CN102500265A - Device for saturating two-phase solutions - Google Patents
Device for saturating two-phase solutions Download PDFInfo
- Publication number
- CN102500265A CN102500265A CN2011103169304A CN201110316930A CN102500265A CN 102500265 A CN102500265 A CN 102500265A CN 2011103169304 A CN2011103169304 A CN 2011103169304A CN 201110316930 A CN201110316930 A CN 201110316930A CN 102500265 A CN102500265 A CN 102500265A
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- Prior art keywords
- separatory funnel
- piston
- oscillator
- gabion
- lower carriage
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- Investigating Strength Of Materials By Application Of Mechanical Stress (AREA)
Abstract
The invention relates to a device for saturating two-phase solutions. The device comprises a separating funnel and an oscillator, wherein a plug and a piston of the separating funnel are provided with fixing devices, so that miss of the plug and the piston during vibration are prevented; the outer layer of the oscillator is a metal box; two parallel metal rods of the same height are arranged above the inside of the metal box, and are connected with a metal basket below through pulleys; and a lower bracket for bearing the separating funnel is embedded into the metal basket. When the separating funnel is placed on the lower bracket, an upper bracket is buckled additionally on the lower bracket, and the lower bracket below is connected through a bolt. The device is convenient to use, a large quantity of oil-water phases can be dissolved and saturated at one time by fully oscillating and mixing, and saturated oil-water phases are provided for testing the oil-water distribution coefficient of a substance with a shake-flask method.
Description
Technical field
The present invention relates to a kind of two phase liquid saturated device each other that makes.
Background technology
The profit distribution coefficient of organic compound is an important physicochemical property, with its influence to environment and human health very big correlation is arranged.Fask oscillating method is the method for traditional mensuration material profit distribution coefficient, and it is accurate that it measures the result, is the method for at present the most frequently used mensuration material profit distribution coefficient.
Use the fask oscillating method at first need required oil phase and water is saturated each other, even because two under the very little situation of separately meltage, also can influence the mensuration result.And do not see as yet at present specially to measuring that the profit distribution coefficient designs and the simple and effective profit two mutual saturated devices that make.
Summary of the invention
The present invention provides a kind of each other saturated device of two phase liquid that makes, can be disposable will be more a large amount of profit two mutually fully vibration mix that to make it reach dissolving each other saturated, the profit distribution coefficient of measuring material for fask oscillating method provides profit two phases after saturated.
The technical scheme that the present invention adopts is following:
A kind of two phase liquid saturated device each other that makes comprises separatory funnel and oscillator, and the stopper and the piston of said separatory funnel are provided with fixture, and stopper and piston are left out when preventing to vibrate; The skin of said oscillator is a metal box, and the metal box inner and upper is provided with the Metallic rod that is parallel to each other of two equal heights, and Metallic rod is connected with the gabion of below through pulley, is inlaying the lower carriage that carries separatory funnel in the gabion.
Preferably, adopt fixedly stopper of plastics cutting ferrule.
Preferably, adorn a fixture, open a duct, fixture is connected with piston with a bolt in the knob end and the perpendicular direction of passage of piston on stop,threeway top.
After being put into separatory funnel on the lower carriage, buckling other upper bracket above, and be connected with bolt with following lower carriage.Lower carriage is through being bolted in the gabion.The right side of gabion links to each other with power set.
As required, can hold 1-3 separatory funnel on the support of oscillator.
Oil phase and water used when at present, measuring material profit distribution coefficient generally reach capacity it through the constant temperature oscillator vibration.Adopt constant temperature oscillator earlier profit two to be added in certain container and shake, make it saturated each other, finally must transfer to the separation of carrying out two phases in the separatory funnel.And the device among the present invention has omitted the process with profit two phase transfers, and operation becomes simple, practical.
Description of drawings
Fig. 1 is the sketch map of the separatory funnel that uses in the device of the present invention;
Fig. 2 is the front view and the side view of the oscillation device that uses in the device of the present invention, wherein,
1, pulley; 2, Metallic rod; 3, metal box; 4, upper bracket; 5, control panel; 6, lower carriage; 7, bolt; 8, gabion; 9, stopper; 10, piston
The specific embodiment
A kind of two phase liquid saturated device each other that makes; Comprise separatory funnel and oscillator; The used separatory funnel of this device is that with the difference of used usually separatory funnel the stopper 9 of said separatory funnel is provided with fixture with piston 10; As shown in Figure 1, can prevent coming off of in the process of shaking stopper 9 and piston 10 like this, thereby cause the unrestrained of reagent.Fixedly stopper 9 usefulness is the plastics cutting ferrules.Adorn a fixture on stop,threeway 10 tops, open a duct, with a bolt fixture is connected with piston 10 to make in the piston earthquake process and can not comes off and to rotate at piston 10 knob ends and the perpendicular direction of passage.
Fig. 2 is the front view and the left view of oscillator.Oscillator can be pressed the button of its right side control panel 5 according to actual needs and regulate frequency of oscillation.The skin of said oscillator is a metal box 3, and metal box 3 inner and upper are provided with the Metallic rod that is parallel to each other 2 of two equal heights, and Metallic rod 2 is connected with the gabion 8 of below through four pulleys 1, is inlaying two lower carriages 6 that carry separatory funnel in the gabion 8.Lower carriage 6 is through being bolted in the gabion 8, and lower carriage 6 has the circular arc opening of different-diameter, with the convenient separatory funnel of placing.The right side of gabion 8 links to each other with power set through a Metallic rod.After being put into separatory funnel on the lower carriage 6, buckle two other upper bracket that has circular arc 4 above, and be connected with bolt accordingly with following lower carriage 6, so just can guarantee can not slide in the separatory funnel earthquake process.
Can hold 1-3 separatory funnel on the support of this oscillator, can adjust flexibly according to testing the required oil phase and the amount of water.
After vibration is accomplished, can directly separatory funnel be taken out and be put into standing demix on the iron stand, at last water and oil phase are separated, store for future use.
Claims (7)
1. one kind makes two phase liquid saturated device each other, comprises separatory funnel and oscillator, it is characterized in that stopper of said separatory funnel (9) and piston (10) are provided with fixture, and stopper when preventing to vibrate (9) and piston (10) are left out; The skin of said oscillator is metal box (3); Metal box (3) inner and upper is provided with the Metallic rod that is parallel to each other (2) of two equal heights; Metallic rod (2) is connected with the gabion (8) of below through pulley (1), is inlaying the lower carriage (6) that carries separatory funnel in the gabion (8).
2. device as claimed in claim 1 is characterized in that, adopts fixedly stopper (9) of plastics cutting ferrule.
3. device as claimed in claim 2 is characterized in that, adorns a fixture on stop,threeway (10) top, opens a duct in the knob end and the perpendicular direction of passage of piston (10), with a bolt fixture is connected with piston (10).
4. device as claimed in claim 1 is characterized in that, after being put into separatory funnel on the lower carriage (6), buckling other upper bracket (4) above, and is connected with bolt with following lower carriage (6).
5. device as claimed in claim 4 is characterized in that, lower carriage (6) is through being bolted in the gabion (8).
6. device as claimed in claim 5 is characterized in that, the right side of gabion (8) links to each other with power set.
7. like the arbitrary described device of claim 1-6, it is characterized in that, can hold 1-3 separatory funnel on the support of oscillator.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011103169304A CN102500265A (en) | 2011-10-18 | 2011-10-18 | Device for saturating two-phase solutions |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011103169304A CN102500265A (en) | 2011-10-18 | 2011-10-18 | Device for saturating two-phase solutions |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN102500265A true CN102500265A (en) | 2012-06-20 |
Family
ID=46212432
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2011103169304A Pending CN102500265A (en) | 2011-10-18 | 2011-10-18 | Device for saturating two-phase solutions |
Country Status (1)
| Country | Link |
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| CN (1) | CN102500265A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103076210A (en) * | 2012-10-17 | 2013-05-01 | 中国石油化工股份有限公司 | Pretreatment device and method for determining distribution coefficient of substance in n-octanol / water system |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5478478A (en) * | 1993-12-22 | 1995-12-26 | E. I. Du Pont De Nemours And Company | Apparatus and method for preventing vortexing of a liquid in a separatory funnel |
| CN2469990Y (en) * | 2001-03-23 | 2002-01-09 | 上海智城分析仪器制造有限公司 | Swing-angle adjustable oscillator |
| CN1636627A (en) * | 2003-12-19 | 2005-07-13 | 东京理化器械株式会社 | Separatory funnel support for oscillating machine |
| JP2007271768A (en) * | 2006-03-30 | 2007-10-18 | Casio Electronics Co Ltd | Method for manufacturing electrophotographic color toner |
| CN201394458Y (en) * | 2009-03-20 | 2010-02-03 | 上海理工大学 | Ultrasonic thermostatic water bath vibrator |
-
2011
- 2011-10-18 CN CN2011103169304A patent/CN102500265A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5478478A (en) * | 1993-12-22 | 1995-12-26 | E. I. Du Pont De Nemours And Company | Apparatus and method for preventing vortexing of a liquid in a separatory funnel |
| CN2469990Y (en) * | 2001-03-23 | 2002-01-09 | 上海智城分析仪器制造有限公司 | Swing-angle adjustable oscillator |
| CN1636627A (en) * | 2003-12-19 | 2005-07-13 | 东京理化器械株式会社 | Separatory funnel support for oscillating machine |
| JP2007271768A (en) * | 2006-03-30 | 2007-10-18 | Casio Electronics Co Ltd | Method for manufacturing electrophotographic color toner |
| CN201394458Y (en) * | 2009-03-20 | 2010-02-03 | 上海理工大学 | Ultrasonic thermostatic water bath vibrator |
Non-Patent Citations (1)
| Title |
|---|
| 朱权等: "《化学基础实验实训》", 31 May 2009, article "使用分液漏斗前必须做好哪些检查", pages: 130 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103076210A (en) * | 2012-10-17 | 2013-05-01 | 中国石油化工股份有限公司 | Pretreatment device and method for determining distribution coefficient of substance in n-octanol / water system |
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Application publication date: 20120620 |