CN102500265A - Device for saturating two-phase solutions - Google Patents

Device for saturating two-phase solutions Download PDF

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Publication number
CN102500265A
CN102500265A CN2011103169304A CN201110316930A CN102500265A CN 102500265 A CN102500265 A CN 102500265A CN 2011103169304 A CN2011103169304 A CN 2011103169304A CN 201110316930 A CN201110316930 A CN 201110316930A CN 102500265 A CN102500265 A CN 102500265A
Authority
CN
China
Prior art keywords
separatory funnel
piston
oscillator
gabion
lower carriage
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN2011103169304A
Other languages
Chinese (zh)
Inventor
张宏哲
张帆
董国胜
王慧欣
张金梅
王亚琴
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Petroleum and Chemical Corp
Sinopec Qingdao Safety Engineering Institute
Original Assignee
China Petroleum and Chemical Corp
Sinopec Qingdao Safety Engineering Institute
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China Petroleum and Chemical Corp, Sinopec Qingdao Safety Engineering Institute filed Critical China Petroleum and Chemical Corp
Priority to CN2011103169304A priority Critical patent/CN102500265A/en
Publication of CN102500265A publication Critical patent/CN102500265A/en
Pending legal-status Critical Current

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Abstract

The invention relates to a device for saturating two-phase solutions. The device comprises a separating funnel and an oscillator, wherein a plug and a piston of the separating funnel are provided with fixing devices, so that miss of the plug and the piston during vibration are prevented; the outer layer of the oscillator is a metal box; two parallel metal rods of the same height are arranged above the inside of the metal box, and are connected with a metal basket below through pulleys; and a lower bracket for bearing the separating funnel is embedded into the metal basket. When the separating funnel is placed on the lower bracket, an upper bracket is buckled additionally on the lower bracket, and the lower bracket below is connected through a bolt. The device is convenient to use, a large quantity of oil-water phases can be dissolved and saturated at one time by fully oscillating and mixing, and saturated oil-water phases are provided for testing the oil-water distribution coefficient of a substance with a shake-flask method.

Description

A kind of two phase liquid saturated device each other that makes
Technical field
The present invention relates to a kind of two phase liquid saturated device each other that makes.
Background technology
The profit distribution coefficient of organic compound is an important physicochemical property, with its influence to environment and human health very big correlation is arranged.Fask oscillating method is the method for traditional mensuration material profit distribution coefficient, and it is accurate that it measures the result, is the method for at present the most frequently used mensuration material profit distribution coefficient.
Use the fask oscillating method at first need required oil phase and water is saturated each other, even because two under the very little situation of separately meltage, also can influence the mensuration result.And do not see as yet at present specially to measuring that the profit distribution coefficient designs and the simple and effective profit two mutual saturated devices that make.
Summary of the invention
The present invention provides a kind of each other saturated device of two phase liquid that makes, can be disposable will be more a large amount of profit two mutually fully vibration mix that to make it reach dissolving each other saturated, the profit distribution coefficient of measuring material for fask oscillating method provides profit two phases after saturated.
The technical scheme that the present invention adopts is following:
A kind of two phase liquid saturated device each other that makes comprises separatory funnel and oscillator, and the stopper and the piston of said separatory funnel are provided with fixture, and stopper and piston are left out when preventing to vibrate; The skin of said oscillator is a metal box, and the metal box inner and upper is provided with the Metallic rod that is parallel to each other of two equal heights, and Metallic rod is connected with the gabion of below through pulley, is inlaying the lower carriage that carries separatory funnel in the gabion.
Preferably, adopt fixedly stopper of plastics cutting ferrule.
Preferably, adorn a fixture, open a duct, fixture is connected with piston with a bolt in the knob end and the perpendicular direction of passage of piston on stop,threeway top.
After being put into separatory funnel on the lower carriage, buckling other upper bracket above, and be connected with bolt with following lower carriage.Lower carriage is through being bolted in the gabion.The right side of gabion links to each other with power set.
As required, can hold 1-3 separatory funnel on the support of oscillator.
Oil phase and water used when at present, measuring material profit distribution coefficient generally reach capacity it through the constant temperature oscillator vibration.Adopt constant temperature oscillator earlier profit two to be added in certain container and shake, make it saturated each other, finally must transfer to the separation of carrying out two phases in the separatory funnel.And the device among the present invention has omitted the process with profit two phase transfers, and operation becomes simple, practical.
Description of drawings
Fig. 1 is the sketch map of the separatory funnel that uses in the device of the present invention;
Fig. 2 is the front view and the side view of the oscillation device that uses in the device of the present invention, wherein,
1, pulley; 2, Metallic rod; 3, metal box; 4, upper bracket; 5, control panel; 6, lower carriage; 7, bolt; 8, gabion; 9, stopper; 10, piston
The specific embodiment
A kind of two phase liquid saturated device each other that makes; Comprise separatory funnel and oscillator; The used separatory funnel of this device is that with the difference of used usually separatory funnel the stopper 9 of said separatory funnel is provided with fixture with piston 10; As shown in Figure 1, can prevent coming off of in the process of shaking stopper 9 and piston 10 like this, thereby cause the unrestrained of reagent.Fixedly stopper 9 usefulness is the plastics cutting ferrules.Adorn a fixture on stop,threeway 10 tops, open a duct, with a bolt fixture is connected with piston 10 to make in the piston earthquake process and can not comes off and to rotate at piston 10 knob ends and the perpendicular direction of passage.
Fig. 2 is the front view and the left view of oscillator.Oscillator can be pressed the button of its right side control panel 5 according to actual needs and regulate frequency of oscillation.The skin of said oscillator is a metal box 3, and metal box 3 inner and upper are provided with the Metallic rod that is parallel to each other 2 of two equal heights, and Metallic rod 2 is connected with the gabion 8 of below through four pulleys 1, is inlaying two lower carriages 6 that carry separatory funnel in the gabion 8.Lower carriage 6 is through being bolted in the gabion 8, and lower carriage 6 has the circular arc opening of different-diameter, with the convenient separatory funnel of placing.The right side of gabion 8 links to each other with power set through a Metallic rod.After being put into separatory funnel on the lower carriage 6, buckle two other upper bracket that has circular arc 4 above, and be connected with bolt accordingly with following lower carriage 6, so just can guarantee can not slide in the separatory funnel earthquake process.
Can hold 1-3 separatory funnel on the support of this oscillator, can adjust flexibly according to testing the required oil phase and the amount of water.
After vibration is accomplished, can directly separatory funnel be taken out and be put into standing demix on the iron stand, at last water and oil phase are separated, store for future use.

Claims (7)

1. one kind makes two phase liquid saturated device each other, comprises separatory funnel and oscillator, it is characterized in that stopper of said separatory funnel (9) and piston (10) are provided with fixture, and stopper when preventing to vibrate (9) and piston (10) are left out; The skin of said oscillator is metal box (3); Metal box (3) inner and upper is provided with the Metallic rod that is parallel to each other (2) of two equal heights; Metallic rod (2) is connected with the gabion (8) of below through pulley (1), is inlaying the lower carriage (6) that carries separatory funnel in the gabion (8).
2. device as claimed in claim 1 is characterized in that, adopts fixedly stopper (9) of plastics cutting ferrule.
3. device as claimed in claim 2 is characterized in that, adorns a fixture on stop,threeway (10) top, opens a duct in the knob end and the perpendicular direction of passage of piston (10), with a bolt fixture is connected with piston (10).
4. device as claimed in claim 1 is characterized in that, after being put into separatory funnel on the lower carriage (6), buckling other upper bracket (4) above, and is connected with bolt with following lower carriage (6).
5. device as claimed in claim 4 is characterized in that, lower carriage (6) is through being bolted in the gabion (8).
6. device as claimed in claim 5 is characterized in that, the right side of gabion (8) links to each other with power set.
7. like the arbitrary described device of claim 1-6, it is characterized in that, can hold 1-3 separatory funnel on the support of oscillator.
CN2011103169304A 2011-10-18 2011-10-18 Device for saturating two-phase solutions Pending CN102500265A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2011103169304A CN102500265A (en) 2011-10-18 2011-10-18 Device for saturating two-phase solutions

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2011103169304A CN102500265A (en) 2011-10-18 2011-10-18 Device for saturating two-phase solutions

Publications (1)

Publication Number Publication Date
CN102500265A true CN102500265A (en) 2012-06-20

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN2011103169304A Pending CN102500265A (en) 2011-10-18 2011-10-18 Device for saturating two-phase solutions

Country Status (1)

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CN (1) CN102500265A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103076210A (en) * 2012-10-17 2013-05-01 中国石油化工股份有限公司 Pretreatment device and method for determining distribution coefficient of substance in n-octanol / water system

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5478478A (en) * 1993-12-22 1995-12-26 E. I. Du Pont De Nemours And Company Apparatus and method for preventing vortexing of a liquid in a separatory funnel
CN2469990Y (en) * 2001-03-23 2002-01-09 上海智城分析仪器制造有限公司 Swing-angle adjustable oscillator
CN1636627A (en) * 2003-12-19 2005-07-13 东京理化器械株式会社 Separatory funnel support for oscillating machine
JP2007271768A (en) * 2006-03-30 2007-10-18 Casio Electronics Co Ltd Method for manufacturing electrophotographic color toner
CN201394458Y (en) * 2009-03-20 2010-02-03 上海理工大学 Ultrasonic thermostatic water bath vibrator

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5478478A (en) * 1993-12-22 1995-12-26 E. I. Du Pont De Nemours And Company Apparatus and method for preventing vortexing of a liquid in a separatory funnel
CN2469990Y (en) * 2001-03-23 2002-01-09 上海智城分析仪器制造有限公司 Swing-angle adjustable oscillator
CN1636627A (en) * 2003-12-19 2005-07-13 东京理化器械株式会社 Separatory funnel support for oscillating machine
JP2007271768A (en) * 2006-03-30 2007-10-18 Casio Electronics Co Ltd Method for manufacturing electrophotographic color toner
CN201394458Y (en) * 2009-03-20 2010-02-03 上海理工大学 Ultrasonic thermostatic water bath vibrator

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
朱权等: "《化学基础实验实训》", 31 May 2009, article "使用分液漏斗前必须做好哪些检查", pages: 130 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103076210A (en) * 2012-10-17 2013-05-01 中国石油化工股份有限公司 Pretreatment device and method for determining distribution coefficient of substance in n-octanol / water system

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Application publication date: 20120620