CN102400403A - Clean and industrial production method for high-grade rice paper pulp - Google Patents
Clean and industrial production method for high-grade rice paper pulp Download PDFInfo
- Publication number
- CN102400403A CN102400403A CN2010102768737A CN201010276873A CN102400403A CN 102400403 A CN102400403 A CN 102400403A CN 2010102768737 A CN2010102768737 A CN 2010102768737A CN 201010276873 A CN201010276873 A CN 201010276873A CN 102400403 A CN102400403 A CN 102400403A
- Authority
- CN
- China
- Prior art keywords
- pulp
- rice paper
- minutes
- slurry
- grade rice
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 235000007164 Oryza sativa Nutrition 0.000 title claims abstract description 12
- 235000009566 rice Nutrition 0.000 title claims abstract description 12
- 229920001131 Pulp (paper) Polymers 0.000 title claims abstract 4
- 238000009776 industrial production Methods 0.000 title description 3
- 238000000034 method Methods 0.000 title description 3
- 240000007594 Oryza sativa Species 0.000 title 1
- 241000209094 Oryza Species 0.000 claims abstract description 11
- LHJQIRIGXXHNLA-UHFFFAOYSA-N calcium peroxide Chemical compound [Ca+2].[O-][O-] LHJQIRIGXXHNLA-UHFFFAOYSA-N 0.000 claims abstract description 10
- 238000006243 chemical reaction Methods 0.000 claims abstract description 8
- 239000004343 Calcium peroxide Substances 0.000 claims abstract description 5
- 239000004115 Sodium Silicate Substances 0.000 claims abstract description 5
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims abstract description 5
- 235000019402 calcium peroxide Nutrition 0.000 claims abstract description 5
- 210000002615 epidermis Anatomy 0.000 claims abstract description 5
- 239000001301 oxygen Substances 0.000 claims abstract description 5
- 229910052760 oxygen Inorganic materials 0.000 claims abstract description 5
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims abstract description 5
- 229910052911 sodium silicate Inorganic materials 0.000 claims abstract description 5
- 238000003756 stirring Methods 0.000 claims abstract description 5
- 239000002023 wood Substances 0.000 claims abstract description 5
- 239000007788 liquid Substances 0.000 claims abstract description 4
- 238000000197 pyrolysis Methods 0.000 claims abstract description 4
- 239000002994 raw material Substances 0.000 claims abstract description 3
- 239000002002 slurry Substances 0.000 claims description 16
- 239000002699 waste material Substances 0.000 claims description 5
- 235000002710 Ilex cornuta Nutrition 0.000 claims description 4
- 241001310146 Ilex cornuta Species 0.000 claims description 4
- 235000010326 Osmanthus heterophyllus Nutrition 0.000 claims description 4
- 230000005622 photoelectricity Effects 0.000 claims description 4
- 235000019795 sodium metasilicate Nutrition 0.000 claims description 4
- 238000010009 beating Methods 0.000 claims description 3
- 239000002738 chelating agent Substances 0.000 claims description 3
- 238000012216 screening Methods 0.000 claims description 3
- 235000014347 soups Nutrition 0.000 claims description 3
- 241000237502 Ostreidae Species 0.000 claims description 2
- 239000012141 concentrate Substances 0.000 claims description 2
- 235000020636 oyster Nutrition 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 6
- 239000000835 fiber Substances 0.000 abstract description 3
- 238000004537 pulping Methods 0.000 abstract description 3
- 239000000203 mixture Substances 0.000 abstract description 2
- KEQXNNJHMWSZHK-UHFFFAOYSA-L 1,3,2,4$l^{2}-dioxathiaplumbetane 2,2-dioxide Chemical compound [Pb+2].[O-]S([O-])(=O)=O KEQXNNJHMWSZHK-UHFFFAOYSA-L 0.000 abstract 1
- 240000006248 Broussonetia kazinoki Species 0.000 abstract 1
- 241000196324 Embryophyta Species 0.000 abstract 1
- 239000013522 chelant Substances 0.000 abstract 1
- 239000003814 drug Substances 0.000 abstract 1
- 238000007873 sieving Methods 0.000 abstract 1
- 230000003068 static effect Effects 0.000 abstract 1
- 230000008961 swelling Effects 0.000 abstract 1
- 230000001954 sterilising effect Effects 0.000 description 3
- 238000004659 sterilization and disinfection Methods 0.000 description 3
- 229920002472 Starch Polymers 0.000 description 2
- 238000004061 bleaching Methods 0.000 description 2
- 230000001877 deodorizing effect Effects 0.000 description 2
- 231100000614 poison Toxicity 0.000 description 2
- 230000007096 poisonous effect Effects 0.000 description 2
- 235000019698 starch Nutrition 0.000 description 2
- 239000008107 starch Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- ZKQDCIXGCQPQNV-UHFFFAOYSA-N Calcium hypochlorite Chemical compound [Ca+2].Cl[O-].Cl[O-] ZKQDCIXGCQPQNV-UHFFFAOYSA-N 0.000 description 1
- 238000004887 air purification Methods 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000010411 cooking Methods 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000004570 mortar (masonry) Substances 0.000 description 1
- 238000010422 painting Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Detergent Compositions (AREA)
- Paper (AREA)
Abstract
The invention relates to a clean production method for high-grade rice paper pulp, and aims to solve the problems of manual operation, long time, low efficiency and serious pollution of the conventional rice paper pulp. The clean production method is technically and basically characterized by comprising the following steps of: decomposing wingceltis and papermulberry branches into velvet barks, epidermis and wood shavings by using a squeezed thread splitter; conveying the velvet barks to a 'plant fiber photoelectric oxygen comprehensive generator', and adding a chelant, calper calcium peroxide and sodium silicate to generate resonance with the inner wall of the generator by the irradiation of ordinary ultraviolet light and the vibration of a motor; stirring continuously at the temperature of between 70 and 90 DEG C under the condition that pulp concentration is between 25 and 35 percent to uniformly mix pulp and liquid medicine are mixed uniformly and perform swelling, pyrolysis, softening, decoloration and linkage for 30 minutes, and conveying to a static reaction tower, and reacting at the temperature of 100 DEG C for 60 minutes; and extruding effluent (the milk white effluent is concentrated and dried to be used as industrial raw materials) by using a high-concentration pulp squeezer, conveying the pulp to a pulp pond, rinsing again according to required whiteness, defibering, pulping, sieving and removing dregs to obtain the pulp for preparing high-grade rice paper.
Description
Technical field the present invention is a kind of cleaned industry production method in environmental protection field.
Background technology is used for the high-grade rice paper of painting and calligraphy creation and still continues to use the pulping and papermaking method in ancient times, with peeling after wingceltis, the boiling of Chinese holly tree epicormic branch, bark is soaked in limewash two to three months; Pull the manual work of letter sorting back out and carry on the back on the slabstone of endroit airing half a year to one-year age; At any time stir,, bleaching softening by exposing to the sun and rain is cut into filament with cutting knife again; Be put in the stock tank (ancient be stone mortar) and mash pulping, look whiteness and mend with calcium hypochlorite again and float.There are three big defectives in this method: one, manually-operated labour intensity is big, and efficient is extremely low, is difficult to large-scale industrial production; Two, cooking waste liquor polluted source; Three, stock quality is difficult to control, and the pulp brightness in season that thunderstorm is many is high, and the time stock quality that thunderstorm is few is relatively poor.Even to this day, produce rice paper and remain workshop-based production technology.Because bark is difficult to bleaching, the expert thinks that the rice paper slurry is definitely to have done not suitability for industrialized production.
Summary of the invention the present invention adopts " the comprehensive generator of string photoelectricity oxygen " (utility model patent: ZI200620138146.3) divide a silk machine to decomposite velvet shape bark and epidermis, wood chip with press type the wingceltis that dries, Chinese holly branch bar; Velvet shape bark is delivered to the comprehensive generator of string photoelectricity oxygen; Starch dense 25-35%; Temperature: 70-90 degree, time: 30 minutes, add chelating agent, calper calcium peroxide, sodium metasilicate; Produce under the resonance with the generator inwall in common ultraviolet irradiation and motor rotation vibrations; Slurry and soup do not stop to stir and mix and take place that profit rises, pyrolysis, softening, decolouring, link reaction, slurry is delivered in the arrest reaction tower 100 spent in the temperature arrest reaction 60 minutes again, adopt high dense press master to extrude waste liquid; Looking whiteness floats again again; Whiteness can reach 95%ISO, after making beating, screening, slagging-off, can become whiteness height, fiber good, do not have any poisonous and harmful substance, have sterilization, the high-grade rice paper slurry of anticorrosion, sterilization, deodorizing, air purification function.
The specific embodiment 1, divide a silk machine to decomposite velvet shape bark, epidermis and wood chip air-dry wingceltis, Chinese holly branch strip adoption press type, wood chip and epidermis are done its usefulness in addition.
2, velvet shape bark is transported in the comprehensive generator of string photoelectricity oxygen; Starch dense 25-35%; Temperature 70-90 degree, adds chelating agent, calper calcium peroxide, sodium metasilicate at 30 minutes time; Produce resonance down at common ultraviolet irradiation and motor rotation vibrations and generator inwall, slurry and soup do not stop to stir to mix and take place to moisten and rise, pyrolysis, soften, decolour, link reaction.
3, slurry being delivered to the arrest reaction tower reacted 60 minutes in 100 degree temperature.
4, adopt high dense press master waste liquid to be extruded (the about 1-2 ton of ton slurry, oyster white concentrate the dry raw material of industry of making in back), slurry gets into stock tank.
5, looking whiteness need float in stock tank more again, floats again to add an amount of sodium metasilicate and calper calcium peroxide, and whiteness can reach 95%ISO.
6, will float good slurry and discongest making beating, screening, remove the gred, promptly obtain whiteness height, fiber good, do not have any poisonous and harmful substance, can sterilize, high-grade rice paper slurry that anticorrosion, sterilization, deodorizing purify air.
This preparation method can be carried out large-scale industrial production, the omnidistance no black liquor of making, and free from extraneous odour, the no waste discharge of wastewater, about 6 tons of ton slurry water, slurry yield are more than 85%, and ton is starched 1/3rd of the not enough conventional method of cost of manufacture.
Claims (1)
1. the cleaned industry working system of high-grade rice paper slurry, its basic technical features are to adopt press type to divide the silk machine that wingceltis, Chinese holly branch bar are decomposited velvet shape bark, epidermis and wood chip, velvet shape bark are delivered to " the comprehensive generator of string photoelectricity oxygen "; Add chelating agent, calper calcium peroxide, sodium metasilicate; Produce resonance in common ultraviolet irradiation and motor vibrations with the generator inwall, temperature 70-90 degree is starched under the condition of dense 25-35%; Do not stop to stir slurry and soup are mixed and take place that profit rises, pyrolysis, softening, decolour, link reaction; Be delivered to the arrest reaction tower after 30 minutes and in 100 degree temperature, reacted 60 minutes, adopt high dense press master to extrude waste liquid (oyster white concentrates, dries the back as the raw material of industry) again; Slurry is delivered to stock tank; The demand whiteness of looking is floated again, discongests making beating, screening, slagging-off again, promptly becomes the paper pulp of making high-grade rice paper.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201010276873.7A CN102400403B (en) | 2010-09-09 | 2010-09-09 | The cleaned industry working system of high-grade rice paper slurry |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201010276873.7A CN102400403B (en) | 2010-09-09 | 2010-09-09 | The cleaned industry working system of high-grade rice paper slurry |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102400403A true CN102400403A (en) | 2012-04-04 |
| CN102400403B CN102400403B (en) | 2015-09-23 |
Family
ID=45883015
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201010276873.7A Expired - Fee Related CN102400403B (en) | 2010-09-09 | 2010-09-09 | The cleaned industry working system of high-grade rice paper slurry |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102400403B (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103422387A (en) * | 2012-05-15 | 2013-12-04 | 李跃怡 | Disinfecting, sterilizing and deodorizing (TCF) photocatalytic writing and painting paper and manufacturing method thereof |
| CN103422392A (en) * | 2012-05-15 | 2013-12-04 | 李跃怡 | Disinfecting, sterilizing, antiseptic and deodorizing toilet paper (TCF) and preparation method thereof |
| CN103522830A (en) * | 2012-07-05 | 2014-01-22 | 李朝旺 | Green painting and calligraphy art with appreciation and ecological functions |
| CN105887549A (en) * | 2014-08-28 | 2016-08-24 | 李朝旺 | Total chlorine free functional type rice paper and making method thereof |
| CN105887550A (en) * | 2014-08-28 | 2016-08-24 | 李朝旺 | Total chlorine free functional type rice paper guniting machine |
| CN107287953A (en) * | 2016-04-12 | 2017-10-24 | 李朝旺 | The ecological rice paper preparation method of Chinese Chinese rose |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3107828B2 (en) * | 1994-12-16 | 2000-11-13 | リグノツィム ゲゼルシャフト ミット ベシュレンクテル ハフツング | Compositions for altering, degrading or bleaching lignin or lignin-containing substances |
| CN1619055A (en) * | 2003-11-20 | 2005-05-25 | 罗学刚 | Highly pure lignin, high efficiency fiber separating equipment system |
| CN1707019A (en) * | 2005-05-30 | 2005-12-14 | 刘长如 | Fast enviornment protection cold soaking pulping process with broad-leaved wood material |
| CN101063276A (en) * | 2006-04-26 | 2007-10-31 | 北京国力源高分子科技研发中心 | Method for hybrid giant napier producing in oxygen free radical doffing/bleaching integrated reactor with albefaction paper stuff |
| CN101591864A (en) * | 2009-06-17 | 2009-12-02 | 刘长如 | A kind of environment friendly pulping process |
-
2010
- 2010-09-09 CN CN201010276873.7A patent/CN102400403B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3107828B2 (en) * | 1994-12-16 | 2000-11-13 | リグノツィム ゲゼルシャフト ミット ベシュレンクテル ハフツング | Compositions for altering, degrading or bleaching lignin or lignin-containing substances |
| CN1619055A (en) * | 2003-11-20 | 2005-05-25 | 罗学刚 | Highly pure lignin, high efficiency fiber separating equipment system |
| CN1707019A (en) * | 2005-05-30 | 2005-12-14 | 刘长如 | Fast enviornment protection cold soaking pulping process with broad-leaved wood material |
| CN101063276A (en) * | 2006-04-26 | 2007-10-31 | 北京国力源高分子科技研发中心 | Method for hybrid giant napier producing in oxygen free radical doffing/bleaching integrated reactor with albefaction paper stuff |
| CN101591864A (en) * | 2009-06-17 | 2009-12-02 | 刘长如 | A kind of environment friendly pulping process |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103422387A (en) * | 2012-05-15 | 2013-12-04 | 李跃怡 | Disinfecting, sterilizing and deodorizing (TCF) photocatalytic writing and painting paper and manufacturing method thereof |
| CN103422392A (en) * | 2012-05-15 | 2013-12-04 | 李跃怡 | Disinfecting, sterilizing, antiseptic and deodorizing toilet paper (TCF) and preparation method thereof |
| CN103522830A (en) * | 2012-07-05 | 2014-01-22 | 李朝旺 | Green painting and calligraphy art with appreciation and ecological functions |
| CN105887549A (en) * | 2014-08-28 | 2016-08-24 | 李朝旺 | Total chlorine free functional type rice paper and making method thereof |
| CN105887550A (en) * | 2014-08-28 | 2016-08-24 | 李朝旺 | Total chlorine free functional type rice paper guniting machine |
| CN105887550B (en) * | 2014-08-28 | 2018-09-14 | 李朝旺 | Completely without chlorine functional form rice paper whitewashing instrument |
| CN107287953A (en) * | 2016-04-12 | 2017-10-24 | 李朝旺 | The ecological rice paper preparation method of Chinese Chinese rose |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102400403B (en) | 2015-09-23 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102400403A (en) | Clean and industrial production method for high-grade rice paper pulp | |
| US20080295982A1 (en) | Process for Producing Fiber Pulp Utilizing Bamboo and Pulp Produced Using the Same | |
| CN100494566C (en) | Biocatalytic clean pulping agent and application process thereof | |
| CN101210394B (en) | Technique for producing pure biological paper pulp | |
| CN101694075B (en) | Low energy consumption clean paper pulp extracting method and papermaking process thereof | |
| CN103422387A (en) | Disinfecting, sterilizing and deodorizing (TCF) photocatalytic writing and painting paper and manufacturing method thereof | |
| CN1948611A (en) | Self coupled oxidation cleaning pulp making method | |
| CN101319471A (en) | Environment friendly energy-saving circulation type non-pollution pulping process and its system apparatus | |
| CN102321992B (en) | Agent for recycling straws by using biologically cold fermentation method and process for producing plant fibers by using straws with biologically cold fermentation method | |
| CN101792980B (en) | Mechanical pulping method for biological bacteria liquid | |
| CN102747435B (en) | Biological bacterial degumming method for raw hemp | |
| CN103343468A (en) | Clean production technology based on steam explosion slurrying | |
| CN104109978B (en) | A kind of method preparing cotton linter dissolving pulp | |
| CN103174045B (en) | Production method of bark-forming handmade paper bleaching pulp | |
| KR20110026635A (en) | Method of manufacture pulp for bamboos fiber | |
| CN101260629B (en) | Physical method ecological paper pulp manufacturing technique | |
| KR101282830B1 (en) | Production Method of Solubility Pulp Made From Dioscorea batatas | |
| EP1088937A1 (en) | Process for preparing high quality paper from vegetable residuals | |
| CN112538775A (en) | Biological pulping process for papermaking | |
| CN103882752A (en) | Clean production method for Xuan paper pulp | |
| CN203700850U (en) | Cotton linter KOH stewing and pulping system | |
| CN103556515A (en) | Papermaking pulping technology | |
| KR101282831B1 (en) | Solubility Pulp Made From Dioscorea batatas | |
| CN1085755C (en) | Paper-making pulping process without black liquid | |
| CN101871135A (en) | Method for producing bleaching man-made fiber pulp |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| DD01 | Delivery of document by public notice |
Addressee: Li Chaowang Document name: the First Notification of an Office Action |
|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20180302 Address after: 101200 Pinggu, Pinggu District, Beijing, Pinggu Town, shady North Street, No. 13, No. 1, Room 802, Room 802 Patentee after: San Fu Co. Ltd. Address before: 100029 Beijing city Xicheng District Yumin Road No. 6 Yu RI building two Room 502 Patentee before: Li Chaowang |
|
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150923 Termination date: 20190909 |