CN102406954A - Plant extract deodorant and preparation method thereof - Google Patents

Plant extract deodorant and preparation method thereof Download PDF

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Publication number
CN102406954A
CN102406954A CN2011103670730A CN201110367073A CN102406954A CN 102406954 A CN102406954 A CN 102406954A CN 2011103670730 A CN2011103670730 A CN 2011103670730A CN 201110367073 A CN201110367073 A CN 201110367073A CN 102406954 A CN102406954 A CN 102406954A
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China
Prior art keywords
extraction liquid
plant extraction
plant extract
deodorizer
pericarpium citri
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Pending
Application number
CN2011103670730A
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Chinese (zh)
Inventor
解清杰
段明飞
吴春笃
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Jiangsu University
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Jiangsu University
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Publication date
Application filed by Jiangsu University filed Critical Jiangsu University
Priority to CN2011103670730A priority Critical patent/CN102406954A/en
Publication of CN102406954A publication Critical patent/CN102406954A/en
Pending legal-status Critical Current

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Abstract

The invention relates to a plant extract deodorant, in particular to a deodorant using orange peel or shaddock peel as an extracting source. The preparation method comprises the following steps of: cleaning orange peel or shaddock peel, crushing the orange peel or shaddock peel for 30-60 min by using a crusher, adding distilled water, and immersing the crushed orange peel or shaddock for 60-90 min; boiling the solution for 30-60 min, filtering out the decoction, adding distilled water into filter residue, decocting the mixture for 30 min, and merging the filtrates of two times; centrifuging the mixture at 2500-3000 r/min for 20-30 min, taking the supernate, and heating and concentrating the extract to obtain 100% concentration plant extract deodorant by using a rotary evaporator at constant temperature of 60 DEG C. The plant extract is diluted according to different needs. The plant extract deodorant provided by the invention has the characteristics of good deodorization effect, rapid effect taking and no secondary pollution.

Description

A kind of plant extraction liquid deodorizer and preparation method thereof
Technical field
The present invention relates to a kind of plant extraction liquid deodorizer and preparation method thereof, be specially a kind of Pericarpium Citri Reticulatae, Pericarpium Citri grandis extracting solution of utilizing and prepare deodorizer.
Background technology
The foul gas that produces in the municipal sewage treatment process mainly concentrates on pump house, setting pot, Aeration tank, sedimentation tank and Treatment of Sludge district, and major pollutants have Organic substances such as inorganic matters such as hydrogen sulfide, ammonia and low-molecular-weight fatty acid, amine, aldehydes, ketone, ethers, halogenated hydrocarbons.Handle industrial malodorous common method at present WATER-WASHING METHOD, medicinal liquid ablution, active carbon adsorption, ozone oxidation method, static deodorization process, soil deodorization method, firing method and biological deodorizing method etc. are arranged; Wherein, The plant extraction liquid deodorization process has that non-secondary pollution, disposal cost are low, convenient operating maintenance, odor removal efficient advantages of higher, in the lift pump room of the big municipal wastewater treatment plant of foul smell generation, foul gas between sludge dewatering are handled, more and more receives publicity.
At present, absorption method is the common method of administering foul gas, and active carbon, peat are to use the widest absorbing and deodorizing agent, but cost is higher, complex manufacturing.Patent No. CN1411872A has proposed a kind of microbial deodorant, and this deodorizer effect is remarkable, and cost is lower, but manufacturing process is complicated, unsuitable large-scale promotion.
Summary of the invention
The objective of the invention is to propose a kind of plant extraction liquid deodorizer, have good deodorization effect, instant effect, the characteristics of non-secondary pollution.
The used plant source of the present invention is Pericarpium Citri Reticulatae or Pericarpium Citri grandis.
Method for preparing of the present invention is following:
Clean Pericarpium Citri Reticulatae or Pericarpium Citri grandis, pulverize 30-60min with pulverizer, adding distil water soaks 60-90min; Boil 30-60min then, leach decocting liquid, in the filtering residue again adding distil water decoct 30min; 2 filtratings are merged,, get supernatant in the centrifugal 20-30min of 2500-3000r/min; Use 60 ℃ of Rotary Evaporators steady temperatures, the extracting solution heating is concentrated promptly obtain 100% concentration plant extraction liquid deodorizer.According to different needs, plant extraction liquid is diluted.
Deodorizer preparation flow of the present invention is simple, and the used common equipment that is is easy to control, need not add any additional medicaments, and raw material is twice laid, and cost is very little, is suitable for large-scale production.Plant extraction liquid deodorizer of the present invention is mainly used in sewage pump plant etc. and has the foul odour place, has deodorizing effect preferably than existing product.
The specific embodiment
Embodiment one:
Get Pericarpium Citri Reticulatae 100g and clean, pulverize 30min with pulverizer, adding distil water 500ml soaks 60min; Boil 30min then, leach decocting liquid, in the filtering residue again adding distil water 200ml decoct 30min; 2 filtratings are merged,, get supernatant in the centrifugal 20min of 2500r/min; Use 60 ℃ of Rotary Evaporators steady temperatures, the extracting solution heating is concentrated into 100ml, promptly obtain 100% concentration plant extraction liquid deodorizer.With deodorizer and water in proportion 1:1 dilute, can be used for the deodorization in sewage pump room.
Embodiment two:
Get Pericarpium Citri grandis 100g and clean, pulverize 30min with pulverizer, adding distil water 500ml soaks 60min; Boil 30min then, leach decocting liquid, in the filtering residue again adding distil water 200ml decoct 30min; 2 filtratings are merged,, get supernatant in the centrifugal 20min of 2500r/min; Use 60 ℃ of Rotary Evaporators steady temperatures, the extracting solution heating is concentrated into 100ml, promptly obtain 100% concentration plant extraction liquid deodorizer.With deodorizer and water in proportion 1:1 dilute, can be used for the deodorization in sewage pump room.
Embodiment three:
Pericarpium Citri Reticulatae and Pericarpium Citri grandis press mass ratio 1:1 altogether 100g clean, pulverize 60min with pulverizer, adding distil water 500ml soaks 90min; Boil 60min then, leach decocting liquid, in the filtering residue again adding distil water 200ml decoct 30min; 2 filtratings are merged,, get supernatant in the centrifugal 30min of 3000r/min; Use 60 ℃ of Rotary Evaporators steady temperatures, the extracting solution heating is concentrated into 100ml, promptly obtain 100% concentration plant extraction liquid deodorizer.With deodorizer and water in proportion 1:1.5 dilute, can be used for the deodorization between sludge dewatering.

Claims (3)

1. a plant extraction liquid deodorizer method for distilling is characterized in that, cleans Pericarpium Citri Reticulatae or Pericarpium Citri grandis, pulverizes 30-60min with pulverizer; Adding distil water soaks 60-90min, boils 30-60min then, leaches decocting liquid; In the filtering residue again adding distil water decoct 30min, 2 filtratings are merged, in the centrifugal 20-30min of 2500-3000r/min; Get supernatant, use 60 ℃ of Rotary Evaporators steady temperatures, the extracting solution heating is concentrated promptly obtain 100% concentration plant extraction liquid deodorizer.
2. a kind of according to claim 1 plant extraction liquid deodorizer method for distilling is characterized in that used plant extract source is Pericarpium Citri Reticulatae and Pericarpium Citri grandis.
3. a plant extraction liquid deodorizer is characterized in that, the plant extraction liquid deodorizer that utilizes claim 1 or 2 said plant extraction liquid deodorizer method for distilling to obtain.
CN2011103670730A 2011-11-18 2011-11-18 Plant extract deodorant and preparation method thereof Pending CN102406954A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2011103670730A CN102406954A (en) 2011-11-18 2011-11-18 Plant extract deodorant and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2011103670730A CN102406954A (en) 2011-11-18 2011-11-18 Plant extract deodorant and preparation method thereof

Publications (1)

Publication Number Publication Date
CN102406954A true CN102406954A (en) 2012-04-11

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CN (1) CN102406954A (en)

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102698303A (en) * 2012-05-25 2012-10-03 上海复振科技有限公司 Plant source compound deodorant, preparation method and application of plant source compound deodorant
CN102861350A (en) * 2012-06-11 2013-01-09 中国科学院成都生物研究所 Compound biological agent for deodorizing public toilets, and preparation method and application of compound biological agent
CN103283965A (en) * 2013-06-03 2013-09-11 王真明 Plant flavor changer and method for preparing animal feed by using same
CN103920178A (en) * 2013-01-16 2014-07-16 封新娥 Simply made natural orange flavor environment-friendly refreshing agent
CN103990166A (en) * 2014-06-17 2014-08-20 陈智辉 Preparation method of aquilaria sinensis leaf composite aromatic vinegar
CN104739709A (en) * 2015-02-12 2015-07-01 广州市增城杰佳精细化工厂 Deodorant as well as preparation method and application thereof
CN110127931A (en) * 2018-02-08 2019-08-16 河北容公环保科技有限公司 A kind of Combined sewage processing equipment
CN110801526A (en) * 2019-11-22 2020-02-18 高军利 Preparation method of deodorant
CN111545032A (en) * 2020-03-30 2020-08-18 江苏省家禽科学研究所 Traditional Chinese medicine deodorant for treating odor of livestock and poultry manure, preparation method thereof and purification device for treating odor of livestock and poultry manure

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1390462A (en) * 2002-07-03 2003-01-15 舒朝然 Biologic insecticidal bactericide without environmental pollution
CN1416905A (en) * 2002-12-06 2003-05-14 周士强 Natural perfume for automobile and its prepn process and use device
CN1613325A (en) * 2004-09-20 2005-05-11 南开大学 Natural lemon antiseptics and preparation thereof
CN1958078A (en) * 2005-11-03 2007-05-09 黄素芳 Multi purpose fresh deodorizer
KR100719857B1 (en) * 2006-12-12 2007-05-18 (주)원일실업 Manufacturing method for deodorizer composition
CN101879320A (en) * 2010-05-28 2010-11-10 华南农业大学 Refrigerator deodorant and preparation method thereof
CN101920029A (en) * 2009-06-09 2010-12-22 魏大祥 Bacteriostatic and deodorizing stock solution extracted from plants

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1390462A (en) * 2002-07-03 2003-01-15 舒朝然 Biologic insecticidal bactericide without environmental pollution
CN1416905A (en) * 2002-12-06 2003-05-14 周士强 Natural perfume for automobile and its prepn process and use device
CN1613325A (en) * 2004-09-20 2005-05-11 南开大学 Natural lemon antiseptics and preparation thereof
CN1958078A (en) * 2005-11-03 2007-05-09 黄素芳 Multi purpose fresh deodorizer
KR100719857B1 (en) * 2006-12-12 2007-05-18 (주)원일실업 Manufacturing method for deodorizer composition
CN101920029A (en) * 2009-06-09 2010-12-22 魏大祥 Bacteriostatic and deodorizing stock solution extracted from plants
CN101879320A (en) * 2010-05-28 2010-11-10 华南农业大学 Refrigerator deodorant and preparation method thereof

Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102698303A (en) * 2012-05-25 2012-10-03 上海复振科技有限公司 Plant source compound deodorant, preparation method and application of plant source compound deodorant
CN102698303B (en) * 2012-05-25 2016-08-10 上海复振科技有限公司 Plant source compound deodorant and its preparation method and application
CN102861350A (en) * 2012-06-11 2013-01-09 中国科学院成都生物研究所 Compound biological agent for deodorizing public toilets, and preparation method and application of compound biological agent
CN103920178A (en) * 2013-01-16 2014-07-16 封新娥 Simply made natural orange flavor environment-friendly refreshing agent
CN103283965A (en) * 2013-06-03 2013-09-11 王真明 Plant flavor changer and method for preparing animal feed by using same
CN103283965B (en) * 2013-06-03 2015-07-08 王真明 Plant flavor changer and method for preparing animal feed by using same
CN103990166A (en) * 2014-06-17 2014-08-20 陈智辉 Preparation method of aquilaria sinensis leaf composite aromatic vinegar
CN103990166B (en) * 2014-06-17 2016-06-01 陈智辉 The fragrant leaf compound perfume of a kind of tabernaemontanus bulrush smokes the preparation method of vinegar
CN104739709A (en) * 2015-02-12 2015-07-01 广州市增城杰佳精细化工厂 Deodorant as well as preparation method and application thereof
CN110127931A (en) * 2018-02-08 2019-08-16 河北容公环保科技有限公司 A kind of Combined sewage processing equipment
CN110801526A (en) * 2019-11-22 2020-02-18 高军利 Preparation method of deodorant
CN111545032A (en) * 2020-03-30 2020-08-18 江苏省家禽科学研究所 Traditional Chinese medicine deodorant for treating odor of livestock and poultry manure, preparation method thereof and purification device for treating odor of livestock and poultry manure

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Application publication date: 20120411