameter 3.5-5um, and the vacuum heat-insulating plate cost that the glass fibre cotton of length 5-20mm is made is low.
And the glass fibre cotton that adopts flame method to make, diameter is short, and the glass fibre cotton density that obtains is bigger, and the core material of vacuum heat insulation plate thermal conductivity of processing is lower, but the glass fibre cotton manufacturing cost that adopts flame method to produce is high.
The concrete steps that the invention also discloses a kind of this making method of manufacture method of core material of vacuum heat insulation plate are following:
(1) cut-off directly is 3.5-5um, and glass fibre cotton and diameter that length is produced for the 5-20mm centrifuge method are 1.5-2.5um, and length is the glass fibre cotton that 1-5mm flame method is produced; The glass fibre cotton that said flame method is produced accounts for 70wt%, and the glass fibre cotton that said centrifuge method is produced accounts for 30wt%;
(2) two kinds of glass fibre cottons added to send into after water stirs join stock tank dilution, diluted concentration to 0.3-0.6%:
(3) will dilute good glass fibre cotton slurries sends into and holds stock tank;
The slurry that (4) will hold in the stock tank is sent into breast box, adopts forming net to the glass fibre cotton moulding of dewatering then, processes glass fibre cotton core blank;
(5) adopt pressure roller to glass fibre core blank carry out vertically, lateral surfaces is smooth, simultaneously the thickness of glass fibre core blank adjusted, and makes glass fibre core blank thickness unanimity;
(6) environment that the glass fibre core blank that will accomplish shaping is put into negative pressure of vacuum with glass fibre core blank 60%-
70% moisture removal;
(7) the glass fibre core blank that will remove 60%-70% moisture is then sent into baking and curing in the roasting chamber, and baking the temperature inside the box is controlled at 250-400 degree centigrade, and stoving time is 3-15 minutes; After accomplishing, baking forms the whole plate of glass fibre core;
(8) then the whole plate of glass fibre core is cooled to normal temperature;
(9) according to customer requirement the whole plate of glass fibre core is carried out cutting, the glass fibre core of the standard that completes.
Glass fibre core blank thickness is 0 5-30mm in the step described in the present invention (5).Because making the glass fibre cotton of central layer employing is that diameter is 3.5-5um, length is the glass fibre cotton that the 5-20mm centrifuge method is produced, and said glass fibre core blank optimum thickness is 0.5-8mm.
When (4) forming net dewaters to glass fibre cotton in the step described in the present invention, the speed of forming net be 2-5 rice/minute.Adopt in the glass fibre cotton core blank that this speed can effectively guarantee to produce through forming net glass fibre cotton density even, integral thickness is even relatively, does not occur high low situation on one side on one side, has improved the core material of vacuum heat insulation plate of producing
End product quality.
Beneficial effect: core material of vacuum heat insulation plate according to the invention has the following advantages:
1, adopt glass fibre cotton that glass fibre cotton that 30 wt% centrifuge method produce and 70 wt% flame method produce as the core material of vacuum heat insulation plate raw material among the present invention, the vacuum heat-insulating plate of producing; The core thermal conductivity is at 0.0025-0004W/m; K; Its heat insulating coefficient with respect to the glass fibre cotton that adopts 100% flame method to produce be the core material of vacuum heat insulation plate of raw material high 0.0005 W/m.k; The heat insulation effect influence is little, the manufacture cost of but having practiced thrift core material of vacuum heat insulation plate greatly; And the thickness of core for o.5-8mm, thickness and the glass fibre cotton that adopts 100% flame method to produce are that the core material of vacuum heat insulation plate of raw material is more or less the same.
2, core material of vacuum heat insulation plate according to the invention has open-celled structure speed exhaust performance.
3, the glass fibre cotton that centrifuge method is produced among the present invention has flame retardant property, and the vacuum heat-insulating plate using scope of producing is extensive.Can satisfy sound-absorbing, nontoxic, environmental protection requirement.
4, process for integrally manufacturing of the present invention is simple, adapts to industrialized production.
Embodiment
Below in conjunction with specific embodiment, further illustrate the present invention, should understand that these embodiments only are used to explain wood invention and
Be not used in restriction scope of the present invention, after having read the present invention, those skilled in the art are to the various equivalent form of values of wood invention
Modification all fall within the application's accompanying claims and limit.
Embodiment
A kind of core material of vacuum heat insulation plate, it is 3.5-5um by diameter, and length is that glass fibre cotton and the diameter that 5-20mm centrifuge method is produced is 1.5-2.5um, and length is that the glass fibre cotton that 1-5mm flame method is produced is mixed and made into; The glass fibre cotton that said flame method is produced accounts for 70 wt%, and the glass fibre cotton that said centrifuge method is produced accounts for 30 wt%.
[00,171 one kind of manufacture method of core material of vacuum heat insulation plate, concrete steps are following:
(1) cut-off directly is 3.5-5um; Length is that glass fibre cotton and the diameter that 5-20mm centrifuge method is produced is 1 5-2.5um; Length is the glass fibre cotton that 1-5mm flame method is produced: the glass fibre cotton that said flame method is produced accounts for 70 wt%, and the glass fibre cotton that said centrifuge method is produced accounts for 30 wt%;
(2) two kinds of glass fibre cottons are added to send into after water stirs join stock tank dilution, diluted concentration is to o.4%
(3) will dilute good glass fibre cotton slurries sends into and holds stock tank;
The slurry that (4) will hold in the stock tank is sent into breast box, adopts forming net to the glass fibre cotton moulding of dewatering then, processes glass fibre cotton core blank; When forming net dewatered to glass fibre cotton in this step, the speed of forming net was 2 meters/minute:
(5) adopt the twice pressure roller to glass fibre core blank increase the weight of to compress into row vertically, horizontal table and smooth, simultaneously the thickness of glass fibre core blank is adjusted, make glass fibre core blank thickness be adjusted into 3mm;
(6) the glass fibre core blank that will accomplish shaping is put into the moisture removal of the environment of negative pressure of vacuum with glass fibre core blank 60%, makes glass fibre core blank water content be controlled at 40%:
(7) the glass fibre core blank that will remove 60% moisture is then sent into baking and curing in the roasting chamber, and baking the temperature inside the box is controlled at 350 degrees centigrade, and stoving time is 8 minutes; After accomplishing, baking forms the whole plate of glass fibre core
(8) then the whole plate of glass fibre core is cooled to normal temperature;
(9) according to customer requirement the whole plate of glass fibre core is carried out cutting, cut into the square core material of vacuum heat insulation plate finished product of 5mm X 5mm.

Claims (10)

1. an insulated panel core material is 3.5-5um by diameter, and length is that glass fibre cotton and the diameter that 5-20mm centrifuge method is produced is 1.5-2.5um, and length is that the glass fibre cotton that 1-5mm flame method is produced is mixed and made into; The glass fibre cotton that said flame method is produced accounts for 70%, and the glass fibre cotton that said centrifuge method is produced accounts for 30%.
2. according to the said insulated panel core material of claim 1, the thickness that it is characterized in that said core is 0 5-30mm.
3. according to the said insulated panel core material of claim 2, the thickness that it is characterized in that said core is 0 5-8mm.
4. insulated panel core material making method, this method may further comprise the steps:
(1) cut-off directly is 3.5-5um, and glass fibre cotton and diameter that length is produced for the 5-20mm centrifuge method are 1.5-2.5um, and length is the glass fibre cotton that 1-5mm flame method is produced; The glass fibre cotton that said flame method is produced accounts for 70wt%, and the glass fibre cotton that said centrifuge method is produced accounts for 30wt%;
(2) two kinds of glass fibre cottons are added water agitation and dilution concentration to 0.3-0.6%;
(3) the glass fibre cotton slurries sent into held stock tank:
The slurry that (4) will hold in the stock tank is sent into breast box, adopts forming net that glass fibre cotton core blank is processed in glass fibre cotton dehydration moulding then;
(5) adopt pressure roller to glass fibre cotton core blank carry out vertically, lateral surfaces is smooth, simultaneously the bad thickness of glass fibre cotton core hair adjusted, and makes core blank thickness unanimity;
(6) the glass fibre cotton core blank after the shaping is carried out vacuum dehydration, removes the moisture of 60%-70%:
(7), form the whole plate of glass fibre cotton core with the oven dry of core blank:
(8) the whole plate of glass fibre cotton core is cooled to normal temperature;
(9) the whole plate of glass fibre cotton core is cut into the glass fibre cotton core.
5. according to the said insulated panel core material making method of claim 4, the temperature that it is characterized in that said baking step is 250-400 ℃, and drying time is 3-15 minute.
6. according to the said insulated panel core material making method of claim 4, it is characterized in that said glass fibre cotton core blank thickness is 0.5-30mm.
7. according to the said insulated panel core material making method of claim 4, when it is characterized in that said forming net dewaters to glass fibre cotton, the speed of forming net is 2-5 meters/minutes.
8. according to the said insulated panel core material making method of claim 4, it is characterized in that diluted concentration to 0.4% in the said step (2).
9. according to the said insulated panel core material making method of claim 4, it is characterized in that adopting in the said step (5) the twice pressure roller that glass wool core blank is carried out surfacing.
10. according to the said insulated panel core material making method of claim 6, it is characterized in that said glass fibre cotton core blank thickness is 0.5-8mm.
CN201210187543XA 2012-06-08 2012-06-08 Vacuum insulation board core material and manufacture method of vacuum insulation board core material Pending CN102720920A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201210187543XA CN102720920A (en) 2012-06-08 2012-06-08 Vacuum insulation board core material and manufacture method of vacuum insulation board core material

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Application Number Priority Date Filing Date Title
CN201210187543XA CN102720920A (en) 2012-06-08 2012-06-08 Vacuum insulation board core material and manufacture method of vacuum insulation board core material

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Publication Number Publication Date
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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104141859A (en) * 2013-05-10 2014-11-12 常州山由帝武节能新材料制造有限公司 Core material for vacuum heat-insulating plate and vacuum heat-insulating plate
CN104648733A (en) * 2015-02-04 2015-05-27 滁州银兴电气有限公司 Raw material paving machine for silicon dioxide vacuum insulation panel
CN105757400A (en) * 2013-05-10 2016-07-13 糜玥崎 Core material for vacuum insulation plate and vacuum insulation plate form by same
CN107953496A (en) * 2017-12-08 2018-04-24 刘军 A kind of core material of vacuum heat insulation plate and its preparation process

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010116719A1 (en) * 2009-04-07 2010-10-14 シャープ株式会社 Vacuum insulation material and appliance provided therewith
CN101910702A (en) * 2007-12-28 2010-12-08 夏普株式会社 Core material for vacuum insulation material, vacuum insulation material, and processes for producing these
CN102330871A (en) * 2011-07-13 2012-01-25 苏州维艾普新材料有限公司 Vacuum heat insulation plate core material and manufacturing method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101910702A (en) * 2007-12-28 2010-12-08 夏普株式会社 Core material for vacuum insulation material, vacuum insulation material, and processes for producing these
WO2010116719A1 (en) * 2009-04-07 2010-10-14 シャープ株式会社 Vacuum insulation material and appliance provided therewith
CN102330871A (en) * 2011-07-13 2012-01-25 苏州维艾普新材料有限公司 Vacuum heat insulation plate core material and manufacturing method thereof

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104141859A (en) * 2013-05-10 2014-11-12 常州山由帝武节能新材料制造有限公司 Core material for vacuum heat-insulating plate and vacuum heat-insulating plate
CN104141859B (en) * 2013-05-10 2016-05-11 江苏山由帝奥节能新材股份有限公司 A kind of core material of vacuum heat insulation plate and vacuum heat-insulating plate
CN105757400A (en) * 2013-05-10 2016-07-13 糜玥崎 Core material for vacuum insulation plate and vacuum insulation plate form by same
CN104648733A (en) * 2015-02-04 2015-05-27 滁州银兴电气有限公司 Raw material paving machine for silicon dioxide vacuum insulation panel
CN104648733B (en) * 2015-02-04 2016-10-05 滁州银兴新材料科技有限公司 Silicon dioxide vacuum heat-insulating plate raw material paving machine
CN107953496A (en) * 2017-12-08 2018-04-24 刘军 A kind of core material of vacuum heat insulation plate and its preparation process

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Application publication date: 20121010