CN102648768B - Coproduction method of pig bone soup stock, pig bone oil and pig bone extract - Google Patents
Coproduction method of pig bone soup stock, pig bone oil and pig bone extract Download PDFInfo
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Abstract
The invention discloses a coproduction method of pig bone soup stock, pig bone oil and pig bone extract. The method comprises the following steps: crushing pig bones, performing hot-pressing extraction, vibrating to remove slag, standing and separating to obtain the pig bone extract; concentrating the pig bone extract until the solid matter content is 40 percent, adding edible salt in an amount which is 12.8 percent of the mass of the concentrate, and performing high-pressure homogenous emulsion to obtain the finished product pig bone soup stock; performing oil water continuous separation on the pig bone extract by using a tube type separator to obtain pig bone oil and pig bone extract stock solution; washing the pig bone oil with water and removing water to obtain the finished product pig bone oil; and concentrating the pig bone extract stock solution until the solid matter content is 45 percent, adding edible salt in an amount which is 13 percent of the mass of the concentrate and mixing uniformly to obtain the finished product pig bone extract. By the coproduction method, the raw materials have wide sources and the multi-product coproduction process is realized. The produced pig bone soup stock, pig bone oil and pig bone extract are delicious in taste, high in nutritional value and widely applied to food industry, catering industry and home kitchens, and has wide market prospect.
Description
Technical field
The present invention relates to a kind of method of swine bone high-soup, pig animal oil and the coproduction of pig ossein.
Background technology
China has a large amount of discarded pig bones to produce every year, and 2008-2011 China is average annual produces more than 700 ten thousand tons of pig bones, if so many pig bone does not effectively utilize, not only causes the serious waste of resource, and brings white elephant to environmental protection.In the pig bone, nutriment is abundant, and protein content is 12.1%, and fat content is 9.5%, contains the amino acid of needed by human body, the element of 8 kinds of needed by human such as Ca, Fe.In the pig bone, on year-on-year basis higher than cow's milk, pork, other amino acid content is on year-on-year basis higher than egg except isoleucine and methionine for essential amino acids content.But the low value-added products such as the present most processed skeletonization paste of pig bone, bone mud, resource utilization is low.The present invention realized the intensive processing of pig bone by the coproduction of swine bone high-soup, pig animal oil and pig ossein, improved the added value that the pig bone is butchered accessory substance.
Take the bright bones of clean pig (or freezing bone) as raw material, obtain pig bone extract through fragmentation, hot pressing extracting, vibration slagging-off, standing separation.Pig bone extract obtains nutritious through Vacuum Concentration, mediation, emulsifying homogeneous, the swine bone high-soup of delicious flavour.Pig bone extract obtains pig animal oil and pig ossein stoste through water-oil separating, the pig animal oil can dewater and obtain finished product pig animal oil by washing, heating, the pig animal oil can be used for margarine, seasoning wet goods purposes, and pig ossein stoste obtains the pig ossein product of high protein and low fat through Vacuum Concentration and the sterilization that is in harmonious proportion.In pig bone hot pressing extractive process, partially protein is decomposed, be degraded to low-molecular-weight peptide material and have bioactive 17 kinds of necessary free amino acids of human body and strengthened local flavor, contain simultaneously the indispensable Phospholipids of calcium, phosphorus and brain, phosphoprotein etc., these compositions have extremely strong instant capacity, be easy to human body and digest and assimilate, very high nutrition, function value are arranged.
Summary of the invention
A kind of method that the purpose of this invention is to provide swine bone high-soup, pig animal oil and the coproduction of pig ossein.
The method of bone soup-stock provided by the invention, animal oil and ossein coproduction comprises the steps:
1) bone is clean, fragmentation is carried out removing the gred after the hot pressing extracting in water afterwards, obtains the bone extract except the slag of boning after standing separation;
2) described step 1) gained bone extract is concentrated after after mediation, emulsifying and sterilization, obtain described bone soup-stock;
3) described step 1) gained bone extract is carried out water-oil separating, obtain animal oil by oil reservoir, obtain ossein stoste by water layer;
4) with standing after the washing of described step 3) gained animal oil, remove the can of lowering the temperature after being heated to 110 ℃ ~ 120 ℃ after water layer, obtain described animal oil;
5) described step 3) gained ossein stoste concentrated and be in harmonious proportion after, obtain described ossein.
In the described broken step of the described step 1) of said method, the length of broken rear bone is 1.5cm ± 0.5cm;
In described hot pressing extraction steps, the bone after fragmentation and the mass ratio of water are 1:1.5 ~ 1:3, preferred 1:2; Pressure 0.20MPa ± 0.02MPa, temperature is 130 ± 3 ℃, the time is 1 ~ 1.5h;
In described slagging-off step, the aperture of sieve aperture is 40 ~ 80 orders, preferred 40 orders;
In described standing separation step, the time is 1 ~ 3 hour, and preferred 2 hours, temperature was 85 ± 5 ℃;
Described step 2) in described concentration step, method for concentration is Vacuum Concentration;
In described Vacuum Concentration step, temperature is 50～65 ℃, pressure-0.050～-0.074MPa, the quality percentage composition of concentrated gained solid content is 30% ~ 45%, preferred 40%;
In described mediation step, blender is salt; The addition of described blender is 13 ± 2% of concentrated gained solid quality; Temperature is 82～90 ℃, and the time is 30～40min;
In described emulsifying step, pressure is 30 ± 2MPa, and the time is 10 ~ 15min, preferred 10min;
In described sterilisation step, method for disinfection is pasteurize; Sterilization temperature is 85 ± 3 ℃;
In the described water-oil separating step of described step 3), rotating speed is 13000 ~ 16000r/min, preferred 15000r/min;
In the described water-washing step of described step 4), the consumption of water is 8% ~ 12% of described animal oil quality, preferred 10%; The temperature of water is 75 ~ 85 ℃, preferred 80 ℃; Rotating speed is 10 ~ 15r/min; Time is 20 ~ 45 minutes, preferred 30 minutes;
In described standing step, the time is 15 ~ 30 minutes, preferred 20 minutes;
In described cooling can step, the time is not more than 3 hours;
In the described concentration step of described step 5), method for concentration is Vacuum Concentration;
In described Vacuum Concentration step, temperature is 50～65 ℃, pressure-0.050～-0.074MPa, the quality percentage composition of concentrated gained solid content is 30% ~ 45%, preferred 45%;
In described mediation step, blender is salt; The addition of described blender is 13 ± 2% of concentrated gained solid quality; Temperature is 82～90 ℃, and the time is 30～40min.
Concrete, described bone is that the bright bone of pig or pig are frozen bone.
In addition, at least a in bone soup-stock, animal oil and ossein that the method that provides according to the invention described above prepares and contain at least a product in described bone soup-stock, animal oil and ossein also belongs to protection scope of the present invention.
The co-production of swine bone high-soup provided by the invention, pig animal oil and pig ossein, be after cleaning the bright bones of pig (or freezing bone) through fragmentation, hot pressing extracting, vibration remove the gred, standing separation obtains pig bone extract, it is to add 12.8% edible salt by the concentrate quality after 40% to transfer that pig bone extract is concentrated into solid content, obtains the swine bone high-soup finished product after high-pressure homogeneous emulsification.With channel separator with pig bone extract carry out the profit continuous separate from, obtain pig animal oil and pig ossein stoste, the pig animal oil is through washing, obtain finished product pig animal oil after dewatering.It is 45% that pig ossein stoste is concentrated into solid content, presses the concentrate quality and adds 13% edible salt, is in harmonious proportion and evenly obtains pig ossein finished product.Raw material sources of the present invention are extensive, realized the multi-product coproduction on technique, the swine bone high-soup of producing, pig animal oil, pig ossein delicious flavour, and nutritive value is abundant, is widely used in food industry, catering trade and family kitchen, and market prospects are wide.
Description of drawings
Fig. 1 is the process chart of the co-production of swine bone high-soup, pig animal oil and pig ossein.
The specific embodiment
The present invention is further elaborated below in conjunction with specific embodiment, but the present invention is not limited to following examples.Described in following example, the preparation method if no special instructions, is conventional method.Described reagent and material all can obtain if no special instructions from commercial channels.
The method of bone soup-stock provided by the invention, animal oil and ossein coproduction specifically can comprise the steps:
1) the bright bone of pig (or freezing bone) is cleaned, being broken into length is 1.5cm ± 0.5cm fritter.The present invention is that after the bright bone of pig (freezing bone) is cleaned, input is pricked in the bone machine broken.
2) pig bone broken in step 1) is carried out the hot pressing extracting.The present invention packs broken pig bone in cage, and cage is put into the hot pressing extracting tank, and than 1:2, extracting pressure 0.20MPa ± 0.02MPa carries out the hot pressing extracting under 130 ± 3 ℃ of conditions of extraction temperature at bone water, and the hot pressing extracting time is controlled at 1 ~ 1.5h.
3) with step 2) middle hot pressing extract vibration slagging-off.The present invention is that to be extracted completing opened the hot pressing extracting tank after pressure release, takes out cage, collects hot pressing extracting tank in-seam soup and adopts vibratory sieve to remove the bulk slag, and mesh size is 40 orders.
4) with the bone soup standing separation after slagging-off in step 3), go bottom bone slag to obtain pig bone extract.The present invention allows the standing natural separation of bone soup in the standing separation cylinder, time of repose is 2h, and temperature is controlled at 85 ± 5 ℃.
5) pig bone extract Vacuum Concentration in step 4) is obtained the swine bone high-soup semi-finished product.The present invention concentrates pig bone extract suction concentration systems, and temperature is controlled at 50～65 ℃, and pressure is controlled at-0.050～-0.074MPa, be concentrated into when solid content is 40% and stop concentrating.
6) swine bone high-soup semi-finished product in step 5) are in harmonious proportion.The swine bone high-soup semi-finished product that the present invention will concentrate are evacuated in the mediation groove, press the concentrate quality and add 13 ± 2% salt, add after conscientious weighing, stir in groove and make that in groove, temperature is controlled at 82～90 ℃ being in harmonious proportion, the constant temperature time harmonic is controlled between 30～40min, makes it to be in harmonious proportion evenly.
7) emulsifying of swine bone high-soup semi-finished product, the pasteurize that in step 6), mediation is good obtained the swine bone high-soup finished product.It is that 85 ± 3 ℃ of pasteurizes obtain the swine bone high-soup finished product by temperature that the present invention uses homogenizer homogeneous under 30 ± 2MPa condition.
8) with the pig bone extract water-oil separating in step 4), obtain pig animal oil and pig ossein stoste.The present invention with channel separator carry out the profit continuous separate from, rotating speed is 15000r/min, collects pig animal oil and the pig bone made soup (pig ossein stoste) that deoils at oil-out and delivery port respectively.
9) with pig animal oil washing in step 8).It is the water of 80 ℃ that the present invention adds 10% temperature in the pig animal oil, and revolution is slowly to stir standing 20min after 30min under 10 ~ 15r/min condition, standing complete by the slow draining in the lower mouth of a river until stop draining when having oil to get rid of.
10) residual moisture is removed in the pig animal oil heating after the step 9) washing, after cooling, can obtains finished product pig animal oil.After in the present invention, the pig animal oil being heated to 120 ℃, the can of lowering the temperature rapidly, this process is strict controlled in 3h.
11) with the pig bone made soup Vacuum Concentration that deoils in step 8).The present invention concentrates the pig bone made soup suction concentration systems that deoils, and when concentrated, jacket steam pressure is controlled at below 0.10Mpa, guarantees concentrated stationarity; Temperature is controlled at 50～65 ℃, and pressure is controlled at-0.050～-0.074MPa, be concentrated into when solid content is 45% and stop concentrating.
12) concentrate mediation sterilization in step 11) is prepared into the pig ossein.The semi-finished product that the present invention will concentrate are evacuated in the mediation groove, press the concentrate quality and add 13 ± 2% edible salts, stir in groove and make that in groove, temperature is controlled at 82～90 ℃ being in harmonious proportion, the constant temperature time harmonic is controlled between 30～40min, makes it to be in harmonious proportion evenly to obtain pig ossein finished product.
The method of embodiment 1, coproduction swine bone high-soup, pig animal oil and pig ossein
Technological process is as shown in Figure 1:
1) the bright bones of pig (or freezing bone) are cleaned after, drop into to prick in the bone machine and be broken into the fritter that length is 1.5cm ± 0.5cm;
The pig bone of the fragmentation cage of packing into, cage is put into the hot pressing extracting tank again, than 1:2, extracting pressure 0.20MPa carries out the hot pressing extracting under 130 ℃ of conditions of extraction temperature at bone water, and the hot pressing extracting time is 80min;
To be extracted completing opened the hot pressing extracting tank after pressure release, takes out cage, collects hot pressing extracting tank in-seam soup and adopts vibratory sieve to remove bulk bone slag, and mesh size is 40 orders;
Again in the pig bone made soup suction standing separation cylinder of vibration slagging-off, allow the standing natural separation of bone soup, time of repose is 2h, temperature is controlled at 90 ℃, removes bottom bone slag and obtains pig bone extract.
2) step 1) gained pig bone extract suction concentration systems is concentrated, when concentrated, jacket steam pressure is controlled at below 0.10Mpa, guarantees concentrated stationarity; Temperature is controlled at 60 ℃, and pressure is-0.06MPa, is concentrated into when solid content is 40% to stop concentrating;
The swine bone high-soup semi-finished product that will concentrate again are evacuated in the mediation groove, press the concentrate quality and add 12.8% edible salt, add after conscientious weighing, stir in groove and make that in groove, temperature is controlled at 85 ℃ being in harmonious proportion, the constant temperature time harmonic is controlled at 30min, makes it to be in harmonious proportion evenly;
Re-use homogenizer in emulsifying under the 31MPa condition after 15 minutes, 87 ℃ of sterilizations obtain the swine bone high-soup finished product.
The pig ossein soup-stock that said method obtains, delicate mouthfeel, meat aromatic flavour, the nutritious natural soup stock that can be used as in food.
3) with step 1) gained pig bone extract with channel separator carry out the profit continuous separate from, rotating speed is 15000r/min, collects pig animal oil and the pig bone made soup (pig ossein stoste) that deoils at oil-out and delivery port respectively;
4) adding the temperature of pig animal oil quality 10% in the step 3) gained pig animal oil is the water of 80 ℃ again, revolution be slowly stir under the 15r/min condition wash after 30min after standing 20min again, standing complete by the slow draining in the lower mouth of a river until stop draining when having oil to get rid of;
Again the pig animal oil after the gained washing is heated to 120 ℃ and removes residual moisture, after cooling, can obtains finished product pig animal oil rapidly, and this process is strict controlled in 3h.
The pig animal oil that said method obtains, recovery rate are 5%-6%, and the pig animal oil meat aromatic flavour of extraction can be used for margarine and seasoning wet goods purposes.
5) step 3) gained pig ossein stoste suction concentration systems is carried out Vacuum Concentration, when concentrated, jacket steam pressure is controlled at below 0.10Mpa, and temperature is controlled at 65 ℃, and pressure is controlled at-0.06MPa, is concentrated into when solid content is 45% to stop concentrating;
Concentrated good pig ossein semi-finished product are evacuated in the mediation groove, press the concentrate quality and add 13% edible salt, add after conscientious weighing, stir in groove and make that in groove, temperature is controlled at 90 ℃ being in harmonious proportion, the constant temperature time harmonic is controlled at 30min, makes it to be in harmonious proportion evenly to obtain pig ossein finished product.
The pig ossein outward appearance that said method obtains is the brown paste, pig ossein extract content is 35%, protein content is 25%, fat content is 0.41%, the amino acid A wide selection of colours and designs has good organoleptic quality and meat flavor, is typical high nutrition low fat flavouring, adopt automatic amino acid analyzer to measure amino acid contamination is wherein measured, acquired results is as shown in table 1.
Table 1, pig ossein amino acid contamination
As shown in Table 1, this embodiment prepares that in gained pig ossein, amino acid whose total content is 205.4268mg/g, kind is substantially complete, be flavor amino acid and account for 63.62% of total amino acid, wherein be delicate flavour amino acid (L-aminobutanedioic acid, glutamic acid) and account for 22.60%, be sweet taste amino acid (serine, glycine, alanine, proline) and account for 41.02%.
Claims (3)
1. the method for a bone soup-stock, animal oil and ossein coproduction, comprise the steps:
1) bone is clean, fragmentation is carried out removing the gred after the hot pressing extracting in water afterwards, obtains the bone extract except the slag of boning after standing separation;
2) described step 1) gained bone extract is concentrated after after mediation, emulsifying and sterilization, obtain described bone soup-stock;
3) described step 1) gained bone extract is carried out water-oil separating, obtain animal oil by oil reservoir, obtain ossein stoste by water layer;
4) with standing after the washing of described step 3) gained animal oil, remove the can of lowering the temperature after being heated to 110 ℃～120 ℃ after water layer, obtain described animal oil;
5) described step 3) gained ossein stoste concentrated and be in harmonious proportion after, obtain described ossein;
In the described broken step of described step 1), the length of broken rear bone is 1.5cm ± 0.5cm;
In described hot pressing extraction steps, the bone after fragmentation and the mass ratio of water are 1:1.5～1:3; Pressure 0.20MPa ± 0.02MPa, temperature is 130 ± 3 ℃, the time is 1～1.5h;
In described slagging-off step, the aperture of sieve aperture is 40～80 orders;
In described standing separation step, the time is 1.5～3 hours, and temperature is 85 ± 5 ℃;
Described step 2) in described concentration step, method for concentration is Vacuum Concentration;
In described Vacuum Concentration step, temperature is 50～65 ℃, pressure-0.050～-0.074MPa, the quality percentage composition of concentrated gained solid content is 30%～45%;
In described mediation step, blender is salt; The addition of described blender is 13 ± 2% of concentrated gained solid quality; Temperature is 82～90 ℃, and the time is 30～40min;
In described emulsifying step, pressure is 30 ± 2MPa, and the time is 10～15min;
In described sterilisation step, method for disinfection is pasteurize; Sterilization temperature is 85 ± 3 ℃;
In the described water-oil separating step of described step 3), rotating speed is 13000～16000r/min;
In the described water-washing step of described step 4), the consumption of water is 8%～12% of described animal oil quality; The temperature of water is 75～85 ℃; Rotating speed is 10～15r/min; Time is 20～45 minutes;
In described standing step, the time is 15～30 minutes;
In described cooling can step, the time is not more than 3 hours;
In the described concentration step of described step 5), method for concentration is Vacuum Concentration;
In described Vacuum Concentration step, temperature is 50～65 ℃, pressure-0.050～-0.074MPa, the quality percentage composition of concentrated gained solid content is 30%～45%;
In described mediation step, blender is salt; The addition of described blender is 13 ± 2% of concentrated gained solid quality; Temperature is 82～90 ℃, and the time is 30～40min.
2. method according to claim 1, it is characterized in that: in described step 1), in described hot pressing extraction steps, the bone after fragmentation and the mass ratio of water are 1:2;
In described slagging-off step, the aperture of sieve aperture is 40 orders;
In described standing separation step, the time is 2 hours;
Described step 2) in, in described Vacuum Concentration step, the quality percentage composition of concentrated gained solid content is 40%;
In the described water-oil separating step of described step 3), rotating speed is 15000r/min;
In described step 4), the consumption of water is 10% of described animal oil quality; The temperature of water is 80 ℃; Time is 30 minutes;
In described standing step, the time is 20 minutes;
In described step 5), in described Vacuum Concentration step, the quality percentage composition of concentrated gained solid content is 45%.
3. method according to claim 1 and 2 is characterized in that: described bone is that the bright bone of pig or pig are frozen bone.
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| CN102860488A (en) * | 2012-09-28 | 2013-01-09 | 湖南省汇湘轩生物科技有限公司 | Pork-flavored paste essence and preparation method thereof |
| CN102860487A (en) * | 2012-09-28 | 2013-01-09 | 湖南省汇湘轩生物科技有限公司 | Pork-flavor powdered essence and preparation method thereof |
| CN104336636B (en) * | 2013-08-07 | 2018-07-13 | 青岛博研达工业技术研究所(普通合伙) | A method of extracting nutriment from pig bone |
| CN105029346A (en) * | 2015-07-02 | 2015-11-11 | 中盐工程技术研究院有限公司 | Pig bone flavor seasoning salt and preparation method thereof |
| CN105124661A (en) * | 2015-07-29 | 2015-12-09 | 河南永达美基食品股份有限公司 | Method for preventing extracted soup oil emulsification |
| CN105249262B (en) * | 2015-11-12 | 2018-12-18 | 中国农业科学院农产品加工研究所 | The method of one breeder bone protein gel, soup-stock and bone calcium powder coproduction |
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| CN109527499A (en) * | 2018-10-09 | 2019-03-29 | 临沂新程金锣肉制品集团有限公司 | A kind of processing technology that ossein voluptuousness is remarkably reinforced |
| CN110506921A (en) * | 2019-09-27 | 2019-11-29 | 湖南省嘉品嘉味生物科技有限公司 | A kind of pig bone element flavor peptide and preparation method |
| CN110558521A (en) * | 2019-10-21 | 2019-12-13 | 漯河市青山高科技生物技术开发有限公司 | Pig bone white soup and production process thereof |
| CN111109573B (en) * | 2019-12-31 | 2022-10-21 | 临沂新程金锣肉制品集团有限公司 | Sectional type extraction production process for bone element |
| CN113854528A (en) * | 2021-08-20 | 2021-12-31 | 山东龙盛科达产业技术研究院有限公司 | Environment-friendly preparation method for recycling byproducts in ossein production |
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