CN102425917B - Multifunctional rectifying tower - Google Patents

Multifunctional rectifying tower Download PDF

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Publication number
CN102425917B
CN102425917B CN 201110252564 CN201110252564A CN102425917B CN 102425917 B CN102425917 B CN 102425917B CN 201110252564 CN201110252564 CN 201110252564 CN 201110252564 A CN201110252564 A CN 201110252564A CN 102425917 B CN102425917 B CN 102425917B
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column
tower
crude argon
hypomere
rectifying
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CN 201110252564
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CN102425917A (en
Inventor
杨修玲
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Hang Yang Group Co ltd
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Hangzhou Hangyang Co Ltd
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Abstract

The invention relates to a multifunctional rectifying column mainly comprising a rectifying column and a crude argon column, wherein the rectifying column comprises an upper column and a lower column; the crude argon column is connected with the rectifying column; the upper column is divided into an upper section and a lower section by using an argon friction extract opening as a cutting point; the lower section of the upper column is connected with the crude argon column to form a column body; the upper section of the upper column serves as an auxiliary column and is connected with the lower section of the upper column through a rising steam pipe orifice; the lower part of the rectifying column is communicated with the lower section of the upper column through a liquid distributor; the upper section of the upper column is connected with the liquid distributor through a backflow liquid pipe orifice and is communicated with the lower part of the lower section of the upper column through the liquid distributor; and the multifunctional rectifying column has the characteristics of reasonable structure, stable operation, energy saving and consumption reduction and the like.

Description

A kind of Multifunctional rectifying column
Technical field
What the present invention relates to is a kind of Multifunctional rectifying column, a kind of function that not only can realize simultaneously tower and crude argon column, and can also save energy and reduce the cost, the reduce cost cost belongs to energy class air separation technology field.
Background technology
Along with the fast development of China's industry, the enterprises such as smelting iron and steel, petrochemical industry, Coal Chemical Industry, large chemical fertilizer sharply increase the demand of oxygen argon nitrogen, and are also increasing with gas and fluid volume, thereby drive developing towards large-scale and large of rectifying column.The tower diameter of rectifying column and highly be mutually to restrict, the increase that reduces to cause tower height of tower diameter, to cause gas-liquid skewness in the tower and the rectifying column tower diameter is excessive, and many-sided problem such as installation, manufacturing, transportation, excessive height will be had higher requirement at aspects such as Material selection, wind load, securities to ice chest, researched and developed the gas-liquid distributed architecture of various complexity for each enterprise of the problems referred to above and researcher, so not only increased gas-liquid distributed architecture manufacture difficulty, but also increased production cost, prolonged the production cycle.
At present, distribute for the gas uniform of the large tower diameter rectifying column of air separation unit and to realize by gas distributor that mainly the distribution of gas inequality not only affects the rectification effect of rectifying column, but also increase the rectifying column energy consumption.
Summary of the invention
The objective of the invention is to overcome the deficiencies in the prior art, and provide a kind of do not need on tower extract in the situation of argon cut steam, just can realize the normal operation of crude argon column, simultaneously successful solution the upper tower argon cut steam uneven problem of distribution of gas that enters crude argon column, can also reduce the Multifunctional rectifying column of tower height, saving cost.
The objective of the invention is to finish by following technical solution, it mainly includes a rectifying column that is comprised of Shang Ta and lower tower, one crude argon column that links to each other with rectifying column, described upper tower is taken out mouthful as cut-point take the argon cut and is divided into two sections, wherein tower and described crude argon column are connected to a tower body on the hypomere, and tower on the epimere is also linked to each other with tower on the hypomere by the rising steam mouth of pipe as secondary tower; The bottom of described rectifying column is connected with tower on the hypomere by a liquid distribution trough, and tower links to each other with described liquid distribution trough by the phegma mouth of pipe on the described epimere, and the bottom of passing through tower on this liquid distribution trough and the hypomere is connected.
Described crude argon column is connected on the hypomere in the tower by a upper cone and consists of a combination tower body; The feed gas of described crude argon column is distributed as the rising steam of tower on the hypomere from distribution.
The present invention by with crude argon column as the secondary tower of tower on the hypomere and be designed to one the combination tower body, saved material, reduce cost, compare with traditional rectifying column, can greatly improve the initial distribution that argon cut steam enters into crude argon column, have the characteristics such as rational in infrastructure, stable, energy-saving and cost-reducing.
Description of drawings
Fig. 1 is the structural principle schematic diagram of prior art.
Fig. 2 is structural principle schematic diagram of the present invention.
The specific embodiment
The present invention is further illustrated below in conjunction with accompanying drawing: Fig. 1 is conventional rectification tower structure principle schematic, it comprises tower 11, crude argon column 12, the specific works process is as follows: take out mouthful extraction argon cut steam as the charging of crude argon column 12 from upper tower 11 argon cuts, the liquid of crude argon column 12 tower reactors is back in the upper tower 11 as argon cut phegma.Along with air separation plant towards large scale development, the tower diameter of rectifying column and tower height also constantly increase, the distributing homogeneity of the height of ice chest and rectifying column air inlet becomes urgent problem.
Fig. 2 is the structural principle schematic diagram of Multifunctional rectifying column of the present invention, it mainly includes a rectifying column that is comprised of Shang Ta and lower tower, one crude argon column that links to each other with rectifying column 21, described upper tower is taken out mouthful as cut-point take the argon cut and is divided into two sections, wherein tower 22 is connected to a combination tower body with described crude argon column 21 on the hypomere, and tower on the epimere 23 is also linked to each other with tower 22 on the hypomere by the rising steam mouth of pipe 24 as secondary tower; The bottom of described crude argon column 21 is connected with tower 22 on the hypomere by a liquid distribution trough 25, and tower 23 links to each other with described liquid distribution trough 25 by the phegma mouth of pipe 26 on the described epimere, and the bottom of passing through tower 22 on this liquid distribution trough 25 and the hypomere is connected.
Described crude argon column 21 is connected on the hypomere in the tower 22 by a upper cone 27 and consists of a combination tower body; The feed gas of described crude argon column 21 is distributed as the rising steam of tower 22 on the hypomere from distribution.
The specific works process is as follows: the rising steam of tower 22 bottoms and lower flowing liquid carry out heat and mass on the hypomere, tower 22 tops on hypomere (being crude argon column 21 bottoms) reach argon cut concentration, part argon cut steam enters into crude argon column 21 and participates in rectifying under the effect of pressure, another part argon cut steam enters into tower 23 sustainable participation rectifying on the epimere by the rising steam mouth of pipe 24.
The present invention does not need to extract the argon cut from upper tower, enter into crude argon column 21 after distributing again by gas distributor and carry out rectifying, but directly tower on the hypomere 22 and crude argon column 21 are connected to a tower body, so that entering into crude argon column 21, argon cut steam carries out rectifying by the certainly distribution of gas in tower body, can greatly improve the distribution situation of argon cut steam in crude argon column, improved the rectification effect of crude argon column, played energy-saving and cost-reducing effect, simultaneously the present invention will save the connecting line between tower 22 tops and two end sockets in crude argon column 21 bottoms and crude argon column 21 and upper tower on the hypomere, not only saved material, and reduced tower height, be a kind of energy-efficient, the rectifying device of economical rationality.

Claims (2)

1. Multifunctional rectifying column, it mainly includes a rectifying column that is comprised of Shang Ta and lower tower, one crude argon column that links to each other with rectifying column, it is characterized in that described upper tower is taken out mouthful as cut-point take the argon cut is divided into two sections, wherein tower and described crude argon column are connected to a tower body on the hypomere, and tower on the epimere is also linked to each other with tower on the hypomere by the rising steam mouth of pipe as secondary tower; The bottom of described crude argon column is connected with tower on the hypomere by a liquid distribution trough, and tower links to each other with described liquid distribution trough by the phegma mouth of pipe on the described epimere, and the bottom of passing through tower on this liquid distribution trough and the hypomere is connected.
2. Multifunctional rectifying column according to claim 1 is characterized in that described crude argon column is connected on the hypomere in the tower by a upper cone and consists of a combination tower body; The feed gas of described crude argon column is distributed as the rising steam of tower on the hypomere from distribution.
CN 201110252564 2011-08-30 2011-08-30 Multifunctional rectifying tower Active CN102425917B (en)

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CN102425917B true CN102425917B (en) 2013-04-10

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Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106642996A (en) * 2016-12-20 2017-05-10 杭州杭氧股份有限公司 Cryogenic rectification device and method in process argon recovery system
CN110487025A (en) * 2019-08-23 2019-11-22 乔治洛德方法研究和开发液化空气有限公司 A kind of air-separating plant

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0870524A1 (en) * 1997-04-11 1998-10-14 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Plant for separating a gas mixture by distillation
CN202254636U (en) * 2011-08-30 2012-05-30 杭州杭氧股份有限公司 Multifunctional rectifying column

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH05280862A (en) * 1992-03-31 1993-10-29 Nippon Sanso Kk Apparatus and method for liquefying and separating air

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0870524A1 (en) * 1997-04-11 1998-10-14 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Plant for separating a gas mixture by distillation
CN202254636U (en) * 2011-08-30 2012-05-30 杭州杭氧股份有限公司 Multifunctional rectifying column

Non-Patent Citations (5)

* Cited by examiner, † Cited by third party
Title
JP特开平5-280862A 1993.10.29
关于粗氩塔分段方式的探讨;李耀等;《深冷技术》;20080630(第3期);第29-31页 *
填料层内液体的分布及液体分布器的选型;陈桂珍等;《深冷技术》;20010228(第1期);第10-13页 *
李耀等.关于粗氩塔分段方式的探讨.《深冷技术》.2008,(第3期),第29-31页.
陈桂珍等.填料层内液体的分布及液体分布器的选型.《深冷技术》.2001,(第1期),第10-13页.

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Address after: No.799, Xiangfu Road, Qingshanhu street, Lin'an District, Hangzhou City, Zhejiang Province

Patentee after: Hangzhou oxygen generator group Co.,Ltd.

Address before: 310004 No. 388 Dong Xin Road, Xiacheng District, Zhejiang, Hangzhou

Patentee before: HANGZHOU HANGYANG Co.,Ltd.

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CP01 Change in the name or title of a patent holder

Address after: 799 Xiangfu Road, Qingshanhu street, Lin'an District, Hangzhou City, Zhejiang Province

Patentee after: Hang Yang Group Co.,Ltd.

Address before: 799 Xiangfu Road, Qingshanhu street, Lin'an District, Hangzhou City, Zhejiang Province

Patentee before: Hangzhou oxygen generator group Co.,Ltd.