CN102436874B - Equipment for producing aeolotropic conductive film - Google Patents

Equipment for producing aeolotropic conductive film Download PDF

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Publication number
CN102436874B
CN102436874B CN 201110275705 CN201110275705A CN102436874B CN 102436874 B CN102436874 B CN 102436874B CN 201110275705 CN201110275705 CN 201110275705 CN 201110275705 A CN201110275705 A CN 201110275705A CN 102436874 B CN102436874 B CN 102436874B
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magnetic field
magnetic pole
equipment
current
conductive film
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CN102436874A (en
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王宇
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SHANXI JINKAIYUAN INDUSTRY Co Ltd
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SHANXI JINKAIYUAN INDUSTRY Co Ltd
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Abstract

The invention discloses equipment for producing an aeolotropic conductive film, which comprises a rack used as a magnetic yoke, an upper magnetic pole and a lower magnetic pole, wherein the upper magnetic pole and the lower magnetic pole are fixed on the rack, at least one of the upper magnetic pole and the lower magnetic pole can vertically move relative to the rack, excitation coils are wound on the upper magnetic pole and the lower magnetic pole, and a forming die of the aeolotropic conductive film is pressed and fixed between the upper magnetic pole and the lower magnetic pole; the producing equipment also comprises a power supply device for the excitation coils, wherein the power supply device comprises a rectification circuit comprising controlled silicon and a computer controller for controlling the conduction angle of the controlled silicon; and under the support of corresponding software, the continuous control of the computer controller to the output current of the rectification circuit of the controlled silicon according to the set current function I = I (t) is realized. According to the current function I = I (t), the condition that the transformation curve of a magnetic field approaches to a rectangular wave is ensured, and the requirement of orientation of the magnetic field of a conductive substance inside the film is met, so that the aeolotropic conductive film which can be used for actual application is produced by the equipment. The producing equipment has a simple structure and is convenient to operate.

Description

Equipment for producing aeolotropic conductive film
Technical field
The present invention relates to a kind of conductive film production equipment, particularly relate to a kind of equipment for producing aeolotropic conductive film.
Background technology
Anisotropic conducting film is because it only is conductivity at thickness direction, need not weld or means such as machinery assembling etc. can realize being electrically connected closely, thereby be widely used in the circuit arrangement of the accurate electrical equipment such as computer, video camera, obtains increasingly extensive attention.Equipment for the production of anisotropic conducting film is also paid attention to widely.Along with updating of anisotropic conducting film production technology, Secretary is proposed constantly also for the production equipment of anisotropic conducting film.Generally speaking may be summarized to be following some: 1, conductive film will obtain the conductivity on the thickness direction, must be the conductive materials orientation in the film under magnetic field, and magnetic field is stronger, more is conducive to formation and the improvement of electric conductivity.General alignment magnetic field is greater than 1.6T.2, in order to guarantee the insulating properties between the adjacent conductive circuit, requirement makes magnetic fields in the operation of conductive material layer, after stopping the effect of magnetic field to conductive material layer, reuse the reverse strong magnetic field action that waits in conductive material layer, number of times repeatedly is more, the faster effect of the speed of magnetic field conversion is better, particularly is even more important when the conducting wire distance is narrower.General Requirements is orientated more than 5 times repeatedly.As shown in Figure 5, desirable magnetic field conversion curve should be as far as possible near square wave.Magnetic field rises to peaked time T from 0 1And magnetic field drops to 0 time T from maximum 2That tries one's best is little, generally should be not more than 5 seconds.3, the fluidity macromolecular material that comprises conductive materials after magnetic field orientating is finished, just can be finished through overcuring the manufacturing of anisotropic conducting film, and solidification process will be kept the stationary magnetic field and keep certain curing temperature.
The anisotropic conducting film manufacturing equipment will satisfy above-mentioned 3 process conditions, just can produce the anisotropic conducting film of practical use.But when Practical manufacturing, how to satisfy above-mentioned 3 process conditions, how to guarantee that particularly the alignment magnetic field conversion curve does not have mature technology near square wave (being close to what degree) as far as possible and can use for reference, bring technical obstacle therefore for the manufacturing of the production equipment of anisotropic conducting film.At present, the main dependence on import of anisotropic conducting film, the domestic equipment of producing anisotropic conducting film that has no also has no the report of pertinent literature.
Summary of the invention
The present invention is the problem that does not have at present equipment for producing aeolotropic conductive film in order to solve, and a kind of equipment for producing aeolotropic conductive film is provided.
The present invention has adopted following technical scheme to realize: a kind of equipment for producing aeolotropic conductive film, comprise the frame as yoke, be fixed in the upper and lower magnetic pole on the frame, upper and lower magnetic pole has at least one to be that relative frame is movable up and down, be wound with magnet exciting coil on the upper and lower magnetic pole, press solidly the mould of anisotropic conducting film between the upper and lower magnetic pole; This production equipment also comprises the electric supply installation of magnet exciting coil, described electric supply installation comprises the rectification circuit that controllable silicon consists of, the computer control that is used for the control thyristor operating angle, wherein the signal input part of computer control is connected with the magnetic field strength transducer that places between two magnetic poles and the electric current that is connected in the magnet exciting coil current supply circuit and passes (mutually) sensor; Computer control is under corresponding software is supported, according to the current function I=I(t that sets) output current of SCR rectification circuit is realized continuous control; Described current function I=I(t) expression is:
Figure 13653DEST_PATH_IMAGE001
Wherein: I 0=excitation saturation current;
I mBe the setting current value greater than excitation saturation current value;
B(t) be the real-time magnetic field intensity magnetic field strength transducer collection and that be transferred to computer control;
B 0=saturation magnetic field intensity;
T 1Be magnetic field rise time section, namely magnetic field rises to the peaked time period from 0;
T 2Be the magnetic field section of holding time, i.e. the retention time section of maximum value of magnetic field;
T 3Be magnetic field section fall time, namely magnetic field drops to for zero time period from maximum;
Wherein set electric current I mTo adopt following method to determine: set current value (I for any given one mI 0), computer control is under corresponding software is supported ,According to the current function I=I(t that sets) output current of SCR rectification circuit is realized continuous control, observe the at this moment waveform in magnetic field that magnet exciting coil is built, magnetic field rise time section T in field waveform at oscilloscope 1During less than or equal to 3 seconds, this moment, corresponding setting current value was exactly set point value; This equipment also comprises the solidification equipment of anisotropic conducting film.
The those skilled in the art can easily design various structures and realize that upper and lower magnetic pole has at least a relative frame up and down.
Mould is for the manufacture of the anisotropic conducting film with a plurality of conductive path forming portions and insulation division, and it is insulated from each other that insulation division forms parts with these conductive paths.With respect to the structure of anisotropic conducting film, bossing and negative area are arranged on the apparent surface of the upper and lower mould of mould, the bossing magnetic conduction is to form the conductive path on the conductive film.The basic structure of this mould and the course of work are that the art personnel are known.
Computer control is under the support of corresponding software, control the electric current of output by the angle of flow of control SCR rectification circuit, the specific works process is: after aliving in the magnet exciting coil, produce magnetic field between magnetic pole, magnetic field strength transducer imports the real-time magnetic field intensity between magnetic pole into computer control, and electric current passes (mutually) sensor with the real-time current intensity I in the wire loop RealImport computer control into, computer control is under the support of corresponding software, and the control SCR rectification circuit is according to current function I(t) output current.Concretely, I MeterBeing given reference current, is according to current function I(t) the time dependent electric current that calculates, I RealIt then is the feedback signal of actual current; If I Meter-I Real=δ, δ are current error signal, and computer is adjusted output current by the real-time relatively value of δ.When δ be on the occasion of the time, the expression actual current is less than specified current flow, this moment, the computer control silicon controlled angle of flow became large, so that output current becomes large, until I Meter≈ I RealWhen δ was negative value, the expression actual current was greater than specified current flow, and this moment, the computer control silicon controlled angle of flow diminished, so that output current diminishes, until I Meter≈ I RealLike this, so that actual current is followed the tracks of the current function I=I(t of setting well), thereby guarantee that field curve is close to square wave.
The control computer carries out the technology of real-time tracking to output current, belongs to known content, and corresponding software is that these those skilled in the art write out easily.
After electric current was selected, equipment was started working.Mould is added in magnetic field on the conductive film and covers upper half-wave near rectangle, blanking time section T 4, through relay commutation output current-I(t), mould is added in magnetic field on the conductive film and covers lower half-wave near rectangle, again blanking time section T 4Finish the magnetic field conversion of one-period, so pass through 5-20 magnetic field change-over period, the conductive materials orientation in the conductive film is finished.
The solidification equipment of anisotropic conducting film is that the conductive film after orientation is finished is cured heating, and its structure is that those skilled in the art realize easily.
The invention provides a kind of equipment for producing aeolotropic conductive film, solved and produced the technical difficulty that anisotropic conducting film faces, current function I=I(t particularly) proposition makes the magnetic field conversion curve near square wave, realized the magnetic field orientating to conductive film inner conductive material, thereby produce the anisotropic conducting film of practical use, this current function form is simple, is convenient to working control.This device structure is simple, and is easy to operate.
Description of drawings
The agent structure schematic diagram of this equipment for producing aeolotropic conductive film of Fig. 1.
The mould structure schematic diagram of this equipment for producing aeolotropic conductive film of Fig. 2.
The electric supply installation schematic diagram of this equipment for producing aeolotropic conductive film of Fig. 3.
Fig. 4 Electric radiant Heating Film, thermocouple and Electric radiant Heating Film temperature control power supply schematic diagram.
Fig. 5 is according to Current Control function I=I(t) the B-t curve image that draws.
Among the figure: 1-yoke, 2-magnetic pole, 3-magnet exciting coil, 4-mould, 5-anisotropic conducting film, the 6-magnetic field sensor, the 7-electric current passes (mutually) sensor, 8-magnet exciting coil electric supply installation, 9-Electric radiant Heating Film, 10-thermocouple, 11-temperature control power supply, 12-supporting bracket, 13-screw rod, 14-handwheel.
Embodiment
A kind of equipment for producing aeolotropic conductive film, comprise the frame 1 as yoke, be fixed in the upper and lower magnetic pole 2 on the frame, upper and lower magnetic pole has at least one to be that relative frame is movable up and down, be wound with magnet exciting coil 3 on the upper and lower magnetic pole, press solidly the mould 4 of anisotropic conducting film between the upper and lower magnetic pole; This production equipment also comprises the electric supply installation 8 of magnet exciting coil, described electric supply installation comprises the rectification circuit that controllable silicon consists of, the computer control that is used for the control thyristor operating angle, wherein the signal input part of computer control is connected with the magnetic field strength transducer 6 that places between two magnetic poles and the electric current that is connected in the magnet exciting coil current supply circuit and passes (mutually) sensor 7; Computer control is under corresponding software is supported, according to the current function I=I(t that sets) output current of SCR rectification circuit is realized continuous control; Described current function I=I(t) expression is:
Wherein: I 0=excitation saturation current;
I mBe the setting current value greater than excitation saturation current value;
B(t) be the real-time magnetic field intensity magnetic field strength transducer collection and that be transferred to computer control;
B 0=saturation magnetic field intensity;
T 1Be magnetic field rise time section, namely magnetic field rises to the peaked time period from 0;
T 2Be the magnetic field section of holding time, i.e. the retention time section of maximum value of magnetic field;
T 3Be magnetic field section fall time, namely magnetic field drops to for zero time period from maximum;
Wherein set electric current I mTo adopt following method to determine: set current value (I for any given one mI 0), computer control is under corresponding software is supported ,According to the current function I=I(t that sets) output current of SCR rectification circuit is realized continuous control, observe the at this moment waveform in magnetic field that magnet exciting coil is built, magnetic field rise time section T in field waveform at oscilloscope 1During less than or equal to 3 seconds, this moment, corresponding setting current value was exactly set point value; This equipment also comprises the solidification equipment of anisotropic conducting film.
During concrete the manufacturing, up and down for realizing the relative frame of magnetic pole, adopt following structure: namely, frame 1 top has draw-in groove, and the top of upper magnetic pole is limited in the draw-in groove; Be provided with the supporting bracket 12 fixing with frame on draw-in groove top, have screw on the supporting bracket and be provided with screw rod 13 in screw, the upper end of screw rod is provided with handwheel 14, and the lower end of screw rod 13 and upper magnetic pole are fixed.Draw-in groove can guarantee that magnetic pole does not rotate in moving up and down process, handwheel can make things convenient for the rotation of screw rod.The work starting stage, regulate distance between two poles so that upper lower magnetic pole is close to die surface, prevent leakage field.This structural design is simple, and operating maintenance is convenient, and the magnetic field that can utilize to greatest extent magnetic pole to produce.
The temperature control power supply 11 that solidification equipment includes the Electric radiant Heating Film 9 that is attached on the mould 4 upper and lower mould opposite faces, the thermocouple 10 that is connected with Electric radiant Heating Film and powers to pyroelectric film 9; Temperature control power supply 11 includes computer control system; The signal output part of thermocouple 10 is connected with the signal input part of temperature control electric source computer control system.Magnet exciting coil electric supply installation 8 was kept saturation current I after conductive materials orientation in the conductive film was finished 0, saturation magnetic field B is kept in the magnetic field that mould is added on the conductive film 5 0Solidify beginning, thermocouple 10 is transferred to the temperature signal of Electric radiant Heating Film 9 computer control system of temperature control power supply in real time, and this control system is controlled mains switch according to the temperature of setting under the support of corresponding software.When the temperature of Electric radiant Heating Film 9 reached design temperature, the control system output order was cut off the electricity supply.This moment, solidification process was finished.This solidification equipment has improved the automaticity of solidification process owing to be furnished with thermocouple and computer control system, and is easy and simple to handle, saved manpower.

Claims (3)

1. equipment for producing aeolotropic conductive film, it is characterized in that comprising the frame (1) as yoke, be fixed in the upper and lower magnetic pole (2) on the frame, upper and lower magnetic pole has at least one to be that relative frame is movable up and down, be wound with magnet exciting coil (3) on the upper and lower magnetic pole, press solidly the mould (4) of anisotropic conducting film between the upper and lower magnetic pole, described mould is made of upper die and lower die; This production equipment also comprises the electric supply installation (8) of magnet exciting coil, described electric supply installation comprises the rectification circuit that controllable silicon consists of, be used for the computer control of control thyristor operating angle, wherein the signal input part of computer control is connected with the magnetic field strength transducer (6) that places between two magnetic poles and the current sensor (7) that is connected in the magnet exciting coil current supply circuit; Computer control is under corresponding software is supported, according to the current function I=I(t that sets) output current of SCR rectification circuit is realized continuous control; Described current function I=I(t) expression is:
Figure 529439DEST_PATH_IMAGE001
Wherein: I 0=excitation saturation current;
I mBe the setting current value greater than excitation saturation current value;
B(t) be the real-time magnetic field intensity magnetic field strength transducer collection and that be transferred to computer control;
B 0=saturation magnetic field intensity;
T 1Be magnetic field rise time section, namely magnetic field rises to the peaked time period from 0;
T 2Be the magnetic field section of holding time, i.e. the retention time section of maximum value of magnetic field;
T 3Be magnetic field section fall time, namely magnetic field drops to for zero time period from maximum;
Wherein set electric current I mBe to adopt following method to determine: set current value for any given one, computer control is under corresponding software is supported ,According to the current function I=I(t that sets) output current of SCR rectification circuit is realized continuous control, observe the at this moment waveform in magnetic field that magnet exciting coil is built, magnetic field rise time section T in field waveform at oscilloscope 1During less than or equal to 3 seconds, this moment, corresponding setting current value was exactly set point value; This equipment also comprises the solidification equipment of anisotropic conducting film.
2. equipment for producing aeolotropic conductive film as claimed in claim 1, the solidification equipment that it is characterized in that described anisotropic conducting film include the Electric radiant Heating Film (9) that is attached on mould (4) the upper and lower mould opposite face, the thermocouple (10) that is connected with Electric radiant Heating Film and to the temperature control power supply (11) of Electric radiant Heating Film power supply; Described temperature control power supply (11) includes computer control system; The signal output part of described thermocouple (10) is connected with the signal input part of temperature control electric source computer control system.
3. equipment for producing aeolotropic conductive film as claimed in claim 1 or 2 is characterized in that frame (1) top has draw-in groove, and the top of upper magnetic pole is limited in the draw-in groove; Be provided with the supporting bracket (12) fixing with frame on draw-in groove top, have screw on the supporting bracket (12) and be provided with screw rod (13) in screw, the upper end of screw rod is provided with handwheel (14), and lower end and the upper magnetic pole of screw rod (13) are fixed.
CN 201110275705 2011-09-17 2011-09-17 Equipment for producing aeolotropic conductive film Expired - Fee Related CN102436874B (en)

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CN105506315B (en) * 2015-12-15 2017-06-27 中国科学院合肥物质科学研究院 A kind of equipment for preparing anisotropic conductive composite under magnetic fields on demand

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