CN102564811B - Sulfur hexafluoride gas sampling device - Google Patents

Sulfur hexafluoride gas sampling device Download PDF

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Publication number
CN102564811B
CN102564811B CN 201210002586 CN201210002586A CN102564811B CN 102564811 B CN102564811 B CN 102564811B CN 201210002586 CN201210002586 CN 201210002586 CN 201210002586 A CN201210002586 A CN 201210002586A CN 102564811 B CN102564811 B CN 102564811B
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gas
sampling
hydrogen fluoride
sulfur hexafluoride
fixed seat
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CN102564811A (en
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李建国
汪献忠
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Henan Relations Co Ltd
Henan Relations Electronics Co Ltd
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Henan Relations Co Ltd
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Abstract

The invention discloses a sulfur hexafluoride gas sampling device, comprising a base and a shell which is provided with an external equipment interface and is arranged on the base. A gas washing bottle, a sampling bottle and a multi-way valve with at least four connection openings are arranged in the shell; a hydrogen fluoride gas colorimetric mechanism is arranged outside the shell; the four connection openings of the multi-way valve are respectively connected with the connection opening of the external equipment of the shell, the gas washing bottle, the sampling bottle and the hydrogen fluoride gas colorimetric mechanism through a gas guide pipe; and an operation handle for opening and closing each connection opening of the multi-way valve is externally arranged on the shell. The hydrogen fluoride gas colorimetric mechanism disclosed by the invention has the advantages of compact and reasonable structure, beautiful and elegant appearance, simple and clear operation process, convenience for maintenance, flexibility in use and relatively individual functions, and has functions of carrying out hydrogen fluoride gas colorimetric detection, displaying pressure of a sampled gas on a pressure meter during sampling, assisting in heating in a process of vacuumizing the sampling device and the like. Therefore, the vacuumization is accelerated and residual matters in a container of the sampling device are released completely, so as to achieve a real numerical value which is the same of the numerical value of an original gas when the sampling is carried out.

Description

Sulfur hexafluoride gas sampling device
Technical field
The present invention relates to a kind of gas sample pick-up unit, relate in particular to a kind of sulfur hexafluoride gas sampling device.
Background technology
The stable performance of sulfur hexafluoride (SF6) aerochemistry has good insulation and arc extinction performance, is widely used in the middle of high voltage electric equipment.The parameters such as the kind of the purity of sulfur hexafluoride gas, dew point, micro-water content, decomposition product and content have direct impact to the safe and reliable work of high voltage electric equipment, therefore, the relevant criterion of State Grid's industry such as GB8905-1996 " The guide for processing and measuring SF6 gas in power apparatus ", DL/T639-1997 " sulfur hexafluoride electrical equipment operation, test and maintainer's security protection detailed rules and regulations " all regulation want regularly the sulfur hexafluoride gas in high voltage electric equipment to be taken a sample to detect to analyze.
At present, electrical equipment, gas-holder and the gas storage cylinder etc. that use sulfur hexafluoride gas are taken a sample generally adopt sampling steel cylinder, this sampling steel cylinder is easy entrained air in sampling process, and there is gaseous impurities at inner wall of steel cylinder, will cause sulfur hexafluoride gas sample like this and decompose and secondary pollution, take the laboratory after sampling and analyze the data nature with regard to out of true, have larger error.
Summary of the invention
The present invention is in order to solve weak point of the prior art, the sulfur hexafluoride gas sampling device that provide a kind of and guarantee that sample is undistorted, the functions such as hydrogen fluoride gas detection in collection gas washing, gas sample and gas is melted into a whole.
For solving the problems of the technologies described above, the present invention adopts following technical scheme: sulfur hexafluoride gas sampling device, comprise the housing with external equipment connector that arranges on base and base, be provided with Drexel bottle, sampling jar in described housing and have at least the multiport valve of four connectors, housing is provided with hydrogen fluoride gas colorimetric mechanism outward, four connectors of multiport valve external equipment connector by wireway and housing, Drexel bottle, sampling jar respectively are connected with hydrogen fluoride gas colorimetric mechanism, and housing is provided with the operating grip of each connector keying of control multiport valve outward.
Described hydrogen fluoride gas colorimetric mechanism comprises upper test tube device and the lower test tube device that is fixedly connected with housing, be inserted with the hydrogen fluoride color comparison tube between upper test tube device and lower test tube device, hydrogen fluoride color comparison tube top is provided with the test tube handle that is used in conjunction with upper test tube device.
Described upper test tube device comprises the upper fixed seat with upper vertical through holes and upper horizontal pore, be communicated with a connector and the upper vertical through holes of multiport valve respectively inside and outside the upper horizontal pore of upper fixed seat, the test tube handle is removably connected with upper motion bar by jackscrew, upper motion bar is plugged in the upper vertical through holes of upper fixed seat, be provided with the upper gas passage that is communicated with the upper horizontal pore of upper fixed seat in upper motion bar, upper motion bar is arranged with the 3rd Compress Spring with upper fixed seat top press fit outward;
Described lower test tube device comprises the lower fixed seat with lower vertical through holes and lower horizontal pore, be communicated with Drexel bottle and lower vertical through holes respectively inside and outside the lower horizontal pore of lower fixed seat, be provided with lower motion bar in the lower vertical through holes of lower fixed seat and be positioned at valve inside under lower motion bar, be provided with the lower gas passage that is communicated with the lower horizontal pore of lower fixed seat in lower motion bar, the corresponding setting in vertical section up and down of lower gas passage and upper gas passage, lower motion bar is arranged with the 4th Compress Spring with lower fixed seat top press fit outward.
Described external equipment connector and hydrogen fluoride gas colorimetric mechanism are located at the housing sidepiece, multiport valve is located at the case top inboard, operating grip is located at outside case top, sampling jar is located at housing central authorities, Drexel bottle is the toroidal cavity that forms between inner walls and sampling jar outer wall, and hydrogen fluoride gas colorimetric mechanism lower end is communicated with Drexel bottle.
be provided with pressure vacuum gauge and constant temperature switch in described base, the base plate of base is provided with socket, pressure vacuum gauge is connected with sampling jar by a piezometric tube, be provided with the heating element of tubular between sampling jar outer wall and Drexel bottle inwall, the top board of base is bolted with carrying bolt, the carrying bolt top is provided with the sampling jar pressing plate, be provided with heat-preservation cotton between bottom sampling jar pressing plate and sampling jar, be provided with in heat-preservation cotton be close to sampling jar bottom be used for guarantee to vacuumize or the temperature sensor of Sample ﹠ hold temperature constant state, the constant temperature switch is connected with temperature sensor by wire.
Described housing sidepiece is provided with handle.
Described case top is provided with the check device of control operation handle return.
described check device comprises non-return button and the register pin that protrudes from respectively the housing upper plate, be located at non-return guide pin bushing and the register pin guide pin bushing of upper plate lower surface, be located at split pin under the non-return guide pin bushing and two ends and be fixedly connected on non-return connecting link on non-return button and register pin, the non-return button passes the non-return guide pin bushing and is connected with split pin, the non-return connecting link is between non-return guide pin bushing and split pin, be arranged with the first Compress Spring on the non-return button between non-return connecting link and split pin, the register pin bottom is located in the register pin guide pin bushing, the bottom shutoff of register pin guide pin bushing, be provided with the second Compress Spring between register pin guide pin bushing bottom and register pin bottom surface, the operating grip bottom surface is provided with dial plate, the register pin upper end is provided with the latch bolt that turns clockwise and pass through with dial plate.
Wireway between described multiport valve and hydrogen fluoride gas colorimetric mechanism is provided with throttling valve.
Described multiport valve is the five-way valve with five connectors, and one of them connector shutoff is closed condition.
Adopt technique scheme, have following beneficial effect:
1, the external equipment connector of housing is the unique external connector of this sampler, is used for vacuumizing, the operations such as gas sample and sample gas output detections; Make the operations such as four interfaces of multiport valve open and close to vacuumize successively, hydrogen fluoride test, gas washing, sampling by the rotating operation handle, so just realize the institutional operations such as hydrogen fluoride gas detection, gas washing and gas sample to sulfur hexafluoride gas.
2, operating grip is rotated to hydrogen fluoride test shelves, use the test tube handle that the hydrogen fluoride color comparison tube is arranged between upper test tube device and lower test tube device, can carry out the hydrogen fluoride test jobs, the hydrogen fluoride test jobs is carried out at the realization scene, the exhaust emissions of hydrogen fluoride color comparison tube is in fixing container (Drexel bottle), realize nontoxic discharging, the centralized recovery purified treatment.
3, constant temperature switch and operating grip are used in conjunction with and vacuumize and the hydrogen fluoride test jobs, pressure vacuum gauge is measured the vacuum tightness in sampling jar when vacuumizing, when vacuumizing operation, needing simultaneously to open heating element heats sampling jar and Drexel bottle, carrying bolt and sampling jar top board play good supporting role, heat-preservation cotton plays the effect into the sampling jar insulation, and temperature sensor plays the effect of perception heating element heating-up temperature, realizes vacuumizing or the Sample ﹠ hold temperature constant state.
4, handle is convenient to housing is fetched; Throttling valve plays in the hydrogen fluoride color comparison tube and is filled with the effect that gas keeps constant rate.
5, multiport valve is five-way valve, and one of them connector is standby connector, and shutoff at ordinary times is closed condition, and in the time of other wireway shutoff, this connector can use.
6, check device be for prevent from reversing operating grip is emitted the sample gas in sampling jar or the front sample gas cylinder of taking a sample in enter the air impact sampling quality, check device can when the sample gas that detection is fetched, be pressed non-return button reversing operating grip and directly emit sample gas to the sampling shelves simultaneously.
Compact conformation of the present invention is reasonable, good looking appearance is generous, simple to operate clear, easy to maintenance, use maneuverability, function opposite independent, and provide that the hydrogen fluoride gas color comparison tube detects for oneself, during sampling tensimeter show the pressure of sample gas, the function such as auxiliary heating when sampler is vacuumized, acceleration vacuumizes, thoroughly discharges residuals in the sampler container, reaching the real numerical value the same with Primordial Qi of value during sampling, is a rare sampling and experimental facilities.Each wireway and sampling jar inwall are through special inertia Passivation Treatment, make after processing its to sulfur hexafluoride gas and analyte thereof without compatibility and adsorbability, thereby guaranteed the time of day of sample, significant to the occasion that is not easy at the scene to carry out with chromatogram or mass spectrum the sulfur hexafluoride gas attributional analysis.The gas that is widely used in using in the electrical equipment to use sulfur hexafluoride gas such as isolating switch, transformer, mutual inductor, combined electrical apparatuses is taken a sample and detects, and also is applicable to the gas that stores in sulfur hexafluoride gas steel cylinder and gas-holder is taken a sample and detected.
Description of drawings
Fig. 1 is structural representation of the present invention;
Fig. 2 is A-A cut-open view in the middle of Fig. 1;
Fig. 3 is the left view of Fig. 1;
Fig. 4 is B-B cut-open view in the middle of Fig. 3;
Fig. 5 is the longitudinal sectional view at the external equipment connector place of housing of the present invention;
Fig. 6 is fundamental diagram of the present invention;
Fig. 7 is the structural representation of check device in the middle of the present invention;
Fig. 8 is the right view of Fig. 7;
Fig. 9 is C-C cut-open view in the middle of Fig. 7;
Figure 10 is D-D cut-open view in the middle of Fig. 7;
Figure 11 is the structural representation of the central hydrogen fluoride gas colorimetric of the present invention mechanism.
Embodiment
as Fig. 1~shown in Figure 11, sulfur hexafluoride gas sampling device, comprise the housing with external equipment connector 23 that arranges on base 1 and base 1, be provided with Drexel bottle 4 in housing 3, sampling jar 5 and the multiport valve 6 with five connectors, a connector shutoff of multiport valve 6 is closed condition, housing 3 is outer is provided with hydrogen fluoride gas colorimetric mechanism, a connector of multiport valve 6 is connected with external equipment connector 2 by wireway 7, a connector is connected with Drexel bottle 4 by wireway 8, a connector is connected with sampling jar 5 by wireway 9, a connector place is provided with throttling valve 27, throttling valve 27 is connected with hydrogen fluoride gas colorimetric mechanism by wireway 10, the outer operating grip 11 that is provided with each connector keying of controlling multiport valve 6 of housing 3, housing 3 tops are provided with the check device 28 that prevents operating grip 11 auto-returneds, housing 3 outside portions are provided with handle 29.External equipment connector 2 and hydrogen fluoride gas colorimetric mechanism are located at housing 3 sidepieces, multiport valve 3 is located at housing 3 inside top, operating grip 11 is located at housing 3 top outer, sampling jar 5 is located at housing 3 central authorities, Drexel bottle 4 is an annular closed cavity, between housing 3 and sampling jar 5, hydrogen fluoride gas colorimetric mechanism lower end is communicated with Drexel bottle 4 by a joint short tube 30.
check device 28 comprises non-return button 33 and the register pin 34 that protrudes from respectively housing 3 upper plates 32, be located at non-return guide pin bushing 35 and the register pin guide pin bushing 36 of upper plate 32 lower surfaces, be located at split pin 37 under non-return guide pin bushing 35 and two ends and be fixedly connected on non-return connecting link 38 on non-return button 33 and register pin 34, non-return button 33 passes non-return guide pin bushing 35 and is connected with split pin 37, non-return connecting link 38 is between non-return guide pin bushing 35 and split pin 37, be arranged with the first Compress Spring 39 on non-return button 33 between non-return connecting link 38 and split pin 37, the first Compress Spring 39 plays non-return connecting link 38 is fixed on the boss of non-return button 33, register pin 34 bottoms are located in register pin guide pin bushing 36, the 36 bottom shutoff of register pin guide pin bushing, be provided with the second Compress Spring 40 between register pin guide pin bushing 36 bottoms and register pin 34 bottom surfaces, operating grip 11 bottom surfaces are provided with dial plate 41, register pin 34 upper ends are provided with the latch bolt 42 that turns clockwise and pass through with dial plate 41, latch bolt 42 plays the effect that makes dial plate 41 one-directional rotation, namely can be along the inclined-plane rotation of latch bolt 42 when dial plate 41 clockwise rotates, latch bolt 42 forms with register pin 34 is integrally manufactured.
be provided with pressure vacuum gauge 12 and constant temperature switch 13 in base 1, the base plate 14 of base 1 is provided with socket 15, pressure vacuum gauge 12 is connected with sampling jar 5 by a piezometric tube 16 and communicates, be provided with the heating element 17 of tubular between sampling jar 5 outer walls and Drexel bottle 4 inwalls, heating element 17 is close to the sampling jar outer wall, the top board 18 of base 1 is bolted with carrying bolt 19, carrying bolt 19 tops are provided with sampling jar pressing plate 20, be provided with heat-preservation cotton 21 between sampling jar pressing plate 20 and sampling jar 5 bottoms, be provided with in heat-preservation cotton 21 and be close to sampling jar 5 bottoms and be used for guaranteeing to vacuumize the temperature sensor 22 that keeps temperature constant state and the temperature sensor 31 that is used for guaranteeing the Sample ﹠ hold temperature constant state, constant temperature switch 13 is connected with temperature sensor with temperature sensor 22 by wire respectively and is connected.
Hydrogen fluoride gas colorimetric mechanism comprises upper test tube device 23 and the lower test tube device 24 that is fixedly connected with housing 3, be inserted with hydrogen fluoride color comparison tube 25 between upper test tube device 23 and lower test tube device 24, hydrogen fluoride color comparison tube 25 tops are provided with the test tube handle 26 that is used in conjunction with upper test tube device 23.
Upper test tube device comprises the upper fixed seat 43 with upper vertical through holes and upper horizontal pore 54, be communicated with wireway 10 and upper vertical through holes respectively inside and outside the upper horizontal pore 54 of upper fixed seat 43, test tube handle 26 is removably connected with upper motion bar 45 by jackscrew 44, upper motion bar 45 is plugged in the upper vertical through holes of upper fixed seat 43, be provided with the upper gas passage 46 that is communicated with the upper horizontal pore 54 of upper fixed seat 43 in upper motion bar 45, be arranged with the 3rd Compress Spring 47 with upper fixed seat 43 top press fits outside upper motion bar 45;
lower test tube device comprises the lower fixed seat 48 with lower vertical through holes and lower horizontal pore 53, be communicated with Drexel bottle 4 and lower vertical through holes respectively inside and outside the lower horizontal pore 53 of lower fixed seat 48, be provided with lower motion bar 49 in the lower vertical through holes of lower fixed seat 48 and be positioned at valve inside 50 under lower motion bar 49, be provided with the lower gas passage 51 that is communicated with the lower horizontal pore 53 of lower fixed seat 48 in lower motion bar 49, the corresponding setting in vertical section up and down of lower gas passage 51 and upper gas passage 46, be arranged with the 4th Compress Spring 52 with lower fixed seat 48 top press fits outside lower motion bar 49.
Operating grip 11 has " hydrogen fluoride test shelves ", " gas washing shelves ", " sampling shelves " and " closing shelves " with clockwise setting, constant temperature switch 13 has " chromatogram shelves ", " closing shelves " and " vacuumizing shelves ", temperature sensor 22 is connected with " vacuumizing shelves ", and temperature sensor 31 is connected with " chromatogram shelves ".
Before the sulfur hexafluoride sampling, first vacuumize operation to sampler, should make it connect external power supply when sampler vacuumizes and carry out auxiliary heating.Concrete steps are as follows:
(1), external equipment connector 2 use flexible pipes are connected and lock with the air intake opening of vacuum pump, the assurance impermeability;
(2), take out circumscripted power line, an end inserts in supply socket 15, the other end of sampler and plugs suitable external power supply;
(3), vacuum pump connects suitable power source, start vacuum pump and move to stable;
(4), slowly open the air-inlet of vacuum pump switch, connecting line is vacuumized, check the impermeability of connecting line according to the vacuum tightness situation of change;
(5), constant temperature switch 13 is pulled to " vacuumize shelves ", 17 pairs of sampling jars 5 of heating element and the Drexel bottle 4 in sampler this moment heated;
(6), then operating grip 11 is threaded to " gas washing " shelves, external equipment connector 2, wireway 7, multiport valve 6, wireway 8 and Drexel bottle 4 are communicated with, Drexel bottle 4 is vacuumized, and when approximately certain hour final vacuum degree reached regulation, Drexel bottle 4 vacuumized complete;
(7), again operating grip is revolved 11 to " sampling " shelves, external equipment connector 2, wireway 7, multiport valve 6, wireway 9 and sampling jar 5 are communicated with, sampling jar 5 is vacuumized, when pressure vacuum gauge is shown as authorised pressure, continue again to take out a few minutes to vacuum tightness when dropping to the authorised pressure left and right, sampling jar 5 vacuumize complete, then with operating grip 11 rotation to " closing shelves ", then close vacuum pump;
(8), sampler vacuumizes and external equipment connector 2 should be put dustproof pipe cap after qualified, with sampler surface wiped clean, and sampler is positioned in suitcase;
(9), application of vacuum finishes, and in time fills in the vacuum pumping release, puts into the clip closed condition.
Can carry out the test of hydrogen fluoride gas colorimetric and gas sample operation after vacuumizing operation and completing, concrete steps are:
(1) sample tap of exact connect ion sulfur hexafluoride electrical equipment to the external equipment connector 2 of sampler, guarantees impermeability;
(2), new hydrogen fluoride color comparison tube 25 is carried out opening and cut off processing;
(3), will be the hydrogen fluoride color comparison tube 25 of opening be arranged on test tube device 23 and lower test tube device 24, during installation, the direction of arrow of hydrogen fluoride color comparison tube 25 is down.Hydrogen fluoride color comparison tube 25 is disposable, installs and uses after holding successfully mouthful, and new hydrogen fluoride color comparison tube 25 need be installed when using at every turn at once;
To be put in without an end of arrow in lower gas passage 51 when (4), hydrogen fluoride color comparison tube 25 is installed, a hand is gently pressed downwards, lower motion bar 49 overcomes the elastic force of the 4th spring 52, and lower motion bar 49 lower end unseat the valve cores 50 make lower gas passage 51 be communicated with Drexel bottle 4;
The another hand upwards gently draws test tube handle 26, in drive, motion bar 45 overcomes the elastic force of the 3rd Compress Spring 47, hydrogen fluoride color comparison tube 25 is vertically placed, unclamp again test tube handle 26, hydrogen fluoride color comparison tube 25 arrow ends are put in gas passage 46, then pinching hydrogen fluoride color comparison tube 25 middle part left rotation and right rotation with finger, that it is aligned is straight, makes air-flow guiding arrow outwardly, and hydrogen fluoride color comparison tube 25 installs;
(5), operating grip 11 is threaded to " hydrogen fluoride test shelves ", external equipment connector 2, wireway 7, multiport valve 6, wireway 10 and hydrogen fluoride color comparison tube 25 are communicated with, then slowly open external equipment sample tap valve and sample gas is arranged by getting final product, throttling valve 27 play vacuumize or when taking a sample gas keep the effect of constant rate under certain pressure, timing about a few minutes, namely complete hydrogen fluoride test (do not need to carry out the hydrogen fluoride test as the scene of taking a sample, operating grip 11 directly is threaded to " gas washing shelves " and carries out gas washing and get final product);
(6), with operating grip 11 dextrorotations to " gas washing shelves ", after timing some seconds, complete gas washing (carried out the hydrogen fluoride test as the scene of taking a sample, need not carry out gas washing, can directly handle be threaded to the sampling shelves and carry out sampling operation);
(7), (or after carrying out the hydrogen fluoride test) after gas washing, operating grip 11 is threaded to " sampling shelves ", when the sampler pressure gauge shows that demonstration reading with sampled electrical equipment pressure gauge is identical, 11 dextrorotations of sampler operating grip to " close shelves " position, are then closed sampling air intake valve on electrical equipment, removed the sampling inlet pipe connection;
(8), take after sample gas, the sampler external interface to be put dust cap, with sampler surface wiped clean, be positioned in suitcase;
(9), gas sample finishes, with the sampling record card filled in, put into the clip closed condition.
After sampling, carry out laboratory gas sample stratographic analysis step as follows:
(1), be connected and lock by decompressor, the assurance impermeability in the middle of the external equipment connector 2 that will fill sample gas and chromatograph interface;
(2), the socket of sampler 15 connects the 220V power supplys, closed electrical source switch, and constant temperature switch 13 is pulled as for " chromatogram shelves " state;
(3), the chromatograph preheating, approximately about 30 minutes, chromatograph is in normal operating conditions in timing;
(4), press the non-return button 33 of the stratographic analysis indication on sampler, non-return button 33 moves down by the elastic force that non-return connecting link 38 drive register pins 34 overcome the second Compress Spring 40, register pin 34 and latch bolt 42 move down, when latch bolt 42 during lower than the dial plate 41 of operating grip 11 bottom surfaces, register pin 34 no longer stops dial plate 41, so just operating grip 11 can be threaded to counterclockwise " sampling shelves " position, can carry out stratographic analysis;
(5), after the laboratory chromatogram detects and completes, successively sampler constant temperature switch 13 is pulled as for " close shelves ", operating grip 11 dextrorotations to " close shelves ", disconnect the sampler power switch, print and preserve the detection data, close the chromatograph switch at last, stratographic analysis is completed;
(6), stratographic analysis should put pipe cap with the sampler external interface after complete, with sampler surface wiped clean, be positioned in suitcase.
The present invention in use should be noted that following item:
(1), transpassivation of connecting tube, protective treatment between inner each parts of sampler, forbid dust, dirty entering.
(2), keep sampler surface clean, clean and tidy, answer wiped clean after each the use, and in time be put in suitcase.
(3), when sampler is not used, external equipment connector 2 should in time put the sealing and dustproof cap, loads onto used hydrogen fluoride color comparison tube 25 at upper test tube device 23 and lower test tube device 24.
(4), sampler belongs to cleaning apparatus, should note waterproof and dustproof and protection against the tide.
(5), sampler vacuumizes and the external power supply of should pegging graft when carrying out sample complexion analysis of spectrum, notices that constant temperature switch 13 selects shelves, must not mistake and mix up.
(6), sampler for a long time not the clean dry nitrogen of used time application of pure rinsed, and the nitrogen that is filled with the certain pressure clean dry in sampling jar is sealed up for safekeeping.
(7), when being carried out high-pressure sampling, gas-holder or steel cylinder should take care.

Claims (10)

1. sulfur hexafluoride gas sampling device, comprise the housing with external equipment connector that arranges on base and base, it is characterized in that: be provided with Drexel bottle, sampling jar in described housing and have at least the multiport valve of four connectors, housing is provided with hydrogen fluoride gas colorimetric mechanism outward, four connectors of multiport valve external equipment connector by wireway and housing, Drexel bottle, sampling jar respectively are connected with hydrogen fluoride gas colorimetric mechanism, and housing is provided with the operating grip of each connector keying of control multiport valve outward.
2. sulfur hexafluoride gas sampling device according to claim 1, it is characterized in that: described hydrogen fluoride gas colorimetric mechanism comprises upper test tube device and the lower test tube device that is fixedly connected with housing, be inserted with the hydrogen fluoride color comparison tube between upper test tube device and lower test tube device, hydrogen fluoride color comparison tube top is provided with the test tube handle that is used in conjunction with upper test tube device.
3. sulfur hexafluoride gas sampling device according to claim 2, it is characterized in that: described upper test tube device comprises the upper fixed seat with upper vertical through holes and upper horizontal pore, be communicated with a connector and the upper vertical through holes of multiport valve respectively inside and outside the upper horizontal pore of upper fixed seat, the test tube handle is removably connected with upper motion bar by jackscrew, upper motion bar is plugged in the upper vertical through holes of upper fixed seat, be provided with the upper gas passage that is communicated with the upper horizontal pore of upper fixed seat in upper motion bar, upper motion bar is arranged with the 3rd Compress Spring with upper fixed seat top press fit outward,
Described lower test tube device comprises the lower fixed seat with lower vertical through holes and lower horizontal pore, be communicated with Drexel bottle and lower vertical through holes respectively inside and outside the lower horizontal pore of lower fixed seat, be provided with lower motion bar in the lower vertical through holes of lower fixed seat and be positioned at valve inside under lower motion bar, be provided with the lower gas passage that is communicated with the lower horizontal pore of lower fixed seat in lower motion bar, the corresponding setting in vertical section up and down of lower gas passage and upper gas passage, lower motion bar is arranged with the 4th Compress Spring with lower fixed seat top press fit outward.
4. according to claim 1 and 2 or 3 described sulfur hexafluoride gas sampling devices, it is characterized in that: described external equipment connector and hydrogen fluoride gas colorimetric mechanism are located at the housing sidepiece, multiport valve is located at the case top inboard, operating grip is located at outside case top, sampling jar is located at housing central authorities, Drexel bottle is the toroidal cavity that forms between inner walls and sampling jar outer wall, and hydrogen fluoride gas colorimetric mechanism lower end is communicated with Drexel bottle.
5. according to claim 1 and 2 or 3 described sulfur hexafluoride gas sampling devices, it is characterized in that: be provided with pressure vacuum gauge and constant temperature switch in described base, the base plate of base is provided with socket, pressure vacuum gauge is connected with sampling jar by a piezometric tube, be provided with the heating element of tubular between sampling jar outer wall and Drexel bottle inwall, the top board of base is bolted with carrying bolt, the carrying bolt top is provided with the sampling jar pressing plate, be provided with heat-preservation cotton between bottom sampling jar pressing plate and sampling jar, be provided with in heat-preservation cotton be close to sampling jar bottom be used for guarantee to vacuumize or the temperature sensor of Sample ﹠ hold temperature constant state, the constant temperature switch is connected with temperature sensor by wire.
6. according to claim 1 and 2 or 3 described sulfur hexafluoride gas sampling devices, it is characterized in that: described housing sidepiece is provided with handle.
7. according to claim 1 and 2 or 3 described sulfur hexafluoride gas sampling devices, it is characterized in that: described case top is provided with the check device of control operation handle return.
8. sulfur hexafluoride gas sampling device according to claim 7, it is characterized in that: described check device comprises non-return button and the register pin that protrudes from respectively the housing upper plate, be located at non-return guide pin bushing and the register pin guide pin bushing of upper plate lower surface, be located at split pin under the non-return guide pin bushing and two ends and be fixedly connected on non-return connecting link on non-return button and register pin, the non-return button passes the non-return guide pin bushing and is connected with split pin, the non-return connecting link is between non-return guide pin bushing and split pin, be arranged with the first Compress Spring on the non-return button between non-return connecting link and split pin, the register pin bottom is located in the register pin guide pin bushing, the bottom shutoff of register pin guide pin bushing, be provided with the second Compress Spring between register pin guide pin bushing bottom and register pin bottom surface, the operating grip bottom surface is provided with dial plate, the register pin upper end is provided with the latch bolt that turns clockwise and match with dial plate.
9. according to claim 1 and 2 or 3 described sulfur hexafluoride gas sampling devices is characterized in that: the wireway between described multiport valve and hydrogen fluoride gas colorimetric mechanism is provided with throttling valve.
10. according to claim 1 and 2 or 3 described sulfur hexafluoride gas sampling devices, it is characterized in that: described multiport valve is the five-way valve with five connectors, one of them connector shutoff is closed condition.
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