CN102707076B - Integrated-three-chamber online analysis system - Google Patents
Integrated-three-chamber online analysis system Download PDFInfo
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- CN102707076B CN102707076B CN201210098166.2A CN201210098166A CN102707076B CN 102707076 B CN102707076 B CN 102707076B CN 201210098166 A CN201210098166 A CN 201210098166A CN 102707076 B CN102707076 B CN 102707076B
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Abstract
The invention relates to an integrated-three-chamber online analysis system, which comprises a cooling chamber, a heating chamber and an air chamber which are adjacent to each other. An air chamber access door for accessing from outside is arranged at one side of the air chamber; a cooling chamber access door leading to the cooling chamber and a heating chamber access door leading to the heating chamber are respectively arranged at the other side of the air chamber; a sample recovery system is arranged outside the cooling chamber; an alarm control system is arranged in the air chamber; the sample recovery system is electrically connected with the alarm control system in the air chamber; the cooling room is provided with an oxygen detection device, a combustible detection device and a fire detection device which are respectively electrically connected with the alarm control system in the air chamber, and a plurality of online analysis meters connected with the sample recovery system; an oxygen detection device, a combustible detection device and a fire detection device which are respectively electrically connected with the alarm control system in the air chamber, and a sample processing system are arranged in the heating chamber; and the sample processing system is respectively connected with meter wind, oxygen and a sample interface from a production line. According to the integrated-three-chamber online analysis system, the problem of difficult transportation and installation caused by overlarge system volume is solved.
Description
Technical field
The present invention relates to the analytic system in a kind of chemical process.Particularly relate to a kind of volume little, be convenient to the three integrated on-line analysis systems in Room mobile and transportation.
Background technology
Original Tianjin EO/EG device on-line analysis system adopts DOW Chemical technique, metered quantity is various, system is controlled complicated, sample processing system and the support equipment requirement difference to environment, some part instrumentations having relatively high expectations to environment, therefore to whole system, be monolithic design, analysis meter, sample processing system, warning system all are integrated in a cabin requirement of the environment that the equipment needs that can not meet in system are identical.
Summary of the invention
Technical matters to be solved by this invention is, provide a kind of and can meet respectively in system distinct device for the different requirements of environment, guarantee that equipment is operated in the adapt circumstance condition, guarantee the stability of analysis meter operation and the three integrated on-line analysis systems in Room of reliability.
The technical solution adopted in the present invention is: a kind of three integrated on-line analysis systems in Room, comprise: the cold house of adjacent setting, hot cell and air chamber, one side of described air chamber is provided with the air chamber access door for entering from outside, the opposite side of described air chamber is respectively arranged with the cold house's access door that leads to cold house and the hot cell access door that leads to hot cell, the arranged outside of described cold house has sample retrieval system, wherein, be provided with alarm control system in described air chamber, described sample retrieval system is electrically connected to the alarm control system in air chamber, be provided with respectively the oxygen detection device be electrically connected to alarm control system in air chamber in described cold house, flammable pick-up unit and fire detection device, and be provided with a plurality of on-line analysis instrument that are connected with described sample retrieval system, be provided with respectively the oxygen detection device be electrically connected to alarm control system in air chamber in described hot cell, flammable pick-up unit and fire detection device, and be provided with sample processing system, described sample processing system connects respectively from the instrument wind on production line, the interface of oxygen and sample.
Described sample retrieval system includes the sample bypass discharge recycling can that the instrument discharge recycling can that is connected with a plurality of on-line analysis instrument in cold house is connected with sample pretreatment system with in hot cell, described instrument discharge recycling can pressure fluctuating in inner scope is at 100KPa (a)～105KPa (a), and described sample bypass discharge recycling can internal pressure remains on 149KPa (a)～154KPa (a).
The physical dimension in described cold house and hot cell is identical to be: 18000 (L) mm * 2500 (W) mm * 3000 (H) mm, the physical dimension of institute's air chamber is 1500 (L) mm * 4500 (W) mm * 3000 (H) mm.
Described air chamber inside is provided with controlling alarm case and the warning lamp siren for settling alarm control system, be provided with the system status monitoring that is connected with the controlling alarm case/reset operation case on the lateral wall of described air chamber, and the warning lamp siren be connected with described alarm control system.
A plurality of on-line analysis instrument that arrange in described cold house include: chromatograph, oxygen analyzer, the TOC analyser, infrared spectrum analyser, near-infrared analyzer, uv analyzer, also be respectively arranged with in described cold house to a plurality of on-line analysis instrument the power distribution cabinet of power supply, the combustible gas detector be connected with the controlling alarm case and smog probe are provided, also be provided with in described cold house in the described cold house of conventional sense case for settling oxygen detection device, temperature-detecting device and pressure-detecting device and also be provided with cold house and escape the row door.
The arranged outside of described cold house has the cold house's heating ventilation and air conditioning system be connected with cold house outside metope, and for hydrogen gas cylinder and the nitrogen cylinder of chromatograph.
The sample inlet entrance that the sample processing system arranged in described hot cell includes Standard Gases setting unit, the first sample pretreatment system, the second sample pretreatment system and is connected with instrument wind, oxygen and sample from production line for the first sample pretreatment system and the second sample pretreatment system, the sample flow outlet of described the first sample pretreatment system and the second sample pretreatment system is connected respectively a plurality of on-line analysis instrument in cold house.
In described hot cell, also be provided with for settling the conventional sense case of oxygen detection device, flammable pick-up unit and fire detection device, provide the power distribution cabinet of power supply for the indoor all devices of thermotropism, the indoor warning lamp siren be connected with the controlling alarm case, smog probe and combustible gas detector.
Described hot cell is respectively arranged with the first hot cell emergency exits and the second hot cell emergency exits, the side that is positioned at the first hot cell emergency exits in the outside in hot cell is provided with the first warning lamp siren be connected with the controlling alarm case, the side that is positioned at the second hot cell emergency exits is provided with the second warning lamp siren be connected with the controlling alarm case, and the outside in described hot cell also is provided with the high-power heating ventilation and air conditioning system in hot cell be connected with the outside, hot cell metope.
Described cold house, hot cell and air chamber are detachable is three independently structures.
The three integrated on-line analysis systems in Room of the present invention, three analyzer house cold house, hot cell, the air chambers different by function form, and can provide different environmental baselines for on-line analysis instrument, sample pretreatment equipment, warning system respectively; Can meet respectively distinct device in system and, for the different requirements of environment, guarantee that equipment is operated in the adapt circumstance condition, and be independent of each other, guarantee stability and the reliability of analysis meter operation.Three Room integrated designs have solved the too huge and problem that is difficult to transportation and installs of system bulk.Because the adapt circumstance condition has guaranteed the stability of equipment work, finally guarantee the stability of a whole set of analytic system work and the reliability of obtained analysis data.The three integrated on-line analysis systems in Room of the present invention, can be divided into three parts and load respectively transportation, solved the problem that is difficult to transportation due to bulky.System can complete splicing after reaching the spot, and by three sub-system in combination, becomes a large total system, completes integrative installation technology.
The accompanying drawing explanation
Fig. 1 is one-piece construction diagram of the present invention;
Fig. 2 is air chamber structure schematic diagram of the present invention;
Fig. 3 is cold room structure schematic diagram of the present invention;
Fig. 4 is hot cell of the present invention structural representation.
In figure:
Embodiment
Below in conjunction with embodiment and accompanying drawing, the three integrated on-line analysis systems in Room of the present invention are described in detail.
As shown in Figure 1, the three integrated on-line analysis systems in Room of the present invention, comprise: the cold house 1 of adjacent setting, hot cell 2 and air chamber 3, a whole set of analytic system physical dimension is: 19500 (L) mm * 4500 (W) mm * 3000 (H) mm, each chamber is divided into three relatively independent parts.Wherein, cold house is of a size of 18000 (L) mm * 2500 (W) mm * 3000 (H) mm and is mainly used in various instrument, the installment and debugging of public work.Hot cell is of a size of 18000 (L) mm * 2500 (W) mm * 3000 (H) mm and is mainly used in installing various sample processing devices, and instrument wind, nitrogen are provided, chilled water, the interfaces such as discharge, after the sample preparation in hot cell, the instrument that enters cold house through threading.Air cell size is 1500 (L) mm * 4500 (W) mm * 3000 (H) mm.
Described cold house 1, hot cell 2 and air chamber 3 be removable is divided into three independently structures.One side of described air chamber 3 is provided with the air chamber access door 31 for entering from outside, the opposite side of described air chamber 3 is respectively arranged with the cold house's access door 33 that leads to cold house 1 and the hot cell access door 32 that leads to hot cell 2, the arranged outside of described cold house 1 has sample retrieval system 4, wherein, be provided with alarm control system in described air chamber 3, the alarm control system that described sample retrieval system 4 is electrically connected in air chamber 3, be provided with the oxygen detection device that interior with air chamber 3 respectively alarm control system is electrically connected in described cold house 1, flammable pick-up unit and fire detection device, and be provided with a plurality of different on-line analysis instrument be connected from described sample retrieval system 4, be provided with the oxygen detection device that interior with air chamber 3 respectively alarm control system is electrically connected in described hot cell 2, flammable pick-up unit and fire detection device, and be provided with sample processing system, described sample processing system connects respectively from the instrument wind on production line, the interface of oxygen and sample.
Described sample retrieval system 4 includes the sample bypass discharge recycling can that the instrument discharge recycling can connected from a plurality of different on-line analysis instrument in cold house 1 is connected with the sample pretreatment system indoor with 2, described instrument discharge recycling can guarantees that the pressure fluctuating in inner scope is at 100KPa (a)～105KPa (a), and described sample bypass discharge recycling can internal pressure remains on 149KPa (a)～154KPa (a).
As shown in Figure 2, described air chamber 3 inside are provided with controlling alarm case 34 and the warning lamp siren 37 for settling alarm control system, be provided with the system status monitoring that is connected with controlling alarm case 34/reset operation case 35 on the lateral wall of described air chamber 3, and the warning lamp siren 36 be connected with described alarm control system.
As shown in Figure 3, a plurality of different on-line analysis instrument of described cold house 1 interior setting includes: 14 10 of chromatographs, 12 6 of oxygen analyzers, 16 3 of TOC analysers, 15 1 of infrared spectrum analysers, 17 1 of near-infrared analyzers, 18 1 of uv analyzers, also be respectively arranged with the power distribution cabinet 12 that power supply is provided to a plurality of different on-line analysis instrument in described cold house 1, the combustible gas detector 13 be connected with controlling alarm case 34 (in Fig. 2) and smog probe 11, in described cold house 1, also be provided with for settling the oxygen detection device, the conventional sense case 110 of temperature-detecting device and pressure-detecting device, also be provided with cold house in described cold house 1 and escape row door 116.
The arranged outside of described cold house 1 has the cold house's heating ventilation and air conditioning system 19 be connected with cold house outside metope, and for hydrogen gas cylinder and the nitrogen cylinder 114 of chromatograph 14.
As shown in Figure 4, the sample inlet entrance 21 that the sample processing system of described hot cell 2 interior settings includes Standard Gases setting unit 24, the first sample pretreatment system 213, the second sample pretreatment system 214 and is connected with instrument wind, oxygen and sample from production line for the first sample pretreatment system 213 and the second sample pretreatment system 214, the sample flow outlet of described the first sample pretreatment system 213 and the second sample pretreatment system 214 is connected respectively a plurality of on-line analysis instrument in cold house 1.
In described hot cell 2, also be provided with for settling the conventional sense case 27 of oxygen detection device, temperature-detecting device and pressure-detecting device, for to hot cell, all devices in 2 provide the power distribution cabinet 28 of power supply, the indoor warning lamp siren 211 be connected with controlling alarm case 34 (in Fig. 2), smog to pop one's head in 210 and combustible gas detector 29.
Described hot cell 2 is respectively arranged with the first hot cell emergency exits 22 and the second hot cell emergency exits 26, the side that 2 the outside is arranged in the first hot cell emergency exits 22 in hot cell is provided with the first warning lamp siren 23 be connected with system alarm control box 34 (Fig. 2), the side that is arranged in the second hot cell emergency exits 26 is provided with the second warning lamp siren 215 be connected with system alarm control box 34 (Fig. 2), and the outside in described hot cell 2 also is provided with the high-power heating ventilation and air conditioning system in hot cell (HVAC) 25 be connected with the outside, hot cell metope.
The three integrated on-line analysis systems in Room of the present invention, concentrate the sample pretreatment system that requires hot environment to be equipped in hot cell; The on-line analysis instrument that requires low temperature environment is concentrated and is equipped in cold house; Warning system that will be higher to requirement of explosion proof is equipped in small volume, possesses the air chamber that malleation purges.Three kinds of respectively corresponding three kinds of operating mode demands of far different working environment, met the environmental requirement of the every part of whole system, guaranteed stability and the reliability of a whole set of analytic system.
The temperature-controlled precision that is separately positioned on the HVAC in cold house and hot cell reached ± and 3 ℃.HVAC of the present invention is for general analysis system configuration explosion-proof, more powerful, temperature adjusting is wider, temperature control precision is higher.This has also promoted the quality of the three integrated on-line analysis systems in Room of the present invention greatly.
Claims (2)
1. the integrated on-line analysis system in Room, it is characterized in that, comprise: the cold house of adjacent setting (1), hot cell (2) and air chamber (3), one side of described air chamber (3) is provided with the air chamber access door (31) for entering from outside, the opposite side of described air chamber (3) is respectively arranged with the cold house's access door (33) that leads to cold house (1) and the hot cell access door (32) that leads to hot cell (2), the arranged outside of described cold house (1) has sample retrieval system (4), wherein, described air chamber is provided with alarm control system in (3), described sample retrieval system (4) is electrically connected to the alarm control system in air chamber (3), be provided with the oxygen detection device that interior with air chamber (3) respectively alarm control system is electrically connected in described cold house (1), flammable pick-up unit and fire detection device, and be provided with a plurality of on-line analysis instrument that are connected with described sample retrieval system (4), be provided with the oxygen detection device that interior with air chamber (3) respectively alarm control system is electrically connected in described hot cell (2), flammable pick-up unit and fire detection device, and be provided with sample processing system, described sample processing system connects respectively from the instrument wind on production line, the interface of oxygen and sample.
2. three integrated on-line analysis systems in Room according to claim 1, it is characterized in that, described sample retrieval system (4) includes the sample bypass discharge recycling can that the instrument discharge recycling can that is connected with a plurality of on-line analysis instrument in cold house (1) is connected with sample pretreatment system in sample processing system with in hot cell, described instrument discharge recycling can pressure fluctuating in inner scope is at 100KPa (a)～105KPa (a), and described sample bypass discharge recycling can internal pressure remains on 149KPa (a)～154KPa (a).
3. three integrated on-line analysis systems in Room according to claim 1, it is characterized in that, identical length * wide * the height that is of the physical dimension of described cold house (1) and hot cell (2): 18000 (L) mm * 2500 (W) mm * 3000 (H) mm, the physical dimension of institute's air chamber (3) is length * wide * height: 1500 (L) mm * 4500 (W) mm * 3000 (H) mm.
4. three integrated on-line analysis systems in Room according to claim 1, it is characterized in that, the arranged outside of described cold house (1) has the cold house's heating ventilation and air conditioning system (19) be connected with cold house outside metope, and for hydrogen gas cylinder and the nitrogen cylinder (114) of chromatograph (14).
5. three integrated on-line analysis systems in Room according to claim 1, it is characterized in that, the sample processing system arranged in described hot cell (2) includes Standard Gases setting unit (24), the first sample pretreatment system (213), the second sample pretreatment system (214) and for the first sample pretreatment system (213) and the second sample pretreatment system (214) with from the instrument wind on production line, the sample inlet entrance (21) that oxygen is connected with sample, the sample flow outlet of described the first sample pretreatment system (213) and the second sample pretreatment system (214) is connected respectively a plurality of on-line analysis instrument in cold house (1).
6. three integrated on-line analysis systems in Room according to claim 1, it is characterized in that, described hot cell (2) is respectively arranged with the first hot cell emergency exits (22) and the second hot cell emergency exits (26), the side that the outside of (2) is positioned at the first hot cell emergency exits (22) in hot cell is provided with the first warning lamp siren (23) be connected with controlling alarm case (34), the side that is positioned at the second hot cell emergency exits (26) is provided with the second warning lamp siren (215) be connected with controlling alarm case (34), the outside in described hot cell (2) also is provided with the high-power heating ventilation and air conditioning system in hot cell (25) be connected with the outside, hot cell metope, described controlling alarm case (34) is for settling described alarm control system.
7. the three integrated on-line analysis systems in Room according to claim 1, is characterized in that, described cold house (1), hot cell (2) and air chamber (3) be removable is divided into three independently structures.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201210098166.2A CN102707076B (en) | 2012-04-05 | 2012-04-05 | Integrated-three-chamber online analysis system |
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| CN201210098166.2A CN102707076B (en) | 2012-04-05 | 2012-04-05 | Integrated-three-chamber online analysis system |
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| CN102707076A CN102707076A (en) | 2012-10-03 |
| CN102707076B true CN102707076B (en) | 2014-01-01 |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4711571A (en) * | 1986-01-15 | 1987-12-08 | Mark Schuman | Radiant emission and absorption multigas analyzer |
| CN1869706A (en) * | 2006-06-08 | 2006-11-29 | 聚光科技（杭州）有限公司 | Method for continuous monitoring smoke discharge and its device |
| CN2854600Y (en) * | 2005-12-31 | 2007-01-03 | 索纪文 | Smoke on-line analyzer |
| CN201344934Y (en) * | 2009-01-13 | 2009-11-11 | 浙江理工大学 | Water quality comprehensive biological toxicity on-line automatic analyzer |
| CN202599961U (en) * | 2012-04-05 | 2012-12-12 | 中国石油化工股份有限公司 | Three-chamber integrated on-line analysis system |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| EP2460002A4 (en) * | 2009-07-31 | 2013-11-27 | Waters Technologies Corp | Method and apparatus for performing mass spectrometry |
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4711571A (en) * | 1986-01-15 | 1987-12-08 | Mark Schuman | Radiant emission and absorption multigas analyzer |
| CN2854600Y (en) * | 2005-12-31 | 2007-01-03 | 索纪文 | Smoke on-line analyzer |
| CN1869706A (en) * | 2006-06-08 | 2006-11-29 | 聚光科技（杭州）有限公司 | Method for continuous monitoring smoke discharge and its device |
| CN201344934Y (en) * | 2009-01-13 | 2009-11-11 | 浙江理工大学 | Water quality comprehensive biological toxicity on-line automatic analyzer |
| CN202599961U (en) * | 2012-04-05 | 2012-12-12 | 中国石油化工股份有限公司 | Three-chamber integrated on-line analysis system |
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