CN102526278B - Health-care product used for relaxing tendon, activating collaterals and alleviating athletic fatigue and preparation method thereof - Google Patents
Health-care product used for relaxing tendon, activating collaterals and alleviating athletic fatigue and preparation method thereof Download PDFInfo
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Abstract
The invention provides a health-care product used for relaxing tendon, activating collaterals and alleviating athletic fatigue and a preparation method thereof. The health-care product is prepared from glabrous sarcandra herb, uncaria, cinnamon, monkshood, fissistigma oldhamii and pomoben. The health-care product has the efficacy on alleviating athletic fatigue, pain in the back and waist, sore muscle and shoulder strain, accelerating blood circulation and the like, and can alleviate the symptoms of body fatigue and sore muscle brought by supermotility, and improves the symptoms of pain in the back and waist because of rheumatism arthritis, pain caused by unsmooth blood and influenza and the like.
Description
Technical field:
The present invention relates to a kind of health product for relaxing muscles and tendons and activating QI and blood in the collateral, relieving sports fatigue and preparation method thereof, belong to the technical field of health product.
Background technology:
The pathogens such as wind and cold is wet are easily invaded human body a little less than the human body deficiency of defensive qi time and are caused a disease.Exposure to wind when sweating, sitting and lying wetland, paddle in spite of the rain etc., all can make the pathogens such as wind and cold is wet invade the body meridians, stay in joint, cause passages through which vital energy circulates QI and blood impatency obstructed, stagnation of QI and blood may bring about pain.The reason of aching of the joint that rheumatic arthritis, exercise fatigue, anemofrigid cold cause and muscle is all to cause because human body suffers rheumatism and arthritis invasion and attack that blood vessels are obstructed, meridians are not smooth.Rheumatic arthritis shows as the limb arthralgia clinically, joint is bent and stretched and is obstructed, and myalgia is met cold hot the alleviating of increasing the weight of, obtain; Usually can produce fatigue after hyperkinesia, the sense of discomfort such as health can produce that myalgia, muscle rigidity, human body are tired, the soft soreness of waist of lower limb, lower limb are heavy; Anemofrigid cold clinically showing as that head-body-pain, podomere are miserable more, coldness of the body, thirsty etc.The joint that shows due to above three kinds of diseases and the pathogenesis of muscular soreness are consistent, for this reason, the invention provides a kind of health product for relaxing muscles and tendons and activating QI and blood in the collateral, relieving sports fatigue, mainly contain effects such as improving sore waist and aching in the waist and the back, muscular soreness, shoulder strain, can be used for the crowds such as hyperkinesia, journey fatigue, Common Cold, insomnia are weak, rheumatism strain.
Summary of the invention:
Technical problem to be solved by this invention is to provide a kind of health product for relaxing muscles and tendons and activating QI and blood in the collateral, relieving sports fatigue and preparation method thereof, and this health product has the effects such as relieving sports fatigue, sore waist and aching in the waist and the back, muscular soreness, shoulder strain, blood circulation promoting.
For solving the problems of the technologies described above, the present invention realizes by the following technical solutions:
A kind of health product for relaxing muscles and tendons and activating QI and blood in the collateral, relieving sports fatigue, calculate according to composition by weight, by following effective ingredient, made: Herba Pileae Scriptae 5-20 part, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil. 5-20 part, Gui Liang 5-20 part, the beautiful 5-20 part of Caulis Akebiae, anvil 5-20 part and mother-in-law are to 5-20 part.
Preferably, aforementioned health product for relaxing muscles and tendons and activating QI and blood in the collateral, relieving sports fatigue, calculate according to composition by weight, by following effective ingredient, made: 15 parts of Herba Pileae Scriptaes, 15 parts of Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil., 15 parts of Gui Liang, U.S. 15 parts of Caulis Akebiae, 15 parts of anvils and mother-in-law do not run quickly 15 parts.
The preparation method of aforesaid health product for relaxing muscles and tendons and activating QI and blood in the collateral, relieving sports fatigue is: proportionally take Herba Pileae Scriptae, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil., Gui Liang, Caulis Akebiae U.S., anvil and mother-in-law and do not run quickly, or with corresponding adjuvant, make up, and according to certain preparation method, process, make corresponding external preparation.
Described external preparation is extractum, lotion, tincture or aerosol.
The preparation method of described extractum is: take in proportion that Herba Pileae Scriptae, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil., Gui Liang, Caulis Akebiae are beautiful, anvil and mother-in-law do not run quickly, get Gui Liang, Herba Pileae Scriptae two flavors extract respectively volatile oil, collect volatile oil, and are standby; Residue and all the other 4 herbal medicines merge, and add 4-10 times of water gaging, soak 0.5-2h, decoct each 1-3h 1-3 time, collecting decoction, filter, and it is the extractum of 1.10-1.30 that filtrate is concentrated into relative density under room temperature, adds above-mentioned volatile oil, mix homogeneously, obtain extractum, packing, sterilizing, obtain.
The preparation method of described lotion is: takes in proportion that Herba Pileae Scriptae, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil., Gui Liang, Caulis Akebiae are beautiful, anvil and mother-in-law do not run quickly, gets Herba Pileae Scriptae, Gui Liang extracts volatile oil, and collection volatile oil, medicinal residues are standby; Residue and all the other 4 herbal medicines merge, and add 4-10 times of water gaging, soak 0.5-2h, decoct 1-3 time, each 1-3h, collecting decoction, filter, it is 1.10-1.15 that filtrate is condensed into relative density, add 95% ethanol to make pure content reach 60-70%, standing 24-48h, filter, reclaim ethanol to without the alcohol flavor, obtain extracting solution; Above-mentioned volatile oil is mixed with extracting solution, add the Tween 80 of amount of preparation 0.1-1% to stir evenly, add distillate to ormal weight, packing, sterilizing, obtain.
the preparation method of described aerosol is: take in proportion that Herba Pileae Scriptae, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil., Gui Liang, Caulis Akebiae are beautiful, anvil and mother-in-law do not run quickly, get Gui Liang, Herba Pileae Scriptae two flavor medicines extract respectively volatile oil, collect volatile oil, and are standby, medicinal residues and all the other 4 herbal medicines merge, add 4-10 times of water gaging, soak 0.5-2h, decoct 1-3 time, each 1-3h, collecting decoction, filter, it is the fluid extract of 1.10-1.15 that filtrate is concentrated into relative density under room temperature, add appropriate amount of ethanol, make pure content reach 70%, placed 24 hours in room temperature, filter, reclaim ethanol to without alcohol, distinguishing the flavor of, 70% ethanol that adds 6 times of amounts of solution after reclaiming, placed 24 hours in room temperature, filter, filtrate adds above-mentioned volatile oil, mix homogeneously, obtain semi-finished product solution, semi-finished product solution is filled into medicine bottle, sealing, be pressed into propellant, packing, get product.
The method that aforementioned Herba Pileae Scriptae extracts volatile oil is supercritical extraction or steam distillation; Described supercritical extraction is: gets Herba Pileae Scriptae, uses supercritical fluid extraction volatile oil, and extracting pressure 15-30Mpa, temperature 30-40 ℃, extraction time 1-5h, obtain; Described steam distillation is: get Herba Pileae Scriptae, put into extractor and adopt vapor distillation to extract 2-5h, collect condensed fluid, standing and demixing, isolate volatile oil, obtains.
The method of the bright extraction volatile oil in aforementioned osmanthus is supercritical extraction or steam distillation; Described supercritical extraction is: gets Gui Liang, uses supercritical fluid extraction volatile oil, and extracting pressure 20-45Mpa, temperature 20-40 ℃, extraction time 1-5h, obtain; Described steam distillation is: get Gui Liang, put into extractor and adopt vapor distillation to extract 3-5h, collect condensed fluid, standing and demixing, isolate volatile oil, obtains.
The preparation method of described tincture is: take in proportion Herba Pileae Scriptae, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil., Gui Liang, Caulis Akebiae U.S., anvil and mother-in-law and do not run quickly, get the water soaking 0.5-3h that above 6 flavors add 8-12 doubly to measure, decoct 1-3 time, decoct 0.5-3h at every turn, filter, filtrate merges, and is condensed into the fluid extract that relative density is 1.10-1.15, gets fluid extract and adds 4-6 and doubly measure 60% ethanol dilution, after mixing, standing, filter, obtain.
Prescription foundation with health product of relaxing muscles and tendons and activating QI and blood in the collateral, relieving sports fatigue of the present invention is: take the wind of precious jade medicine, arrange opinion as basis, precious jade doctor is famous instruction early: " non-wind is not enough to transfer and grows; non-beat be not enough to quick-fried ", wind is beaten phase 5, just brave and cloudy gentle product are harmonious, can roll over it and attack the power of pursuing, it is attacked and not fast, eliminating evilly just not hinder again; Cloudy gentle product are equipped with just brave product, can delay that its power is mended and to make it effect lasting, are to close and the imbody of the principles of formulating prescriptions of going after profit or gain.The present invention adopts precious jade medicine Herba Pileae Scriptae, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil., Gui Liang, Caulis Akebiae U.S., anvil and mother-in-law to run quickly and process.Wherein, Herba Pileae Scriptae, (source: the Herb of golden chestnut orchid Herba Pileae Scriptae Sarcandra glabra (Thunb.) Nakai); Mildly bitter flavor, property are put down, heat-clearing and toxic substances removing, promoting blood circulation to remove blood stasis, expelling wind and removing dampness, reducing swelling and alleviating pain.The mother-in-law does not run quickly, and has another name called mother-in-law not bright tight (source: root, root bark and the bark of Araliaceae Kalopanax septemlobum Kalopanax setemLobus (Thunb.) Koidz.); Its acrid in the mouth, property is flat, expelling wind and removing dampness, blood circulation promoting and blood stasis dispelling, relaxing muscles and tendons and activating QI and blood in the collateral, reducing swelling and alleviating pain, evacuation of pus granulation promoting.Gui Liang, (source: bark, twig, the fruit of canella Cortex Cinnamomi Cinnamomum cassia Presl); Its acrid in the mouth, warm in nature, have warming middle-JIAO YANG invigorating, dispersing cold for relieving pain, qualcomm meridian, except arthralgia chiefly caused by damp pathogen, Herba Pileae Scriptae, mother-in-law do not run quickly and Gui Liangjun belongs to wind class medicine in the precious jade medicine.Anvil, (source: the root of the plant Radix Fissistigmatis Oldhamii Fissistigma oldhamii of Fructus Lycopersici esculenti branch section (Hemsl.) Merr); Acrid in the mouth, little puckery, warm in nature, expelling wind and activating blood circulation, reducing swelling and alleviating pain, bone and muscle strengthening.Caulis Akebiae is beautiful, (source: stem, the fruit of plants of Lardizabalaceae Caulis Akebiae Akebia quinata (Thunb.) Decne.); Bitter in the mouth, cold in nature, detoxifcation diuresis, promoting blood circulation and stopping pain, dehumidifying.Anvil and Caulis Akebiae U.S.A all belong to sprays the class medicine in the precious jade medicine.Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil., (source: the stem and branch with belt hook of Maguireothamnus speciosus Ramulus Uncariae Cum Uncis Uncaria rhynchophylla (Miq.) Miq.ex Havil.); Sweet in the mouth, hardship, cold nature, the heat clearing away suppressing the hyperactive liver, relieve dizziness, high fever, infantile convulsions, epilepsy, etc. and determine convulsion, blood pressure lowering, and the wind that belongs in the precious jade medicine is sprayed the medicine of holding concurrently mutually.Its all medicine wind is beaten phase 5, has the function of soothing the channels and quicking the network vessels, adopts the mode of external bathing to use, and is with health role to rheumatic ostalgia, sore waist and aching in the waist and the back, muscular soreness, shoulder strain etc.; The gentle slow property of wind medicine and the fiery and forthright property compatibility of laxative, when expelling pathogenetic factors and reinforcing antipathogenetic qi, also can reduce the pessimal stimulation of bias of medicine to body simultaneously, reduces side reaction.Above precious jade medicine is combined, and is applicable to the crowds such as hyperkinesia, journey fatigue, Common Cold, rheumatism strain, insomnia be weak.
The applicant has carried out following experiment, and provable the present invention has useful effect:
Experimental example: precious jade medicine extractum of the present invention is alleviated the experimentation of the symptoms such as sore waist and aching in the waist and the back, poor blood circulation, muscular soreness
1. data enters to choose: the routine experimenter of this group 70, age 20-60 year; Random packet, employing parallel control, double blinding are observed, and select the crowd who meets inclusive criteria to observe.In accordance with randomizing scheme, lead the order of sequencing and the sample number into spectrum of sample according to every end user, offer every sample that uses same label, enter at random group.
2. be selected in foundation:
The symptoms such as the sore waist and aching in the waist and the back that shows because of rheumatism and arthritis, exercise fatigue, anemofrigid cold etc., muscular soreness, shoulder strain, poor blood circulation.
3. using method:
(1) matched group
Use " relaxing muscles and tendons and activating QI and blood in the collateral type " precious jade to bathe medicated powder; Take a shower once every day, and each 10-30min, used 30 days.(annotate: " relaxing muscles and tendons and activating QI and blood in the collateral type " is the bath agent that forms with 38 flavor medical herbs such as Herba Pileae Scriptae, nine Ns of rattans, Vernonia parishii Hook. F., soft muscle rattans; , muscular soreness smooth for cervical vertebra, lumbar vertebra strain, rheumatism, rheumatoid, sore waist and aching in the waist and the back, circulation, have the effect of relaxing muscles and tendons and activating QI and blood in the collateral, blood circulation promoting and blood stasis dispelling, blood circulation promoting, anti-inflammatory analgetic, and king of medicine paddy health industry Hong Kong Industrial Co., Ltd. produces)
(2) precious jade medicine extractum group of the present invention
Use precious jade medicine extractum of the present invention, according to the described method preparation of embodiment 1; Take a shower once every day, and each 10-30min, used 30 days.
4. result:
Criterion: produce effects: all characterize and disappear or the main disappearance.Effectively: main is clearly better.Invalid: before and after using, the contrast each side is all without progressive.
Result: in matched group 35 examples, produce effects 5 examples, account for 14.3%; Effective 18 examples, account for 51.4%; Invalid 12 examples, account for 34.3%, and total effective rate is 65.7%.In precious jade medicine extractum group of the present invention 35 examples, produce effects 7 examples, account for 20%; Effective 24 examples, account for 68.6%; Invalid 4 examples, account for 11.4%.Total effective rate is 88.6%.Two groups of effects relatively have significant difference (P＜0.05).
5. conclusion: result of study shows that precious jade medicine extractum of the present invention has the effects such as the sore waist and aching in the waist and the back of alleviation, muscular soreness, shoulder strain, blood circulation promoting.
Compared with prior art, health product of the present invention has the effects such as the sore waist and aching in the waist and the back of alleviation, muscular soreness, shoulder strain, blood circulation promoting; The energy alleviation, because the health that hyperkinesia brings is weak, muscular soreness, improves the sore waist and aching in the waist and the back that is caused by rheumatism, and the symptoms such as pain that the pain that blood does not freely cause and flu cause, reached goal of the invention.
Further illustrate by the following examples the present invention, but not as limitation of the present invention
The specific embodiment
Embodiment 1:
Prescription: Herba Pileae Scriptae 15g, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil. 15g, Gui Liang 15g, Caulis Akebiae beautiful 15g, anvil 15g, mother-in-law are to 15g.
Preparation technology: the preparation method of described extractum is: take in proportion Herba Pileae Scriptae, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil., Gui Liang, Caulis Akebiae U.S., anvil and mother-in-law and do not run quickly, get Herba Pileae Scriptae, use supercritical fluid extraction volatile oil, extracting pressure 25Mpa, 35 ℃ of temperature, extraction time 3h, obtain oily liquids, residue is standby; Get Gui Liang, use supercritical fluid extraction volatile oil, extracting pressure 30Mpa, 30 ℃ of temperature, extraction time 2.5h, obtain oily liquids, and residue is standby; Above-mentioned medicinal residues and all the other 4 herbal medicines merge, and add 8 times of water gagings, soak 1h, decoct 3h, filter, then add 6 times of water gagings to decoct 2h, filter, then add 4 times of water gagings to decoct 1h, filter, filtrate merges, and being concentrated into relative density under room temperature is the extractum of 1.10-1.30, adds above-mentioned volatile oil, mix homogeneously, obtain extractum, packing, sterilizing, obtain.
Using method: bathing method: add the suitable hot water of temperature in bathtub or bath bucket, water level transfers to be sitting in bathtub or bath bucket and arrives chest locations (about 150L～180L), get packaged precious jade medicine extractum approximately 40g (33ml) add in hot water, gently stirring (also can be according to the personal considerations to leaching rear bathing 20～30min fully, the appropriate amount of water of adjusting, and the amount of pressing corresponding proportion increase and reduction precious jade medicine extractum), continuous three times is a course for the treatment of, and every 2-5 days once.
Embodiment 2:
Prescription: Herba Pileae Scriptae 20g, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil. 5g,, Gui Liang 20g, Caulis Akebiae beautiful 20g, anvil 5g, the mother-in-law 5g that runs quickly.
Preparation technology: the preparation method of described extractum is: take in proportion Herba Pileae Scriptae, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil., Gui Liang, Caulis Akebiae U.S., anvil and mother-in-law and do not run quickly, get Herba Pileae Scriptae, use supercritical fluid extraction volatile oil, extracting pressure 30Mpa, 40 ℃ of temperature, extraction time 1h, obtain oily liquids, residue is standby; Get Gui Liang, use supercritical fluid extraction volatile oil, extracting pressure 20Mpa, 40 ℃ of temperature, extraction time 1h, obtain oily liquids, and residue is standby; Above-mentioned medicinal residues and all the other 4 herbal medicines merge, and add 8 times of water gagings, soak 0.5h, decoct each 2h 2 times, collecting decoction, filter, and it is the extractum of 1.10-1.30 that filtrate is concentrated into relative density under room temperature, adds above-mentioned volatile oil, mix homogeneously, obtain extractum, packing, sterilizing, obtain.
Using method: wine is treated the bathing method: add the suitable hot water of temperature in bathtub or bath bucket, water level transfers to be sitting in bathtub or bath bucket and arrives chest locations (about 150L～180L), in getting tail wine 1L-2L and precious jade medicine extractum approximately 20g (17ml) putting hot water, gently stirring (also can be according to the personal considerations to leaching rear bathing 20～30min fully, the appropriate amount of water of adjusting, and the amount of pressing corresponding proportion increase and reduction precious jade medicine extractum), continuous three times is a course for the treatment of, and every 2-5 days once.
Embodiment 3:
Prescription: Herba Pileae Scriptae 5g, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil. 20g, Gui Liang 5g, Caulis Akebiae beautiful 5g, anvil 20g, mother-in-law are to 20g.
Preparation technology: the preparation method of described extractum is: take in proportion Herba Pileae Scriptae, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil., Gui Liang, Caulis Akebiae U.S., anvil and mother-in-law and do not run quickly, get Herba Pileae Scriptae, put into extractor and adopt vapor distillation to extract 3h, collect condensed fluid, standing and demixing, isolate volatile oil, and residue is standby; Get Gui Liang, put into extractor and adopt vapor distillation to extract 4h, collect condensed fluid, standing and demixing, isolate volatile oil, and residue is standby; Above-mentioned medicinal residues and all the other 4 herbal medicines merge, and add 10 times of water gagings, soak 2h, decoct 3h, and decocting liquid filters, and it is the extractum of 1.10-1.30 that filtrate is concentrated into relative density under room temperature, adds above-mentioned volatile oil, and mix homogeneously, obtain extractum, and packing is sterilizing, obtains.
Using method: foot bath method: get packaged precious jade medicine extractum approximately 10g (8ml) put into basin, add warm water, gently stir to leaching rear foot bath and lower limb fully, once a day, each 20-30min.
Embodiment 4:
Prescription: Herba Pileae Scriptae 18g, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil. 15g, Gui Liang 5g, Caulis Akebiae beautiful 20g, anvil 10g, mother-in-law are to 10g.
Preparation technology: the preparation method of described tincture is: take in proportion that Herba Pileae Scriptae, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil., Gui Liang, Caulis Akebiae are beautiful, anvil and mother-in-law do not run quickly, decoct 3h after getting the water soaking 1h that above 6 flavors add 12 times of amounts, filter, filtrate for later use, then add the decocting of 8 times of amounts to boil 2 times, each 0.5h, filter, filtrate merges, and is condensed into the fluid extract that relative density is 1.10-1.15, gets fluid extract and adds 5 times of amount 60% ethanol dilutions, after mixing, standing, filter, obtain.
Using method: get to be coated with in right amount and put the place of aching on the skin, every day 3～5 times.
Embodiment 5:
Prescription: Herba Pileae Scriptae 20g, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil. 20g, Gui Liang 5g, Caulis Akebiae beautiful 15g, anvil 15g, mother-in-law are to 15g.
Preparation technology: the preparation method of described tincture is: take in proportion that Herba Pileae Scriptae, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil., Gui Liang, Caulis Akebiae are beautiful, anvil and mother-in-law do not run quickly, decoct 3h after getting the water soaking 3h that above 6 flavors add 10 times of amounts, filter, filtrate for later use, add the decocting of 8 times of amounts to boil 2h again, filter, filtrate merges, be condensed into the fluid extract that relative density is 1.10-1.15, get fluid extract and add 6 times of amount 60% ethanol dilutions, after mixing, standing, filter, obtain.
Using method: get to be coated with in right amount and put the place of aching on the skin, every day 3～5 times.
Embodiment 6:
Prescription: Herba Pileae Scriptae 8g, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil. 10g, Gui Liang 10g, Caulis Akebiae beautiful 12g, anvil 8g, mother-in-law are to 8g.
Preparation technology: the preparation method of described tincture is: take in proportion Herba Pileae Scriptae, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil., Gui Liang, Caulis Akebiae U.S., anvil and mother-in-law and do not run quickly, get after above 6 flavors add the water soaking 0.5h of 8 times of amounts and decoct 3h, filter, filtrate is condensed into the fluid extract that relative density is 1.10-1.15, get fluid extract and add 4 times of amount 60% ethanol dilutions, after mixing, standing, filter, obtain.
Using method: get to be coated with in right amount and put on the skin in the place of aching, every day 3～5 times.
Embodiment 7:
Prescription: Herba Pileae Scriptae 10g, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil. 12g, Gui Liang 15g, Caulis Akebiae beautiful 20g, anvil 15g, mother-in-law are to 10g.
preparation technology: the preparation method of described aerosol is: take in proportion Herba Pileae Scriptae, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil., Gui Liang, Caulis Akebiae U.S., anvil and mother-in-law and do not run quickly, get Herba Pileae Scriptae, put into extractor and adopt vapor distillation to extract 5h, collect condensed fluid, standing and demixing, isolate volatile oil, and residue is standby, get Gui Liang, use supercritical fluid extraction volatile oil, extracting pressure 45Mpa, 20 ℃ of temperature, extraction time 5h, obtain oily liquids, and residue is standby, medicinal residues and all the other 4 herbal medicines merge, add 10 times of water gagings, soak 2h, decoct 3h, filter, add again 8 times of water gagings to decoct 2h, filter, add again 4 times of water gagings to decoct 1h, filter, filtrate merges, being concentrated into relative density under room temperature is the fluid extract of 1.10-1.15, add appropriate amount of ethanol, make pure content reach 70%, placed 24 hours in room temperature, filter, reclaim ethanol to without alcohol, distinguishing the flavor of, 70% ethanol that adds 6 times of amounts of solution after reclaiming, placed 24 hours in room temperature, filter, filtrate adds above-mentioned volatile oil, mix homogeneously, obtain semi-finished product solution, semi-finished product solution is filled into medicine bottle, sealing, be pressed into propellant, packing, get product.
Using method: be sprayed on the place of aching, every day 3～5 times.
Embodiment 8:
Prescription: Herba Pileae Scriptae 10g, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil. 10g, Gui Liang 10g, Caulis Akebiae beautiful 10g, anvil 10g, mother-in-law are to 10g.
Preparation technology: the preparation method of described aerosol is: take in proportion Herba Pileae Scriptae, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil., Gui Liang, Caulis Akebiae U.S., anvil and mother-in-law and do not run quickly, get Herba Pileae Scriptae, use supercritical fluid extraction volatile oil, extracting pressure 15Mpa, 30 ℃ of temperature, extraction time 5h, obtain oily liquids, residue is standby; Get Gui Liang, put into extractor and adopt vapor distillation to extract 5h, collect condensed fluid, standing and demixing, isolate volatile oil, and residue is standby; Residue and all the other 4 herbal medicines merge, and add 8 times of water gagings, soak 0.5h, decoct 3h, decocting liquid filters, and it is the fluid extract of 1.10-1.15 that filtrate is concentrated into relative density under room temperature, add appropriate amount of ethanol, make pure content reach 70%, in room temperature, placed 24 hours, filter, reclaim ethanol to without alcohol, distinguishing the flavor of, add 70% ethanol of 6 times of amounts of solution after reclaiming, in room temperature, placed 24 hours, filter, filtrate adds above-mentioned volatile oil, mix homogeneously, obtain semi-finished product solution, and semi-finished product solution is filled into medicine bottle, sealing, be pressed into propellant, packing, get product.
Using method: be sprayed on the place of aching, every day 3～5 times.
Embodiment 9:
Prescription: Herba Pileae Scriptae 15g, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil. 10g, Gui Liang 10g, Caulis Akebiae beautiful 5g, anvil 15g, mother-in-law are to 20g.
Preparation technology: the preparation method of described lotion is: take in proportion Herba Pileae Scriptae, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil., Gui Liang, Caulis Akebiae U.S., anvil and mother-in-law and do not run quickly, getting Herba Pileae Scriptae, Gui Liang puts into extractor and adopts vapor distillation to extract 3h, collect condensed fluid, standing and demixing, isolate volatile oil, collect volatile oil, medicinal residues are standby; Residue and all the other 4 herbal medicines merge, and add 10 times of water gagings, soak 2h, decoct 3h, filter, then add 8 times of water gagings to decoct 2h, filter, then add 4 times of water gagings to decoct 1h, filter, filtrate merges, and being condensed into relative density is 1.10-1.15, adds 95% ethanol to make pure content reach 70%, standing 48h, filter, reclaim ethanol to without the alcohol flavor, obtain extracting solution; Above-mentioned volatile oil is mixed with extracting solution, add the Tween 80 of amount of preparation 1% to stir evenly, add distillate to ormal weight, packing, sterilizing, obtain.
Using method: get this product and pour in right amount in basin, add warm water to preference temperature, foot bath and lower limb, once a day, each 20-30min.
Embodiment 10:
Prescription: Herba Pileae Scriptae 10g, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil. 10g, Gui Liang 5g, Caulis Akebiae beautiful 15g, anvil 15g, mother-in-law are to 10g.
Preparation technology: the preparation method of described lotion is: take in proportion Herba Pileae Scriptae, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil., Gui Liang, Caulis Akebiae U.S., anvil and mother-in-law and do not run quickly, get Herba Pileae Scriptae, put into extractor and adopt vapor distillation to extract 3h, collect condensed fluid, standing and demixing, isolate volatile oil, and residue is standby; Get Gui Liang, put into extractor and adopt vapor distillation to extract 4h, collect condensed fluid, standing and demixing, isolate volatile oil, and residue is standby; Residue and all the other 4 herbal medicines merge, and add 8 times of water gagings, soak 0.5h, decoct each 1.5h 2 times, collecting decoction, filter, and it is 1.10-1.15 that filtrate is condensed into relative density, adds 95% ethanol to make pure content reach 60%, standing 24h, filter, and reclaims ethanol to without the alcohol flavor, obtains extracting solution; Above-mentioned volatile oil is mixed with extracting solution, add the Tween 80 of amount of preparation 0.1% to stir evenly, add distillate to ormal weight, packing, sterilizing, obtain.
Using method: get this product and pour in right amount in basin, add warm water to preference temperature, foot bath and lower limb, once a day, each 20-30min.
Claims (9)
1. health product that is used for relaxing muscles and tendons and activating QI and blood in the collateral, relieving sports fatigue, it is characterized in that: calculate according to composition by weight, by following effective ingredient, made: 15 parts of Herba Pileae Scriptaes, 15 parts of Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil., 15 parts of Gui Liang, U.S. 15 parts of Caulis Akebiae, 15 parts of anvils and mother-in-law do not run quickly 15 parts.
2. the preparation method for preparing the health product for relaxing muscles and tendons and activating QI and blood in the collateral, relieving sports fatigue claimed in claim 1, it is characterized in that: proportionally take Herba Pileae Scriptae, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil., Gui Liang, Caulis Akebiae U.S., anvil and mother-in-law and do not run quickly, or with corresponding adjuvant, make up, and according to certain preparation method, process, make corresponding external preparation.
3. method according to claim 2, it is characterized in that: described external preparation is extractum, lotion, tincture or aerosol.
4. method according to claim 3, it is characterized in that: the preparation method of described extractum is: take in proportion Herba Pileae Scriptae, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil., Gui Liang, Caulis Akebiae U.S., anvil and mother-in-law and do not run quickly, get Gui Liang, Herba Pileae Scriptae two flavors and extract respectively volatile oil, collect volatile oil, standby; Residue and all the other 4 herbal medicines merge, and add 4-10 times of water gaging, soak 0.5-2h, decoct each 1-3h 1-3 time, collecting decoction, filter, and it is the extractum of 1.10-1.30 that filtrate is concentrated into relative density under room temperature, adds above-mentioned volatile oil, mix homogeneously, packing, sterilizing, obtain extractum.
5. method according to claim 3, it is characterized in that: the preparation method of described lotion is: take in proportion that Herba Pileae Scriptae, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil., Gui Liang, Caulis Akebiae are beautiful, anvil and mother-in-law do not run quickly, get Herba Pileae Scriptae, Gui Liang extracts volatile oil, collection volatile oil, medicinal residues are standby; Residue and all the other 4 herbal medicines merge, and add 4-10 times of water gaging, soak 0.5-2h, decoct 1-3 time, each 1-3h, collecting decoction, filter, it is 1.10-1.15 that filtrate is condensed into relative density, add 95% ethanol to make pure content reach 60-70%, standing 24-48h, filter, reclaim ethanol to without the alcohol flavor, obtain extracting solution; Above-mentioned volatile oil is mixed with extracting solution, add the Tween 80 of amount of preparation 0.1-1% to stir evenly, add distillate to ormal weight, packing, sterilizing, obtain.
6. method according to claim 3, it is characterized in that: the preparation method of described aerosol is: take in proportion Herba Pileae Scriptae, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil., Gui Liang, Caulis Akebiae U.S., anvil and mother-in-law and do not run quickly, get Gui Liang, Herba Pileae Scriptae two flavor medicines and extract respectively volatile oil, collect volatile oil, standby, medicinal residues and all the other 4 herbal medicines merge, add 4-10 times of water gaging, soak 0.5-2h, decoct 1-3 time, each 1-3h, collecting decoction, filter, it is the fluid extract of 1.10-1.15 that filtrate is concentrated into relative density under room temperature, add appropriate amount of ethanol, make pure content reach 70%, placed 24 hours in room temperature, filter, reclaim ethanol to without alcohol, distinguishing the flavor of, 70% ethanol that adds 6 times of amounts of solution after reclaiming, placed 24 hours in room temperature, filter, filtrate adds above-mentioned volatile oil, mix homogeneously, obtain semi-finished product solution, semi-finished product solution is filled into medicine bottle, sealing, be pressed into propellant, packing, get product.
7. the described method of any one according to claim 4-6, it is characterized in that: the method that described Herba Pileae Scriptae extracts volatile oil is supercritical extraction or steam distillation; Described supercritical extraction is: gets Herba Pileae Scriptae, uses supercritical fluid extraction volatile oil, and extracting pressure 15-30Mpa, temperature 30-40 ℃, extraction time 1-5h, obtain; Described steam distillation is: get Herba Pileae Scriptae, put into extractor and adopt vapor distillation to extract 2-5h, collect condensed fluid, standing and demixing, isolate volatile oil, obtains.
8. the described method of any one according to claim 4-6, it is characterized in that: the method for the bright extraction volatile oil in described osmanthus is supercritical extraction or steam distillation; Described supercritical extraction is: gets Gui Liang, uses supercritical fluid extraction volatile oil, and extracting pressure 20-45Mpa, temperature 20-40 ℃, extraction time 1-5h, obtain; Described steam distillation is: get Gui Liang, put into extractor and adopt vapor distillation to extract 3-5h, collect condensed fluid, standing and demixing, isolate volatile oil, obtains.
9. method according to claim 3, it is characterized in that: the preparation method of described tincture is: take in proportion that Herba Pileae Scriptae, Stem and branch with hook of Uncaria rhynchophylla (Miq.) Miq.ex Havil., Gui Liang, Caulis Akebiae are beautiful, anvil and mother-in-law do not run quickly, and gets the water soaking 0.5-3h that above 6 flavors add 8-12 doubly to measure, decoct 1-3 time, each 0.5-3h that decocts, filter, and filtrate merges, be condensed into the fluid extract that relative density is 1.10-1.15, get fluid extract and add 4-6 and doubly measure 60% ethanol dilution, after mixing, standing, filter, obtain.
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1190227C (en) * | 2003-04-04 | 2005-02-23 | 贵州黔东南州安平民族制药有限公司 | External-use Chinese medicine preparation for wind-dispelling and dampness-removing and preparing method thereof |
| CN1951364A (en) * | 2006-11-07 | 2007-04-25 | 金平金岭生物瑶药开发有限责任公司 | A Yao medicinal composition for bath |
| CN1994338A (en) * | 2006-12-14 | 2007-07-11 | 暨南大学 | Novel use of Sarcandra glabra aqueous extract |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| KR101141314B1 (en) * | 2010-06-18 | 2012-05-04 | 한국 한의학 연구원 | Composition for immunopotentiating comprising the extract of herbal formula, Ojeok-san |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1190227C (en) * | 2003-04-04 | 2005-02-23 | 贵州黔东南州安平民族制药有限公司 | External-use Chinese medicine preparation for wind-dispelling and dampness-removing and preparing method thereof |
| CN1951364A (en) * | 2006-11-07 | 2007-04-25 | 金平金岭生物瑶药开发有限责任公司 | A Yao medicinal composition for bath |
| CN1994338A (en) * | 2006-12-14 | 2007-07-11 | 暨南大学 | Novel use of Sarcandra glabra aqueous extract |
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