CN102590076A - Measurement device of polymer viscoelastic model and measurement method of model element parameters - Google Patents

Measurement device of polymer viscoelastic model and measurement method of model element parameters Download PDF

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CN102590076A
CN102590076A CN2012100567408A CN201210056740A CN102590076A CN 102590076 A CN102590076 A CN 102590076A CN 2012100567408 A CN2012100567408 A CN 2012100567408A CN 201210056740 A CN201210056740 A CN 201210056740A CN 102590076 A CN102590076 A CN 102590076A
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谢刚
马浩翔
王百合
高明月
迟旭阳
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Heilongjiang University
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Abstract

聚合物粘弹性模型的测量装置及模型元件参数的测量方法,它涉及一种粘弹性模型的测量装置和模型元件参数的测量方法。针对经典的粘弹性力学模型是仅存在于纸面上的抽象模型,无法成为一个实际应用的力学模型等问题而建立。装置一:弹簧与黏壶串联;装置二:弹簧与黏壶并联;装置三:两个弹簧中的一个与两个黏壶中的一个串联组成麦克斯韦模型,另一个弹簧与另一个黏壶并联组成开尔芬模型,然后麦克斯韦模型再与开尔芬模型串联。方法:通过麦克斯韦模型的测量装置测出应力松弛曲线;通过开尔芬模型的测量装置测出蠕变曲线,对四元件力学模型的测量装置施加一个恒定的应力σ0,测出蠕变曲线。本发明可以用于构建实际的聚合物粘弹性力学模型。

Figure 201210056740

A measuring device for a polymer viscoelastic model and a measuring method for model element parameters relate to a measuring device for a viscoelastic model and a measuring method for model element parameters. The classic viscoelastic mechanical model is an abstract model that only exists on paper and cannot become a practical mechanical model. Device 1: the spring is connected in series with the sticky pot; device 2: the spring is connected in parallel with the sticky pot; device 3: one of the two springs is connected in series with one of the two sticky pots to form a Maxwell model, and the other spring is connected in parallel with the other sticky pot The Kelvin model, and then the Maxwell model in series with the Kelvin model. Method: The stress relaxation curve is measured by the measuring device of the Maxwell model; the creep curve is measured by the measuring device of the Kelvin model, and the creep curve is measured by applying a constant stress σ 0 to the measuring device of the four-element mechanical model. The invention can be used to construct the actual polymer viscoelasticity model.

Figure 201210056740

Description

聚合物粘弹性模型的测量装置及模型元件参数的测量方法Measuring device for polymer viscoelasticity model and method for measuring model element parameters

技术领域 technical field

本发明涉及一种粘弹性模型测量装置和模型元件参数的测量方法。The invention relates to a viscoelastic model measuring device and a method for measuring model element parameters.

背景技术 Background technique

经典的聚合物粘弹性力学模型只是一种抽象的概念,理论研究者只能在纸上用一些模型元件,即用抽象弹簧和抽象黏壶组成各种粘弹性力学模型来研究它的粘弹性力学行为。例如:把抽象弹簧和抽象黏壶串联起来组成麦克斯韦模型,把抽象弹簧和抽象黏壶并联起来组成开尔芬模型等,但是抽象弹簧的弹性模量和抽象黏壶的粘度没有具体数值,只在一些微分方程中表示其物理意义。The classic polymer viscoelasticity model is only an abstract concept, and theoretical researchers can only use some model elements on paper, that is, use abstract springs and abstract sticky pots to form various viscoelasticity models to study its viscoelasticity. Behavior. For example: connect the abstract spring and the abstract sticky pot in series to form the Maxwell model, connect the abstract spring and the abstract sticky pot in parallel to form the Kelvin model, etc. However, there are no specific values for the elastic modulus of the abstract spring and the viscosity of the abstract sticky pot. Its physical meaning is expressed in some differential equations.

发明内容 Contents of the invention

本发明为的目的是为解决目前针对经典的聚合物粘弹性力学模型仅存在于纸面上的抽象模型,无法成为一个具象的、可以实际应用的力学模型的问题,因此提出一种聚合物粘弹性模型的测量装置和模型元件参数的测量方法。The purpose of the present invention is to solve the problem that the classical polymer viscoelastic mechanical model only exists as an abstract model on paper and cannot become a concrete mechanical model that can be used in practice. Therefore, a polymer viscoelastic model is proposed. A measuring device for an elastic model and a method for measuring parameters of model elements.

本发明为解决上述技术问题采取的技术方案是:The technical scheme that the present invention takes for solving the problems of the technologies described above is:

本发明的聚合物粘弹性模型的测量装置有三个方案,分别如下:The measuring device of polymer viscoelasticity model of the present invention has three schemes, respectively as follows:

方案一:本发明的聚合物粘弹性模型的测量装置,所述聚合物粘弹性模型的测量装置为麦克斯韦模型的测量装置,所述麦克斯韦模型的测量装置包括底座、测力计、弹簧、黏壶、两个固定端板、四根拉杆及三个活动板;两个固定端板分别是第一固定端板和第二固定端板,三个活动板分别是第一活动板、第二活动板和第三活动板;Option one: the measuring device of the polymer viscoelastic model of the present invention, the measuring device of the polymer viscoelastic model is the measuring device of the Maxwell model, and the measuring device of the Maxwell model includes a base, a dynamometer, a spring, a sticky pot , two fixed end plates, four pull rods and three movable plates; the two fixed end plates are respectively the first fixed end plate and the second fixed end plate, and the three movable plates are respectively the first movable plate and the second movable plate and a third movable panel;

两个固定端板垂直且并列固定在底座上,两个固定端板之间水平且呈矩形阵列式固定有四根拉杆,由四根拉杆和两个固定端板组成框架式结构,三个活动板与两个固定端板平行设置并位于两个固定端板之间,第一活动板与第一固定端板相邻设置,第三活动板与第二固定端板相邻设置,第二活动板设置在第一活动板与第三活动板之间,每个活动板上与四根拉杆相对应位置设有四个通孔,每个活动板的四个通孔套装在四根拉杆上,三个活动板与四根拉杆滑动连接,第一活动板与第二活动板之间固连有弹簧,第二活动板与第三活动板之间固连有黏壶,测力计设置在第一活动板和第二活动板之间,测力计与第一活动板和第二活动板固接。The two fixed end plates are fixed vertically and side by side on the base. Four tie rods are fixed horizontally and in a rectangular array between the two fixed end plates. The frame structure is composed of four tie rods and two fixed end plates. Three movable The plate is set parallel to the two fixed end plates and is located between the two fixed end plates, the first movable plate is adjacent to the first fixed end plate, the third movable plate is adjacent to the second fixed end plate, and the second movable plate The plate is arranged between the first movable plate and the third movable plate, and each movable plate is provided with four through holes corresponding to the four pull rods, and the four through holes of each movable plate are set on the four pull rods, Three movable plates are slidingly connected with four pull rods, a spring is fixedly connected between the first movable plate and the second movable plate, and a sticky pot is fixedly connected between the second movable plate and the third movable plate, and the dynamometer is set at the Between the first movable plate and the second movable plate, the dynamometer is fixedly connected with the first movable plate and the second movable plate.

方案二:聚合物粘弹性模型的测量装置,所述聚合物粘弹性模型的测量装置为开尔芬模型的测量装置,所述开尔芬模型的测量装置包括底座、拉绳、托盘、砝码、定滑轮、应变仪、弹簧、黏壶、连杆、两个固定端板、四根拉杆及三个活动板;两个固定端板分别是第一固定端板和第二固定端板,三个活动板分别是第一活动板、第二活动板和第三活动板;Option two: the measuring device of the polymer viscoelastic model, the measuring device of the polymer viscoelastic model is the measuring device of the Kelvin model, and the measuring device of the Kelvin model includes a base, a drawstring, a tray, and a weight , fixed pulley, strain gauge, spring, sticky pot, connecting rod, two fixed end plates, four pull rods and three movable plates; the two fixed end plates are respectively the first fixed end plate and the second fixed end plate, and the three The first movable board is respectively the first movable board, the second movable board and the third movable board;

两个固定端板垂直且并列固定在底座上,两个固定端板之间水平且呈矩形阵列式固定有四根拉杆,由四根拉杆和两个固定端板组成框架式结构,三个活动板与两个固定端板平行设置并位于两个固定端板之间,第一活动板与第一固定端板相邻设置,第三活动板与第二固定端板相邻设置,第二活动板设置在第一活动板与第三活动板之间,每个活动板上与四根拉杆相对应位置设有四个通孔,每个活动板的四个通孔套装在四根拉杆上,三个活动板与四根拉杆滑动连接,托盘设置在第一固定端板的外部,定滑轮固定在第一固定端板的外侧面上,砝码装在托盘上,第一固定端板上设有拉绳穿过孔,拉绳的一端与托盘固接,拉绳的另一端绕过定滑轮并穿过所述第一固定端板的拉绳穿过孔与第一活动板固接,第二活动板与第三活动板之间并联设置有弹簧和黏壶,第一活动板与第二活动板之间固连有一个连杆,应变仪设置在第一活动板与第二活动板之间,且应变仪与第一活动板固接。The two fixed end plates are fixed vertically and side by side on the base. Four tie rods are fixed horizontally and in a rectangular array between the two fixed end plates. The frame structure is composed of four tie rods and two fixed end plates. Three movable The plate is set parallel to the two fixed end plates and is located between the two fixed end plates, the first movable plate is adjacent to the first fixed end plate, the third movable plate is adjacent to the second fixed end plate, and the second movable plate The plate is arranged between the first movable plate and the third movable plate, and each movable plate is provided with four through holes corresponding to the four pull rods, and the four through holes of each movable plate are set on the four pull rods, The three movable plates are slidingly connected with the four pull rods, the tray is arranged on the outside of the first fixed end plate, the fixed pulley is fixed on the outer surface of the first fixed end plate, the weight is mounted on the tray, and the first fixed end plate is set There is a stay cord passing through the hole, one end of the stay cord is fixedly connected to the tray, the other end of the stay cord goes around the fixed pulley and passes through the stay cord of the first fixed end plate through the hole and is fixedly connected to the first movable plate. A spring and a sticky pot are arranged in parallel between the second movable plate and the third movable plate, a connecting rod is fixedly connected between the first movable plate and the second movable plate, and the strain gauge is arranged between the first movable plate and the second movable plate between, and the strain gauge is fixedly connected to the first movable plate.

方案三:聚合物粘弹性模型的测量装置,所述聚合物粘弹性模型的测量装置为四元件模型的测量装置,所述四元件模型的测量装置包括底座、拉绳、托盘、砝码、定滑轮、测力计、应变仪、两个黏壶、两个弹簧、两个固定端板、四根拉杆及三个活动板;两个固定端板分别是第一固定端板和第二固定端板,三个活动板分别是第一活动板、第二活动板和第三活动板;Scheme three: the measuring device of the polymer viscoelastic model, the measuring device of the polymer viscoelastic model is the measuring device of the four-element model, and the measuring device of the four-element model includes a base, a pull cord, a tray, a weight, a fixed Pulley, dynamometer, strain gauge, two sticky pots, two springs, two fixed end plates, four pull rods and three movable plates; the two fixed end plates are the first fixed end plate and the second fixed end respectively board, the three movable boards are respectively the first movable board, the second movable board and the third movable board;

两个固定端板垂直且并列固定在底座上,两个固定端板之间水平且呈矩形阵列式固定有四根拉杆,由四根拉杆和两个固定端板组成框架式结构,三个活动板与两个固定端板平行设置并位于两个固定端板之间,第一活动板与第一固定端板相邻设置,第三活动板与第二固定端板相邻设置,第二活动板设置在第一活动板与第三活动板之间,每个活动板上与四根拉杆相对应位置设有四个通孔,每个活动板的四个通孔套装在四根拉杆上,三个活动板与四根拉杆滑动连接,托盘设置在第一固定端板的外部,定滑轮固定在第一固定端板的外侧面上,砝码装在托盘上,第一固定端板上设有拉绳穿过孔,拉绳的一端与托盘固接,拉绳的另一端绕过定滑轮并穿过所述第一固定端板的拉绳穿过孔与测力计固接,测力计与第一活动板固接,应变仪设置在第一活动板与第二活动板之间,且应变仪与第一活动板固接,两个弹簧中的一个弹簧固连在第一活动板与第二活动板之间,两个黏壶中的一个黏壶与两个弹簧中的剩余一个弹簧并联于第二活动板与第三活动板之间,两个黏壶中的剩余一个黏壶固连于第三活动板与第二固定端板之间。The two fixed end plates are fixed vertically and side by side on the base. Four tie rods are fixed horizontally and in a rectangular array between the two fixed end plates. The frame structure is composed of four tie rods and two fixed end plates. Three movable The plate is set parallel to the two fixed end plates and is located between the two fixed end plates, the first movable plate is adjacent to the first fixed end plate, the third movable plate is adjacent to the second fixed end plate, and the second movable plate The plate is arranged between the first movable plate and the third movable plate, and each movable plate is provided with four through holes corresponding to the four pull rods, and the four through holes of each movable plate are set on the four pull rods, The three movable plates are slidingly connected with the four pull rods, the tray is arranged on the outside of the first fixed end plate, the fixed pulley is fixed on the outer surface of the first fixed end plate, the weight is mounted on the tray, and the first fixed end plate is set There is a stay rope passing through the hole, one end of the stay rope is fixedly connected to the pallet, the other end of the stay rope goes around the fixed pulley and passes through the stay rope on the first fixed end plate and is fixedly connected to the dynamometer through the hole, and the force measurement The gauge is fixedly connected to the first movable plate, the strain gauge is arranged between the first movable plate and the second movable plate, and the strain gauge is fixedly connected to the first movable plate, and one of the two springs is fixedly connected to the first movable plate Between the second movable plate, one of the two sticky pots and the remaining one of the two springs are connected in parallel between the second movable plate and the third movable plate, and the remaining one of the two sticky pots It is fixedly connected between the third movable plate and the second fixed end plate.

本发明的利用聚合物粘弹性模型的测量装置实现模型元件参数的测量方法,所述测量方法由以下步骤完成:The measuring device utilizing polymer viscoelasticity model of the present invention realizes the measuring method of model element parameter, and described measuring method is finished by the following steps:

步骤一:让麦克斯韦模型的测量装置中的第一活动板和第三活动板同时产生恒定位移,使得麦克斯韦模型产生恒定形变ε0,并通过麦克斯韦模型的测量装置的测力计测出麦克斯韦模型在某时刻应力的大小,绘制应力与时间的关系曲线,即应力松弛曲线;Step 1: Let the first movable plate and the third movable plate in the measuring device of the Maxwell model produce constant displacement at the same time, so that the Maxwell model produces a constant deformation ε 0 , and measure the Maxwell model at The magnitude of the stress at a certain moment, draw the relationship curve between stress and time, that is, the stress relaxation curve;

往开尔芬模型的测量装置的托盘上添加砝码,相当于施加一个恒定的应力σ0,通过开尔芬模型的测量装置的应变仪测出开尔芬模型在某时刻应变的大小,绘制应变与时间的关系曲线,即蠕变曲线。Adding weights to the tray of the measuring device of the Kelvin model is equivalent to applying a constant stress σ 0 , and the strain gauge of the measuring device of the Kelvin model is used to measure the strain of the Kelvin model at a certain moment, and draw The relationship between strain and time, that is, the creep curve.

根据应力松弛公式:According to the stress relaxation formula:

σσ == σσ 00 ee -- EE. ηη ·· tt -- -- -- (( 11 ))

式中:E-弹簧的弹性模量;In the formula: the elastic modulus of E-spring;

η-黏壶的粘度;η-viscosity of sticky pot;

t-作用时间;t-action time;

根据蠕变公式:According to the creep formula:

ϵϵ == ϵϵ 00 (( 11 -- ee -- EE. ηη ·&Center Dot; tt )) -- -- -- (( 22 ))

推导出弹簧的弹性模量公式:The formula for the modulus of elasticity of the spring is derived:

EE. == σσ 00 -- σσ (( tt )) ϵϵ (( tt )) -- -- -- (( 33 ))

式中:σ(t)-某一时间的应力;In the formula: σ(t)-stress at a certain time;

ε(t)-某一时间的应变;ε(t) - strain at a certain time;

黏壶的粘度计算公式:The formula for calculating the viscosity of the sticky pot:

ηη == EE. (( tt )) lnln σσ 00 σσ -- -- -- (( 44 ))

设麦克斯韦模型的测量装置中的弹簧的弹性模量E1、麦克斯韦模型的测量装置中的黏壶的粘度η1Suppose the elastic modulus E 1 of the spring in the measuring device of the Maxwell model, the viscosity η 1 of the sticky pot in the measuring device of the Maxwell model;

设开尔芬模型的测量装置中的弹簧的弹性模量E2、开尔芬模型的测量装置中的黏壶的粘度η2Assuming the elastic modulus E 2 of the spring in the measuring device of the Kelvin model, the viscosity η 2 of the sticky pot in the measuring device of the Kelvin model;

根据上述公式(3)求得麦克斯韦模型的测量装置中的弹簧的弹性模量E1及开尔芬模型的测量装置中的弹簧的弹性模量E2;根据上述公式(4)求得麦克斯韦模型的测量装置中的黏壶的粘度η1及开尔芬模型的测量装置中的黏壶的粘度η2Obtain the modulus of elasticity E 1 of the spring in the measuring device of Maxwell model and the elastic modulus E 2 of the spring in the measuring device of Kelvin model according to above-mentioned formula (3); Obtain Maxwell's model according to above-mentioned formula (4) The viscosity η 1 of the sticky pot in the measuring device and the viscosity η 2 of the sticky pot in the measuring device of the Kelvin model;

步骤二:往四元件模型的测量装置的托盘添加砝码,相当于施加一个恒定的应力σ0,通过所述四元件模型的测量装置的应变仪测出四元件模型应变的大小,绘制应变与时间的关系曲线,即蠕变曲线;再将上述通过计算求得的麦克斯韦模型的测量装置中的弹簧的弹性模量E1、开尔芬模型的测量装置中的弹簧的弹性模量E2、麦克斯韦模型的测量装置中的黏壶的粘度η1及开尔芬模型的测量装置中的黏壶的粘度η2代入四元件力学模型的蠕变方程中,Step 2: Add weights to the tray of the measuring device of the four-element model, which is equivalent to applying a constant stress σ 0 , measure the strain of the four-element model through the strain gauge of the measuring device of the four-element model, and draw the strain and The relationship curve of time, that is, the creep curve; then the elastic modulus E 1 of the spring in the measuring device of the Maxwell model obtained by the above calculation, the elastic modulus E 2 of the spring in the measuring device of the Kelvin model, The viscosity η of the sticky pot in the measuring device of the Maxwell model and the viscosity η of the sticky pot in the measuring device of the Kelvin model 2 are substituted in the creep equation of the four-element mechanics model,

ϵϵ (( tt )) == σσ 00 EE. 11 ++ σσ 00 EE. 22 (( 11 -- ee -- EE. 22 ηη 22 )) ++ σσ 00 ηη 11 tt -- -- -- (( 55 ))

代入不同的时间t得到一个计算的蠕变曲线,将计算得到的蠕变曲线与测定得到的蠕变曲线相叠加对比,得到的结果是上述两种蠕变曲线基本吻合。A calculated creep curve is obtained by substituting different times t, and the calculated creep curve is superimposed and compared with the measured creep curve, and the result obtained is that the above two creep curves are basically consistent.

本发明的有益效果是:本发明把一种经典的、仅存在于纸面上的聚合物粘弹性力学模型转化成为一台实际的聚合物粘弹性力学模型测量装置,通过理论推导和实验数据都证明了该力学模型装置能够比较准确地反映聚合物的粘弹性的一些规律,并且证明了聚合物粘弹性力学模型不再是一个抽象的力学模型,而是一个具象的、可以实际应用的力学模型,实际弹簧的弹性模量E值和实际黏壶的粘度η值是可以测量和计算出来的,实际的力学曲线也可以测量出来,因此本发明填补了聚合物粘弹性理论与实践结合的一个空白。The beneficial effects of the present invention are: the present invention converts a classic polymer viscoelasticity model that only exists on paper into an actual polymer viscoelasticity model measuring device, through theoretical derivation and experimental data It proves that the mechanical model device can accurately reflect some laws of polymer viscoelasticity, and proves that the polymer viscoelastic mechanical model is no longer an abstract mechanical model, but a concrete mechanical model that can be used in practice , the elastic modulus E value of the actual spring and the viscosity η value of the actual sticky pot can be measured and calculated, and the actual mechanical curve can also be measured, so the present invention fills up a gap in the combination of polymer viscoelasticity theory and practice .

附图说明 Description of drawings

图1a是本发明的聚合物粘弹性模型的测量装置的主视图,图中表示的是麦克斯韦模型的测量装置的主视图;图1b是本发明的聚合物粘弹性模型的测量装置的主视图,图中表示的是开尔芬模型的测量装置的主视图;图1c是本发明的聚合物粘弹性模型的测量装置的主视图,图中表示的是三元件模型的测量装置的主视图;图1d是本发明的聚合物粘弹性模型的测量装置的主视图,图中表示的是四元件模型的测量装置的主视图;图2是弹簧I和黏壶I串联以后组成的麦克斯韦模型的测量装置测试得到的应力松弛曲线图;图3是弹簧I和黏壶I并联以后组成的开尔芬模型的测量装置测试得到的蠕变曲线图;图4是弹簧II和黏壶II串联以后组成的麦克斯韦模型的测量装置测试得到的应力松弛曲线图;图5是弹簧II和黏壶II并联以后组成的开尔芬模型的测量装置测试得到的蠕变曲线图;图6是弹簧I、黏壶I、弹簧II及黏壶II组成的四元件模型的测量装置测试得到的蠕变曲线图;图7是经计算得到的E1、E2、η1、η2代入四元件力学模型的蠕变方程,代入不同的时间t得到的计算的蠕变曲线图;图8是实验蠕变曲线与计算蠕变曲线相叠加的对比曲线图,图中与图7形状相近的曲线为计算蠕变曲线,另一条曲线为实验蠕变曲线。Fig. 1 a is the front view of the measuring device of the polymer viscoelastic model of the present invention, and what represent among the figure is the front view of the measuring device of Maxwell model; Fig. 1 b is the front view of the measuring device of the polymer viscoelastic model of the present invention, Represented among the figure is the front view of the measuring device of the Kelvin model; Fig. 1c is the front view of the measuring device of the polymer viscoelasticity model of the present invention, and what represent among the figure is the front view of the measuring device of the three-element model; Fig. 1d is the front view of the measuring device of the polymer viscoelasticity model of the present invention, and what represent among the figure is the front view of the measuring device of the four-element model; Fig. 2 is the measuring device of the Maxwell model that spring I and sticky pot I are connected in series The stress relaxation curve obtained from the test; Figure 3 is the creep curve obtained from the test of the measuring device of the Kelvin model composed of the spring I and the sticky pot I in parallel; Figure 4 is the Maxwell model composed of the spring II and the sticky pot II in series The stress relaxation curve obtained from the measurement device test of the model; Fig. 5 is the creep curve obtained from the measurement device test of the Kelvin model formed after spring II and sticky pot II are connected in parallel; Fig. 6 is the spring I, sticky pot I, The creep curve obtained from the test of the measuring device of the four-element model composed of spring II and sticky pot II; Figure 7 is the calculated creep equation of E 1 , E 2 , η 1 , η 2 substituted into the four-element mechanical model, The calculated creep curve obtained by substituting different time t; Figure 8 is a comparison curve of the superposition of the experimental creep curve and the calculated creep curve. The curve is the experimental creep curve.

具体实施方式 Detailed ways

具体实施方式一:结合图1a说明,本实施方式的聚合物粘弹性模型的测量装置为麦克斯韦模型的测量装置,所述麦克斯韦模型的测量装置底座1、测力计2、弹簧3、黏壶4、两个固定端板5、四根拉杆6及三个活动板7;两个固定端板5分别是第一固定端板5-1和第二固定端板5-2,三个活动板7分别是第一活动板7-1、第二活动板7-2和第三活动板7-3;Specific embodiment one: in conjunction with Fig. 1a explanation, the measuring device of the polymer viscoelasticity model of the present embodiment is the measuring device of Maxwell model, the measuring device base 1 of described Maxwell model, dynamometer 2, spring 3, glue pot 4 , two fixed end plates 5, four pull rods 6 and three movable plates 7; the two fixed end plates 5 are respectively the first fixed end plate 5-1 and the second fixed end plate 5-2, and the three movable plates 7 Respectively the first movable board 7-1, the second movable board 7-2 and the third movable board 7-3;

两个固定端板5垂直且并列固定在底座1上,两个固定端板5之间水平且呈矩形阵列式固定有四根拉杆6,由四根拉杆6和两个固定端板5组成框架式结构,三个活动板7与两个固定端板5平行设置并位于两个固定端板5之间,第一活动板7-1与第一固定端板5-1相邻设置,第三活动板7-3与第二固定端板5-2相邻设置,第二活动板7-2设置在第一活动板7-1与第三活动板7-3之间,每个活动板7上与四根拉杆6相对应位置设有四个通孔,每个活动板7的四个通孔套装在四根拉杆6上,三个活动板7与四根拉杆6滑动连接(三个活动板7可以在四根拉杆6上做平行滑动),第一活动板7-1与第二活动板7-2之间固连有弹簧3,第二活动板7-2与第三活动板7-3之间固连有黏壶4,测力计2设置在第一活动板7-1和第二活动板7-2之间,测力计2与第一活动板7-1和第二活动板7-2固接。Two fixed end plates 5 are fixed vertically and side by side on the base 1, four tie rods 6 are fixed horizontally and in a rectangular array between the two fixed end plates 5, and the frame is composed of four tie rods 6 and two fixed end plates 5 type structure, three movable plates 7 are arranged in parallel with two fixed end plates 5 and are located between the two fixed end plates 5, the first movable plate 7-1 is arranged adjacent to the first fixed end plate 5-1, and the third The movable plate 7-3 is arranged adjacent to the second fixed end plate 5-2, and the second movable plate 7-2 is arranged between the first movable plate 7-1 and the third movable plate 7-3, and each movable plate 7 Four through holes are arranged on the corresponding position with four pull rods 6, and four through holes of each movable plate 7 are set on four pull rods 6, and three movable plates 7 are slidingly connected with four pull rods 6 (three movable Plate 7 can do parallel sliding on four pull rods 6), is fixedly connected with spring 3 between the first movable plate 7-1 and the second movable plate 7-2, the second movable plate 7-2 and the third movable plate 7 -3 is fixedly connected with a sticky pot 4, and the dynamometer 2 is arranged between the first movable plate 7-1 and the second movable plate 7-2, and the dynamometer 2 is connected to the first movable plate 7-1 and the second movable plate 7-1. Movable plate 7-2 is fixedly connected.

麦克斯韦模型中的黏壶4与弹簧3串联,移动第三活动板7-3使其保持一个恒定形变,则麦克斯韦模型会产生的应力松弛现象(即应力随时间的增加而降低)。The sticky pot 4 in the Maxwell model is connected in series with the spring 3, and the third movable plate 7-3 is moved to keep a constant deformation, then the stress relaxation phenomenon (that is, the stress increases with time) will be produced by the Maxwell model.

具体实施方式二:结合图1b说明,本实施方式的聚合物粘弹性模型的测量装置为开尔芬模型的测量装置,所述开尔芬模型的测量装置包括底座1、拉绳8、托盘9、砝码10、定滑轮11、应变仪12、弹簧3、黏壶4、连杆13、两个固定端板5、四根拉杆6及三个活动板7;两个固定端板5分别是第一固定端板5-1和第二固定端板5-2,三个活动板7分别是第一活动板7-1、第二活动板7-2和第三活动板7-3;Specific embodiment two: in conjunction with Fig. 1 b explanation, the measuring device of the polymer viscoelasticity model of the present embodiment is the measuring device of Kelvin model, and the measuring device of described Kelvin model comprises base 1, stay cord 8, tray 9 , weight 10, fixed pulley 11, strain gauge 12, spring 3, sticky pot 4, connecting rod 13, two fixed end plates 5, four pull rods 6 and three movable plates 7; the two fixed end plates 5 are respectively The first fixed end plate 5-1 and the second fixed end plate 5-2, and the three movable plates 7 are respectively the first movable plate 7-1, the second movable plate 7-2 and the third movable plate 7-3;

两个固定端板5垂直且并列固定在底座1上,两个固定端板5之间水平且呈矩形阵列式固定有四根拉杆6,由四根拉杆6和两个固定端板5组成框架式结构,三个活动板7与两个固定端板5平行设置并位于两个固定端板5之间,第一活动板7-1与第一固定端板5-1相邻设置,第三活动板7-3与第二固定端板5-2相邻设置,第二活动板7-2设置在第一活动板7-1与第三活动板7-3之间,每个活动板7上与四根拉杆6相对应位置设有四个通孔,每个活动板7的四个通孔套装在四根拉杆6上,三个活动板7与四根拉杆6滑动连接(三个活动板7可以在四根拉杆6上做平行滑动),托盘9设置在第一固定端板5-1的外部,定滑轮11固定在第一固定端板5-1的外侧面上,砝码10装在托盘9上,第一固定端板5-1上设有拉绳穿过孔5-1-1,拉绳8的一端与托盘9固接,拉绳8的另一端绕过定滑轮11并穿过所述第一固定端板5-1的拉绳穿过孔5-1-1与第一活动板7-1固接,第二活动板7-2与第三活动板7-3之间并联设置有弹簧3和黏壶4,第一活动板7-1与第二活动板7-2之间固连有一个连杆13,应变仪12设置在第一活动板7-1与第二活动板7-2之间,且应变仪12与第一活动板7-1固接。Two fixed end plates 5 are fixed vertically and side by side on the base 1, four tie rods 6 are fixed horizontally and in a rectangular array between the two fixed end plates 5, and the frame is composed of four tie rods 6 and two fixed end plates 5 type structure, three movable plates 7 are arranged in parallel with two fixed end plates 5 and are located between the two fixed end plates 5, the first movable plate 7-1 is arranged adjacent to the first fixed end plate 5-1, and the third The movable plate 7-3 is arranged adjacent to the second fixed end plate 5-2, and the second movable plate 7-2 is arranged between the first movable plate 7-1 and the third movable plate 7-3, and each movable plate 7 Four through holes are arranged on the corresponding position with four pull rods 6, and the four through holes of each movable plate 7 are set on the four pull rods 6, and the three movable plates 7 are slidably connected with the four pull rods 6 (three movable Plate 7 can do parallel sliding on four pull rods 6), tray 9 is arranged on the outside of first fixed end plate 5-1, fixed pulley 11 is fixed on the outer surface of first fixed end plate 5-1, weight 10 Installed on the tray 9, the first fixed end plate 5-1 is provided with a drawstring through hole 5-1-1, one end of the drawstring 8 is fixedly connected to the tray 9, and the other end of the drawstring 8 bypasses the fixed pulley 11 And the stay cord passing through the first fixed end plate 5-1 is affixed to the first movable plate 7-1 through the hole 5-1-1, and the second movable plate 7-2 is connected to the third movable plate 7-3. A spring 3 and a sticky pot 4 are arranged in parallel between them, a connecting rod 13 is fixedly connected between the first movable plate 7-1 and the second movable plate 7-2, and the strain gauge 12 is arranged on the first movable plate 7-1 and the second movable plate 7-2. Between the second movable plates 7-2, the strain gauge 12 is fixedly connected to the first movable plate 7-1.

选择一定的砝码10装在托盘9上使开尔芬模型产生一个恒定的应力,则开尔芬模型会产生一个蠕变现象(即形变随时间的增加而增加)。Select a certain weight 10 to be installed on the tray 9 to make the Kelvin model produce a constant stress, then the Kelvin model will produce a creep phenomenon (that is, the deformation increases with time).

具体实施方式三:结合图1c说明,本实施方式的聚合物粘弹性模型的测量装置为三元件模型的测量装置,所述三元件模型的测量装置包括底座1、拉绳8、托盘9、砝码10、定滑轮11、测力计2、应变仪12、黏壶4、两个弹簧3、两个固定端板5、四根拉杆6及三个活动板7;两个固定端板5分别是第一固定端板5-1和第二固定端板5-2,三个活动板7分别是第一活动板7-1、第二活动板7-2和第三活动板7-3;Specific embodiment three: in conjunction with Fig. 1 c explanation, the measuring device of the polymer viscoelasticity model of the present embodiment is the measuring device of three-element model, and the measuring device of described three-element model comprises base 1, pull cord 8, pallet 9, weight Code 10, fixed pulley 11, dynamometer 2, strain gauge 12, sticky pot 4, two springs 3, two fixed end plates 5, four pull rods 6 and three movable plates 7; two fixed end plates 5 are respectively It is the first fixed end plate 5-1 and the second fixed end plate 5-2, and the three movable plates 7 are respectively the first movable plate 7-1, the second movable plate 7-2 and the third movable plate 7-3;

两个固定端板5垂直且并列固定在底座1上,两个固定端板5之间水平且呈矩形阵列式固定有四根拉杆6,由四根拉杆6和两个固定端板5组成框架式结构,三个活动板7与两个固定端板5平行设置并位于两个固定端板5之间,第一活动板7-1与第一固定端板5-1相邻设置,第三活动板7-3与第二固定端板5-2相邻设置,第二活动板7-2设置在第一活动板7-1与第三活动板7-3之间,每个活动板7上与四根拉杆6相对应位置设有四个通孔,每个活动板7的四个通孔套装在四根拉杆6上,三个活动板7与四根拉杆6滑动连接(三个活动板7可以在四根拉杆6上做平行滑动),托盘9设置在第一固定端板5-1的外部,定滑轮11固定在第一固定端板5-1的外侧面上,砝码10装在托盘9上,第一固定端板5-1上设有拉绳穿过孔5-1-1,拉绳8的一端与托盘9固接,拉绳8的另一端绕过定滑轮11并穿过所述第一固定端板5-1的拉绳穿过孔5-1-1与测力计2固接,测力计2与第一活动板7-1固接,应变仪12设置在第一活动板7-1与第二活动板7-2之间,且应变仪12与第一活动板7-1固接,两个弹簧3中的一个固连在第一活动板7-1与第二活动板7-2之间,两个弹簧3中的剩余一个与黏壶4并联在第二活动板7-2与第三活动板7-3之间。在托盘9上加上砝码10通过定滑轮11产生一个水平力,水平力的大小通过测力计2显示,三元件模型(力学模型)产生的形变通过应变仪12显示。Two fixed end plates 5 are fixed vertically and side by side on the base 1, four tie rods 6 are fixed horizontally and in a rectangular array between the two fixed end plates 5, and the frame is composed of four tie rods 6 and two fixed end plates 5 type structure, three movable plates 7 are arranged in parallel with two fixed end plates 5 and are located between the two fixed end plates 5, the first movable plate 7-1 is arranged adjacent to the first fixed end plate 5-1, and the third The movable plate 7-3 is arranged adjacent to the second fixed end plate 5-2, and the second movable plate 7-2 is arranged between the first movable plate 7-1 and the third movable plate 7-3, and each movable plate 7 Four through holes are arranged on the corresponding position with four pull rods 6, and the four through holes of each movable plate 7 are set on the four pull rods 6, and the three movable plates 7 are slidably connected with the four pull rods 6 (three movable Plate 7 can do parallel sliding on four pull rods 6), tray 9 is arranged on the outside of first fixed end plate 5-1, fixed pulley 11 is fixed on the outer surface of first fixed end plate 5-1, weight 10 Installed on the tray 9, the first fixed end plate 5-1 is provided with a drawstring passing hole 5-1-1, one end of the drawstring 8 is fixedly connected to the tray 9, and the other end of the drawstring 8 bypasses the fixed pulley 11 And the stay cord passing through the first fixed end plate 5-1 is fixedly connected with the dynamometer 2 through the hole 5-1-1, the dynamometer 2 is fixedly connected with the first movable plate 7-1, and the strain gauge 12 It is arranged between the first movable plate 7-1 and the second movable plate 7-2, and the strain gauge 12 is fixedly connected to the first movable plate 7-1, and one of the two springs 3 is fixedly connected to the first movable plate 7 Between -1 and the second movable plate 7-2, the remaining one in the two springs 3 is connected in parallel with the glue pot 4 between the second movable plate 7-2 and the third movable plate 7-3. Adding a weight 10 on the pallet 9 generates a horizontal force through the fixed pulley 11, the size of the horizontal force is displayed by the load cell 2, and the deformation generated by the three-element model (mechanical model) is displayed by the strain gauge 12.

具体实施方式四:结合图1d说明,本实施方式的聚合物粘弹性模型的测量装置为四元件模型的测量装置,所述四元件模型的测量装置包括底座1、拉绳8、托盘9、砝码10、定滑轮11、测力计2、应变仪12、两个黏壶4、两个弹簧3、两个固定端板4、四根拉杆6及三个活动板7;两个固定端板5分别是第一固定端板5-1和第二固定端板5-2,三个活动板7分别是第一活动板7-1、第二活动板7-2和第三活动板7-3;Specific embodiment four: in conjunction with Fig. 1d explanation, the measuring device of the polymer viscoelasticity model of the present embodiment is the measuring device of four-element model, and the measuring device of described four-element model comprises base 1, pull cord 8, pallet 9, weight Code 10, fixed pulley 11, dynamometer 2, strain gauge 12, two sticky pots 4, two springs 3, two fixed end plates 4, four pull rods 6 and three movable plates 7; two fixed end plates 5 are respectively the first fixed end plate 5-1 and the second fixed end plate 5-2, and the three movable plates 7 are respectively the first movable plate 7-1, the second movable plate 7-2 and the third movable plate 7- 3;

两个固定端板5垂直且并列固定在底座1上,两个固定端板5之间水平且呈矩形阵列式固定有四根拉杆6,由四根拉杆6和两个固定端板5组成框架式结构,三个活动板7与两个固定端板5平行设置并位于两个固定端板5之间,第一活动板7-1与第一固定端板5-1相邻设置,第三活动板7-3与第二固定端板5-2相邻设置,第二活动板7-2设置在第一活动板7-1与第三活动板7-3之间,每个活动板7上与四根拉杆6相对应位置设有四个通孔,每个活动板7的四个通孔套装在四根拉杆6上,三个活动板7与四根拉杆6滑动连接(三个活动板7可以在四根拉杆6上做平行滑动),托盘9设置在第一固定端板5-1的外部,定滑轮11固定在第一固定端板5-1的外侧面上,砝码10装在托盘9上,第一固定端板5-1上设有拉绳穿过孔5-1-1,拉绳8的一端与托盘9固接,拉绳8的另一端绕过定滑轮11并穿过所述第一固定端板5-1的拉绳穿过孔5-1-1与测力计2固接,测力计2与第一活动板7-1固接,应变仪12设置在第一活动板7-1与第二活动板7-2之间,且应变仪12与第一活动板7-1固接,两个弹簧3中的一个弹簧3固连在第一活动板7-1与第二活动板7-2之间,两个黏壶4中的一个黏壶4与两个弹簧3中的剩余一个弹簧3并联于第二活动板7-2与第三活动板7-3之间,两个黏壶4中的剩余一个黏壶4固连于第三活动板7-3与第二固定端板5-2之间。Two fixed end plates 5 are fixed vertically and side by side on the base 1, four tie rods 6 are fixed horizontally and in a rectangular array between the two fixed end plates 5, and the frame is composed of four tie rods 6 and two fixed end plates 5 type structure, three movable plates 7 are arranged in parallel with two fixed end plates 5 and are located between the two fixed end plates 5, the first movable plate 7-1 is arranged adjacent to the first fixed end plate 5-1, and the third The movable plate 7-3 is arranged adjacent to the second fixed end plate 5-2, and the second movable plate 7-2 is arranged between the first movable plate 7-1 and the third movable plate 7-3, and each movable plate 7 Four through holes are arranged on the corresponding position with four pull rods 6, and four through holes of each movable plate 7 are set on four pull rods 6, and three movable plates 7 are slidingly connected with four pull rods 6 (three movable Plate 7 can do parallel sliding on four pull rods 6), tray 9 is arranged on the outside of first fixed end plate 5-1, fixed pulley 11 is fixed on the outer surface of first fixed end plate 5-1, weight 10 Installed on the tray 9, the first fixed end plate 5-1 is provided with a drawstring passing hole 5-1-1, one end of the drawstring 8 is fixedly connected to the tray 9, and the other end of the drawstring 8 bypasses the fixed pulley 11 And the stay cord passing through the first fixed end plate 5-1 is fixedly connected with the dynamometer 2 through the hole 5-1-1, the dynamometer 2 is fixedly connected with the first movable plate 7-1, and the strain gauge 12 It is arranged between the first movable plate 7-1 and the second movable plate 7-2, and the strain gauge 12 is fixedly connected to the first movable plate 7-1, and one of the two springs 3 is fixedly connected to the first movable plate Between the plate 7-1 and the second movable plate 7-2, one sticky pot 4 in the two sticky pots 4 and the remaining spring 3 in the two springs 3 are connected in parallel to the second movable plate 7-2 and the third movable plate. Between the plates 7-3, the remaining one of the two sticky pots 4 is fixedly connected between the third movable plate 7-3 and the second fixed end plate 5-2.

在托盘9上加上砝码10通过定滑轮11产生一个水平力作用到四元件模型上使其产生一个恒定的应力,水平力的大小可以通过测力计2显示,四元件模型产生的形变通过应变仪12显示。A weight 10 is added to the tray 9 to generate a horizontal force through the fixed pulley 11 to act on the four-element model to generate a constant stress. The magnitude of the horizontal force can be displayed by the dynamometer 2, and the deformation generated by the four-element model is passed through The strain gauge 12 is displayed.

具体实施方式五:本实施方式的利用具体实施方式一、二及四聚合物粘弹性模型的测量装置实现模型元件参数的测量方法,所述测量方法由以下步骤完成:Specific embodiment five: the measuring device of the utilization specific embodiment one, two and four polymer viscoelasticity models of this embodiment realizes the measuring method of model element parameter, and described measuring method is finished by the following steps:

步骤一:让麦克斯韦模型的测量装置中的第一活动板7-1和第三活动板7-3同时产生恒定位移,使得麦克斯韦模型产生恒定形变ε0,并通过麦克斯韦模型的测量装置的测力计2测出麦克斯韦模型在某时刻应力的大小,绘制应力与时间的关系曲线,即应力松弛曲线;Step 1: Let the first movable plate 7-1 and the third movable plate 7-3 in the measuring device of the Maxwell model produce constant displacement at the same time, so that the Maxwell model produces a constant deformation ε 0 , and measure the force through the measuring device of the Maxwell model Meter 2 measures the magnitude of the stress of the Maxwell model at a certain moment, and draws the relationship curve between stress and time, that is, the stress relaxation curve;

往开尔芬模型的测量装置的托盘9上添加砝码10,相当于施加一个恒定的应力σ0,通过开尔芬模型的测量装置的应变仪12测出开尔芬模型在某时刻应变的大小,绘制应变与时间的关系曲线,即蠕变曲线。Adding a weight 10 to the tray 9 of the measuring device of the Kelvin model is equivalent to applying a constant stress σ 0 , and the strain gauge 12 of the measuring device of the Kelvin model is used to measure the strain of the Kelvin model at a certain moment Size, plot the relationship between strain and time, that is, the creep curve.

根据应力松弛公式:According to the stress relaxation formula:

σσ == σσ 00 ee -- EE. ηη ·· tt -- -- -- (( 11 ))

式中:E-弹簧的弹性模量;In the formula: the elastic modulus of E-spring;

η-黏壶的粘度;η-viscosity of sticky pot;

t-作用时间;t-action time;

根据蠕变公式:According to the creep formula:

ϵϵ == ϵϵ 00 (( 11 -- ee -- EE. ηη ·&Center Dot; tt )) -- -- -- (( 22 ))

推导出弹簧的弹性模量公式:The formula for the modulus of elasticity of the spring is derived:

EE. == σσ 00 -- σσ (( tt )) ϵϵ (( tt )) -- -- -- (( 33 ))

式中:σ(t)-某一时间的应力;In the formula: σ(t)-stress at a certain time;

ε(t)-某一时间的应变;ε(t) - strain at a certain time;

黏壶的粘度计算公式:The formula for calculating the viscosity of the sticky pot:

ηη == EE. (( tt )) lnln σσ 00 σσ -- -- -- (( 44 ))

设麦克斯韦模型的测量装置中的弹簧3的弹性模量E1、麦克斯韦模型的测量装置中的黏壶4的粘度η1Assuming the elastic modulus E 1 of the spring 3 in the measuring device of the Maxwell model, the viscosity η 1 of the sticky pot 4 in the measuring device of the Maxwell model;

设开尔芬模型的测量装置中的弹簧3的弹性模量E2、开尔芬模型的测量装置中的黏壶4的粘度η2The elastic modulus E 2 of the spring 3 in the measuring device of the Kelvin model, the viscosity η 2 of the sticky pot 4 in the measuring device of the Kelvin model;

根据上述公式(3)求得麦克斯韦模型的测量装置中的弹簧3的弹性模量E1及开尔芬模型的测量装置中的弹簧3的弹性模量E2;根据上述公式(4)求得麦克斯韦模型的测量装置中的黏壶的4粘度η1及开尔芬模型的测量装置中的黏壶4的粘度η2Obtain the modulus of elasticity E 1 of the spring 3 in the measuring device of Maxwell model and the elastic modulus E 2 of the spring 3 in the measuring device of the Kelvin model according to above-mentioned formula (3); Obtain according to above-mentioned formula (4) 4 viscosity η 1 of sticky pot in the measuring device of Maxwell model and the viscosity η 2 of sticking pot 4 in the measuring device of Kelvin model;

步骤二:往四元件模型的测量装置的托盘9添加砝码10,相当于施加一个恒定的应力σ0,通过所述四元件模型的测量装置的应变仪12测出四元件模型应变的大小,绘制应变与时间的关系曲线,即蠕变曲线;再将上述通过计算求得的麦克斯韦模型的测量装置中的弹簧3的弹性模量E1、开尔芬模型的测量装置中的弹簧3的弹性模量E2、麦克斯韦模型的测量装置中的黏壶的4粘度η1及开尔芬模型的测量装置中的黏壶4的粘度η2(即经计算得到的E1、E2、η1、η2)代入四元件力学模型的蠕变方程中,Step 2: adding a weight 10 to the tray 9 of the measuring device of the four-element model, which is equivalent to applying a constant stress σ 0 , and measuring the strain of the four-element model through the strain gauge 12 of the measuring device of the four-element model, Draw the relationship curve of strain and time, i.e. the creep curve; then the elastic modulus E 1 of the spring 3 in the measuring device of the Maxwell model obtained by calculation and the elasticity of the spring 3 in the measuring device of the Kelvin model Modulus E 2 , the viscosity η 1 of the sticky pot 4 in the measuring device of the Maxwell model and the viscosity η 2 of the sticky pot 4 in the measuring device of the Kelvin model (that is, the calculated E 1 , E 2 , η 1 , η 2 ) into the creep equation of the four-element mechanical model,

ϵϵ (( tt )) == σσ 00 EE. 11 ++ σσ 00 EE. 22 (( 11 -- ee -- EE. 22 ηη 22 )) ++ σσ 00 ηη 11 tt -- -- -- (( 55 ))

代入不同的时间t得到一个计算的蠕变曲线,将计算得到的蠕变曲线与测定得到的蠕变曲线相叠加对比,得到的结果是上述两种蠕变曲线基本吻合,说明实际的弹簧和黏壶可以代替抽象的弹簧和黏壶,因此表明实际的、具象的力学模型可以代替经典的、抽象的力学模型。Substituting different time t to get a calculated creep curve, and comparing the calculated creep curve with the measured creep curve, the result is that the above two creep curves are basically consistent, indicating that the actual spring and viscous The pot can replace the abstract spring and sticky pot, thus showing that the actual, concrete mechanical model can replace the classical, abstract mechanical model.

实施例1:本实施例是利用本发明的聚合物粘弹性模型的测量装置实现模型元件参数的测量方法,具体方法步骤如下:Embodiment 1: The present embodiment is to utilize the measuring device of polymer viscoelasticity model of the present invention to realize the measuring method of model element parameter, and concrete method step is as follows:

一、E1和η1的测定:One, the mensuration of E 1 and η 1 :

选取一个钢丝拉力弹簧,本实施例中设定弹簧I作为弹性元件,钢丝直径为1.54mm,中径为17.16mm、工作长度为260mm;选取一个黏壶,本实施例中设定黏壶I作为粘性元件,黏壶I内径为19mm、工作长度为166mm,工作介质为牛顿型流体甘油。首先将两种元件(弹簧I和黏壶I)串联(利用麦克斯韦模型的测量装置,见图1a),组成一个实际的Maxwell模型,再施加一个恒定的应变ε0,经过测试得到一个应力松弛曲线,见图2;Choose a steel wire tension spring, set spring I as elastic element in the present embodiment, steel wire diameter is 1.54mm, middle diameter is 17.16mm, working length is 260mm; Choose a sticky pot, set sticky pot I as in the present embodiment Viscous components, the inner diameter of the sticky pot I is 19mm, the working length is 166mm, and the working medium is Newtonian fluid glycerin. First, two elements (spring I and sticky pot I) are connected in series (using the measuring device of the Maxwell model, see Figure 1a) to form an actual Maxwell model, and then a constant strain ε 0 is applied, and a stress relaxation curve is obtained after testing , see Figure 2;

其次,再将上述两种元件并联(利用开尔芬模型的测量装置,见图1b)得到一个实际的Kelvin模型,施加一个恒定的应力σ0,经过测试,得到一个蠕变曲线,见图3;由公式(3)和公式(4)计算并且经过算术平均得到:E1=1068.99MPa,η1=3013.66MPa·s;E1为弹簧I的弹性模量,η1为黏壶I的粘度;Secondly, connect the above two components in parallel (use the Kelvin model measuring device, see Figure 1b) to obtain an actual Kelvin model, apply a constant stress σ 0 , and obtain a creep curve after testing, as shown in Figure 3 ; Calculated by formula (3) and formula (4) and obtained through arithmetic average: E 1 =1068.99MPa, η 1 =3013.66MPa·s; E 1 is the elastic modulus of spring I, and η 1 is the viscosity of sticky pot I ;

步骤二:E2和η2的测定:Step 2: the mensuration of E 2 and η 2 :

选取一个钢丝拉力弹簧,本实施例中设定弹簧II作为弹性元件,弹簧II的钢丝直径为1.75mm、中径为18.78mm、工作长度为90mm;选取一个黏壶,本实施例中设定黏壶II作为粘性元件,黏壶II的内径为30mm、工作长度为136mm,工作介质为甘油。同样方法,将上述两种元件串联(利用麦克斯韦模型的测量装置,见图1a)组成Maxwell模型,得到的应力松弛曲线见图4;将上述两种元件并联(利用开尔芬模型的测量装置,见图1b)组成Kelvin模型,得到的蠕变曲线见图5;经过计算和算术平均得到E2=1299.80MPa,η2=77347.37MPa·s;E1为弹簧II的弹性模量,η1为黏壶II的粘度;Choose a steel wire tension spring, set spring II as the elastic element in this embodiment, the steel wire diameter of spring II is 1.75mm, the middle diameter is 18.78mm, and the working length is 90mm; choose a sticky pot, set sticky pot in this embodiment The pot II is used as a viscous element. The inner diameter of the sticky pot II is 30mm, the working length is 136mm, and the working medium is glycerin. In the same way, the above two components are connected in series (using the measuring device of the Maxwell model, see Figure 1a) to form a Maxwell model, and the stress relaxation curve obtained is shown in Figure 4; the above two components are connected in parallel (using the measuring device of the Kelvin model, See Figure 1b) to form the Kelvin model, and the obtained creep curve is shown in Figure 5; after calculation and arithmetic mean, E 2 =1299.80MPa, η 2 =77347.37MPa·s; E 1 is the elastic modulus of spring II, and η 1 is Viscosity of Sticky Pot II;

步骤三:四元件力学模型的力学曲线测定:Step 3: Determination of the mechanical curve of the four-element mechanical model:

将步骤一中的两个元件(弹簧I和黏壶I)及步骤二中的两个元件(弹簧II和黏壶II)在构筑四元件模型的测量装置中组成一个实际的四元件模型,见图1d,测定其蠕变曲线,见图6;再将计算得到的E1、E2、η1、η2代入四元件力学模型的蠕变方程,代入不同的时间t得到一个计算的蠕变曲线,见图7。The two components in step 1 (spring I and sticky pot I) and the two components in step 2 (spring II and sticky pot II) form an actual four-component model in the measuring device for constructing the four-component model, see Figure 1d, measure its creep curve, see Figure 6; then substitute the calculated E 1 , E 2 , η 1 , η 2 into the creep equation of the four-element mechanical model, and substitute different times t to obtain a calculated creep Curve, see Figure 7.

步骤四:将实验蠕变曲线与计算蠕变曲线相叠加对比见图8,由图可见,两种曲线基本吻合,说明实际的弹簧和黏壶可以代替抽象的弹簧和黏壶,因此表明实际的、具象(抽象的反义词)的力学模型可以代替经典的、抽象的力学模型。Step 4: Superimpose and compare the experimental creep curve and the calculated creep curve, as shown in Figure 8. It can be seen from the figure that the two curves are basically consistent, indicating that the actual spring and sticky pot can replace the abstract spring and sticky pot, so it shows that the actual , Concrete (the antonym of abstract) mechanical model can replace the classic, abstract mechanical model.

综上所述,本发明的一种聚合物粘弹性模型的测试装置不再是一种抽象的概念,而是一个实际的装置,用它可完成不同模型元件的组合,形成实际的麦克斯韦模型、开尔芬模型、三元件模型和四元件模型。然后可以考察和测量其相关的元件的参数和力学曲线。In summary, the test device of a polymer viscoelastic model of the present invention is no longer an abstract concept, but a practical device, with which the combination of different model elements can be completed to form an actual Maxwell model, Kelvin model, three-element model, and four-element model. The parameters and mechanical curves of its associated components can then be investigated and measured.

通过对实际的麦克斯韦模型和开尔芬模型测定,可计算出两个弹性模型元件的弹性模量为E1、E2和两个粘性模型元件的粘度η1、η2。将其代入到四元件力学模型的蠕变方程中,可得到一个蠕变曲线。再通过此装置组成一个实际的四元件力学模型,测定出一个蠕变曲线,该测定出一个蠕变曲线与计算的蠕变曲线相比较,两种曲线基本吻合,因此证明具象的、实际的力学模型可以代替经典的、抽象的力学模型。By measuring the actual Maxwell model and Kelvin model, the elastic moduli of the two elastic model elements can be calculated as E 1 , E 2 and the viscosities η 1 and η 2 of the two viscous model elements. Substituting it into the creep equation of the four-element mechanical model, a creep curve can be obtained. Then use this device to form an actual four-element mechanical model, and measure a creep curve. Compared with the calculated creep curve, the two curves are basically consistent, so it proves the concrete and actual mechanics. Models can replace classical, abstract mechanical models.

Claims (4)

1. the measurement mechanism of a polymer viscoelastic model; It is characterized in that: the measurement mechanism of said polymer viscoelastic model is the measurement mechanism of Maxwell model, and the measurement mechanism of said Maxwell model comprises base (1), dynamometer (2), spring (3), glutinous kettle (4), two fixed charge method end plates (5), four pull bars (6) and three portable plates (7); Two fixed charge method end plates (5) are respectively first fixed charge method end plate (5-1) and second fixed charge method end plate (5-2), and three portable plates (7) are respectively first portable plate (7-1), second portable plate (7-2) and the 3rd portable plate (7-3);
Two fixed charge method end plates (5) vertically and side by side are fixed on the base (1); Level and rectangular array are fixed with four pull bars (6) between two fixed charge method end plates (5); Form tower structure by four pull bars (6) and two fixed charge method end plates (5); Three portable plates (7) and two fixed charge method end plates (5) laterally arrange and are positioned between two fixed charge method end plates (5), first portable plate (7-1) and the adjacent setting of first fixed charge method end plate (5-1), the 3rd portable plate (7-3) and the adjacent setting of second fixed charge method end plate (5-2); Second portable plate (7-2) is arranged between first portable plate (7-1) and the 3rd portable plate (7-3); Each portable plate (7) is gone up with four pull bars (6) opposite position and is provided with four through holes, and four through holes of each portable plate (7) are sleeved on four pull bars (6), and three portable plates (7) are slidingly connected with four pull bars (6); Be fixed with spring (3) between first portable plate (7-1) and second portable plate (7-2); Be fixed with glutinous kettle (4) between second portable plate (7-2) and the 3rd portable plate (7-3), dynamometer (2) is arranged between first portable plate (7-1) and second portable plate (7-2), and dynamometer (2) is affixed with first portable plate (7-1) and second portable plate (7-2).
2. the measurement mechanism of a polymer viscoelastic model; It is characterized in that: the measurement mechanism of said polymer viscoelastic model is the measurement mechanism of degree Kelvin model, and the measurement mechanism of said degree Kelvin model comprises base (1), stay cord (8), pallet (9), counterweight (10), fixed pulley (11), strainmeter (12), spring (3), glutinous kettle (4), connecting rod (13), two fixed charge method end plates (5), four pull bars (6) and three portable plates (7); Two fixed charge method end plates (5) are respectively first fixed charge method end plate (5-1) and second fixed charge method end plate (5-2), and three portable plates (7) are respectively first portable plate (7-1), second portable plate (7-2) and the 3rd portable plate (7-3);
Two fixed charge method end plates (5) vertically and side by side are fixed on the base (1); Level and rectangular array are fixed with four pull bars (6) between two fixed charge method end plates (5); Form tower structure by four pull bars (6) and two fixed charge method end plates (5); Three portable plates (7) and two fixed charge method end plates (5) laterally arrange and are positioned between two fixed charge method end plates (5), first portable plate (7-1) and the adjacent setting of first fixed charge method end plate (5-1), the 3rd portable plate (7-3) and the adjacent setting of second fixed charge method end plate (5-2); Second portable plate (7-2) is arranged between first portable plate (7-1) and the 3rd portable plate (7-3); Each portable plate (7) is gone up with four pull bars (6) opposite position and is provided with four through holes, and four through holes of each portable plate (7) are sleeved on four pull bars (6), and three portable plates (7) are slidingly connected with four pull bars (6); Pallet (9) is arranged on the outside of first fixed charge method end plate (5-1); Fixed pulley (11) is fixed on the lateral surface of first fixed charge method end plate (5-1), and counterweight (10) is contained on the pallet (9), and first fixed charge method end plate (5-1) is provided with stay cord and passes hole (5-1-1); One end of stay cord (8) and pallet (9) are affixed; It is affixed with first portable plate (7-1) that the stay cord that the other end of stay cord (8) is walked around fixed pulley (11) and passed said first fixed charge method end plate (5-1) passes hole (5-1-1), and parallelly connected spring (3) and the glutinous kettle (4) of being provided with between second portable plate (7-2) and the 3rd portable plate (7-3) is fixed with a connecting rod (13) between first portable plate (7-1) and second portable plate (7-2); Strainmeter (12) is arranged between first portable plate (7-1) and second portable plate (7-2), and strainmeter (12) is affixed with first portable plate (7-1).
3. the measurement mechanism of a polymer viscoelastic model; It is characterized in that: the measurement mechanism of said polymer viscoelastic model is the measurement mechanism of quaternary part model, and the measurement mechanism of said quaternary part model comprises base (1), stay cord (8), pallet (9), counterweight (10), fixed pulley (11), dynamometer (2), strainmeter (12), two glutinous kettles (4), two springs (3), two fixed charge method end plates (4), four pull bars (6) and three portable plates (7); Two fixed charge method end plates (5) are respectively first fixed charge method end plate (5-1) and second fixed charge method end plate (5-2), and three portable plates (7) are respectively first portable plate (7-1), second portable plate (7-2) and the 3rd portable plate (7-3);
Two fixed charge method end plates (5) vertically and side by side are fixed on the base (1); Level and rectangular array are fixed with four pull bars (6) between two fixed charge method end plates (5); Form tower structure by four pull bars (6) and two fixed charge method end plates (5); Three portable plates (7) and two fixed charge method end plates (5) laterally arrange and are positioned between two fixed charge method end plates (5); First portable plate (7-1) and the adjacent setting of first fixed charge method end plate (5-1); The 3rd portable plate (7-3) and the adjacent setting of second fixed charge method end plate (5-2), second portable plate (7-2) is arranged between first portable plate (7-1) and the 3rd portable plate (7-3), and each portable plate (7) is gone up with four pull bars (6) opposite position and is provided with four through holes; Four through holes of each portable plate (7) are sleeved on four pull bars (6); Three portable plates (7) are slidingly connected with four pull bars (6), and pallet (9) is arranged on the outside of first fixed charge method end plate (5-1), and fixed pulley (11) is fixed on the lateral surface of first fixed charge method end plate (5-1); Counterweight (10) is contained on the pallet (9); First fixed charge method end plate (5-1) is provided with stay cord and passes hole (5-1-1), and an end of stay cord (8) and pallet (9) are affixed, and it is affixed with dynamometer (2) that the stay cord that the other end of stay cord (8) is walked around fixed pulley (11) and passed said first fixed charge method end plate (5-1) passes hole (5-1-1); Dynamometer (2) is affixed with first portable plate (7-1); Strainmeter (12) is arranged between first portable plate (7-1) and second portable plate (7-2), and strainmeter (12) is affixed with first portable plate (7-1), and the spring (3) in two springs (3) is connected between first portable plate (7-1) and second portable plate (7-2); Glutinous kettle (4) in two glutinous kettles (4) and the spring of residue (3) in two springs (3) are parallel between second portable plate (7-2) and the 3rd portable plate (7-3), and a glutinous kettle of the residue in two glutinous kettles (4) (4) is fixed between the 3rd portable plate (7-3) and second fixed charge method end plate (5-2).
4. measuring method of utilizing the measurement mechanism implementation model component parameters of claim 1,2 and 3 said polymer viscoelastic models, it is characterized in that: said measuring method is accomplished by following steps:
Step 1: let first portable plate (7-1) and the 3rd portable plate (7-3) in the measurement mechanism of Maxwell model produce constant displacement simultaneously, make Maxwell model produce constant deformation ε 0, and the dynamometer (2) of the measurement mechanism through Maxwell model measures the size that Maxwell model is carved stress at a time, draws stress and time relation curve, i.e. stress relaxation curve;
The pallet (9) of the measurement mechanism of past degree Kelvin model is gone up and is added counterweight (10), is equivalent to apply a constant stress σ 0, the strainmeter (12) of the measurement mechanism through the degree Kelvin model is measured the size that the degree Kelvin model is carved strain at a time, draws strain and time relation curve, i.e. creep curve.
According to the stress relaxation formula:
σ = σ 0 e - E η · t - - - ( 1 )
In the formula: the elastic modulus of E-spring;
The viscosity of η-glutinous kettle;
T-action time;
According to the creep formula:
ϵ = ϵ 0 ( 1 - e - E η · t ) - - - ( 2 )
Derive the elastic modulus formula of spring:
E = σ 0 - σ ( t ) ϵ ( t ) - - - ( 3 )
In the formula: the stress of σ (t)-sometime;
The strain of ε (t)-sometime;
The viscosity calculations formula of glutinous kettle:
η = E ( t ) ln σ 0 σ - - - ( 4 )
If the elastic modulus E of the spring in the measurement mechanism of Maxwell model (3) 1, Maxwell model measurement mechanism in the viscosities il of glutinous kettle (4) 1
If the elastic modulus E of the spring in the measurement mechanism of degree Kelvin model (3) 2, the degree Kelvin model measurement mechanism in the viscosities il of glutinous kettle (4) 2
Try to achieve the elastic modulus E of the spring (3) in the measurement mechanism of Maxwell model according to above-mentioned formula (3) 1And the elastic modulus E of the spring (3) in the measurement mechanism of degree Kelvin model 2Try to achieve (4) viscosities il of the glutinous kettle in the measurement mechanism of Maxwell model according to above-mentioned formula (4) 1And the viscosities il of the glutinous kettle (4) in the measurement mechanism of degree Kelvin model 2
Step 2: the pallet (9) of the measurement mechanism of past quaternary part model adds counterweight (10), is equivalent to apply a constant stress σ 0, the strainmeter (12) of the measurement mechanism through said quaternary part model is measured the size of quaternary part model strain, draws strain and time relation curve, i.e. creep curve; Again with the elastic modulus E of the spring (3) in the measurement mechanism of above-mentioned Maxwell model of trying to achieve through calculating 1, the degree Kelvin model measurement mechanism in the elastic modulus E of spring (3) 2, Maxwell model measurement mechanism in (4) viscosities il of glutinous kettle 1And the viscosities il of the glutinous kettle (4) in the measurement mechanism of degree Kelvin model 2In the creep equation of substitution quaternary part mechanical model,
ϵ ( t ) = σ 0 E 1 + σ 0 E 2 ( 1 - e - E 2 η 2 · t ) + σ 0 η 1 t - - - ( 5 )
Substitution different time t obtains the creep curve of a calculating, and with the superimposed contrast of creep curve that creep curve that calculates and mensuration obtain, the result who obtains is that above-mentioned two kinds of creep curves are identical basically.
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CN112485114A (en) * 2020-11-23 2021-03-12 河海大学 Method for predicting ultra-slow creep of concrete
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