CN102374898B - Monochrometer - Google Patents

Monochrometer Download PDF

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Publication number
CN102374898B
CN102374898B CN 201010249947 CN201010249947A CN102374898B CN 102374898 B CN102374898 B CN 102374898B CN 201010249947 CN201010249947 CN 201010249947 CN 201010249947 A CN201010249947 A CN 201010249947A CN 102374898 B CN102374898 B CN 102374898B
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light
box
light reflection
grating
reflection box
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CN102374898A (en
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陈建钢
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Abstract

The invention belongs to the technical field of analytical apparatus equipment, and relates to a monochrometer, and is used for solving the problem that the existing monochrometer can not satisfy individuation requirement, namely optionally change the arrange position and orientations of each component of the monochrometer according to the demand of moulding and specialty function). The monochrometer provided by the invention comprises a light-emitting box and a light reflection box, wherein the light-emitting box at least consists of a light-emitting device, a light-emitting box frame and a light-emitting box bottom; and a light reflection box at least consists of a light reflection device, a light reflection box frame and a light reflection box bottom, the light-emitting is connected with the light reflection box, the top surface and the bottom surface of the light-emitting box bottom are at least provided with installation positions for installing the light-emitting device and the light-emitting box frame and the positions are arranged in a mode of mirror symmetry; the top surface and the bottom surface of the light reflection box bottom are at least provided with installation positions for installing the light reflection device and the light reflection box frame in a mode of mirror symmetry; and technical problems can be effectively solved by adopting the technical scheme.

Description

A kind of monochromator
Technical field
The invention belongs to the analysis Instrument equipment technical field, relate to a kind of monochromator, monochromator of the present invention is grating monochromator, for example can be the grating monochromator that constitutes the ultraviolet-visual spectrometer core component.
Background technology
The structural similarity of monochromator and spectrum spectrograph, for isolate the electromagnetic radiation of a series of narrow band from broadband radiation beam, it has prism monochromator and grating monochromator with the photographic plate on the exit slit replacement spectrograph focal plane.
Wherein grating monochromator relatively is widely used, and in links such as scientific research, production, Quality Controls, no matter is to penetrate absorption spectrum, or fluorescence spectrum, Raman spectrum.But the light reflection box that existing monochromator generally comprises Luminescent cases and the light that Luminescent cases produces injected sample cell, sample box is connected with Luminescent cases by light reflection box, because the restriction on the locations of structures, existing monochromator can only be at a side (being that put on a left side) the bill coloured light of monochromator, want to make monochromator at opposite side (being that put on the right side) bill coloured light, then need to change the positional alignment of Luminescent cases, sample box and light reflection box, but prior art can't change the positional alignment of Luminescent cases, sample box and light reflection box.
Summary of the invention
Technical matters to be solved by this invention is that existing monochromator can't meet individual requirements (namely according to the moulding of outward appearance and the demand of specialized function, the arrangement position of random each assembly of change monochromator and towards), and provide a kind of monochromator at this problem.
The present invention solves the problems of the technologies described above by the following technical programs:
A kind of monochromator comprises at least by the Luminescent cases of forming at the bottom of light-emitting device, Luminescent cases frame and the Luminescent cases; And at least by the light reflection box of forming at the bottom of light reflecting device, light reflection box frame and the light reflection box, Luminescent cases and light reflection box is connected, it is characterized in that end face at the bottom of the described Luminescent cases and bottom surface at least mirror image be symmetrically arranged with the installation position of mounting light emitting device and Luminescent cases frame;
End face at the bottom of the described light reflection box and bottom surface mirror image at least are symmetrically arranged with the installation position that light reflecting device and light reflection box frame are installed.
After adopting said structure, light-emitting device and Luminescent cases frame can be installed in end face and the bottom surface at the bottom of the Luminescent cases, and light reflecting device and light launch-box frame can be installed in end face and the bottom surface at the bottom of the light reflection box; Because at the bottom of the Luminescent cases and end face and bottom surface at the bottom of the light reflection box is the mirror image symmetry, so when Luminescent cases and light reflection box is finished at the bottom of the corresponding Luminescent cases and the end face at the bottom of the light reflection box and bottom surface respectively when installing, formed two monochromators also just in time are mutual mirror image symmetries, also are that variation has taken place the relative position of Luminescent cases and light reflection box.Simultaneously, at the bottom of the Luminescent cases of the present invention and position at the bottom of light reflection box relation also can change, for example can be positioned at the bottom of the Luminescent cases at the bottom of the light reflection box all around, in order to realize this change, at the bottom of the Luminescent cases and can be two independent parts at the bottom of the light reflection box, and connect by some basic connected modes (for example splicing etc.).
The shifting gears of above-mentioned two kinds of relative positions (first kind shift gears be make Luminescent cases and light reflection box respectively at the bottom of the corresponding box of mirror image symmetry the two sides finish installation, second kind shifts gears be at the bottom of the conversion Luminescent cases and light reflection box at the bottom of relative position) comprehensive use, can be according to the operating habit of device operator, the personalized relative position that Luminescent cases and light reflection box are set.
Certainly, the present invention has also considered some problems that above-mentioned change in location is brought, when for example enforcing location changes (particularly Luminescent cases and light launch-box are installed to the mirror symmetry planes at the bottom of the described box), need dismounting Luminescent cases and light reflection box, this may just mean when reinstalling Luminescent cases and light reflection box, need debug light path again, detection with the exempt from customs examination monochromator causes bad influence, obviously, such mode of operation is loaded down with trivial details often, and the efficient of debugging light path is lower.
Technique scheme of the present invention when realizing Luminescent cases and light reflection box change in location, the generation of having avoided the described problem of literal the last period of also trying one's best, this is owing to adopted following structure at least:
End face at the bottom of the described Luminescent cases and bottom surface mirror image at least are symmetrically arranged with the installation position of mounting light emitting device and Luminescent cases frame;
End face at the bottom of the described light reflection box and bottom surface mirror image at least are symmetrically arranged with the installation position that light reflecting device and light reflection box frame are installed.
Described installation position comprises the installation position of the various parts of monochromator, so only need carry out standardized designs to assembling place of installation position and the various parts of monochromator (is that various parts and installation position are designed according to the good design drawing of debugging, thereby parts are packed into behind the corresponding installation position, at least can guarantee that parts do not need to carry out the light path debugging), just exempt the light path debugging in the assembling process, improved the efficient that realizes Luminescent cases and light reflection box change in location greatly.
Description of drawings
Fig. 1 is that put and the right structural representation of putting on the described a kind of monochromator of an embodiment left side;
Fig. 2 is the structural representation of installation position, two sides at the bottom of the Luminescent cases and at the bottom of the light reflection box in the described a kind of monochromator of embodiment;
Fig. 3 is the second box frame in the light reflection box in the described a kind of monochromator of embodiment and the assembling synoptic diagram of light partition member;
Fig. 4 is the enlarged diagram of the described smooth partition member of embodiment;
Fig. 5 is the described smooth partition member of embodiment plane 90 degree twin-beam synoptic diagram;
Fig. 6 is the vertical 90 degree twin-beam synoptic diagram of the described smooth partition member of embodiment;
Fig. 7 is the assembling synoptic diagram that the light in the described a kind of monochromator of embodiment reflects box and crack sheet;
Fig. 8 is a part of structural representation (rotating shaft of not shown grating seat) that drives the Vidacare corp of grating seat rotation in the described a kind of monochromator of embodiment;
Fig. 9 is another part structural representation that drives the Vidacare corp of grating seat rotation in the described a kind of monochromator of embodiment;
Figure 10 is the structural representation (rotating shaft of not shown grating seat) that drives the manual driving device (display screen demonstration wavelength) of grating seat rotation in the described a kind of monochromator of embodiment;
Figure 11 is the structural representation (rotating shaft of not shown grating seat) that drives the manual driving device (index dial demonstration wavelength) of grating seat rotation in the described a kind of monochromator of embodiment;
Figure 12 is the inner structure synoptic diagram of the described a kind of monochromator of embodiment;
Figure 13 installs the structural representation that forms behind light reflection box and the sample box box frame additional on Figure 12 basis;
Figure 14 is the structural representation of the described general euphotic zone of embodiment;
Figure 15 is the structural representation of the described euphotic zone of embodiment.
Embodiment
This embodiment will further be introduced the present invention by reference to the accompanying drawings, so that those skilled in the art can comprehensively understand every technical scheme of the present invention and corresponding technique effect.For convenience of description, the described monochromator of this embodiment can also select to set up sample box according to the needs that detect on the basis of the described monochromator of summary of the invention, and described sample box is connected with Luminescent cases by light reflection box.
See Fig. 1 (not shown sample cell), a kind of monochromator, comprise Luminescent cases 2, comprise the sample box 1 of sample cell and the light reflection box 3 of the light that Luminescent cases 2 produces being injected sample cell, Luminescent cases 2 comprises at the bottom of light-emitting device, Luminescent cases frame 48 and the Luminescent cases, light reflection box 3 comprises at the bottom of light reflecting device, light reflection box frame 47 and the light reflection box, referring to Fig. 2, at the bottom of the described Luminescent cases 4 and light reflection box at the bottom of 5 be an one-piece construction, at the bottom of the Luminescent cases 4 and light reflection box at the bottom of 5 end face and bottom surface mirror image be symmetrically arranged with mounting light emitting device and Luminescent cases frame 48; And the installation position of light reflecting device and light reflection box frame 47.
See Fig. 1 and Fig. 2, this embodiment has realized the change of Luminescent cases 2 and light reflection box 3 positions, for example Luminescent cases 2 is positioned at the right side that light reflects box 3 among the left figure of Fig. 1, and Luminescent cases 2 is positioned at the left side that light reflects box 3 among the right figure of Fig. 1, realize that only need carry out an invention first kind of content part introduction of above-mentioned change in location shifts gears and get final product, and prior art can't realize the change in location of Luminescent cases and light reflection box usually because the Installation and Debugging cost is too high.
The described monochromator of this embodiment has also improved detection efficiency when guaranteeing out light quality, the means that this embodiment improves detection efficiency are that the light that monochromator sends is cut apart, thereby form the dispersed light according to operating personnel's proportion requirement, prior art is to cutting apart of light of general employing dual mode:
The first, light is carried out space segmentation, namely adopt the light treatment element that light is divided into several sections, every part is only continuous, and energy only accounts for the part of light;
The second, the light time of carrying out is cut apart, namely adopt the light treatment element that light is divided into several sections, every portion
Divide only flash of light (discontinuous), and the energy ratio that accounts for light is by break time of flash of light and flash time
Ratio determines.
This embodiment adopts first kind of mode that light is cut apart, in order to realize accurately cutting apart light, and guarantee the quality of monochromator bright dipping, prior art need be debugged monochromator usually, and this embodiment adopts after the technical scheme of summary of the invention part under the situation that does not need to debug, guarantee the light quality that of monochromator, improved the technique effect of detection efficiency when adopting following two kinds of technical schemes can realize at least guaranteeing out light quality on above basis again, first kind of technical scheme is:
Described light reflecting device comprises light-management members and the light partition member that will cut apart in proportion through the light that light-management members is handled;
Referring to Fig. 3, described light reflection box frame 47 comprises that the first box frame 49 reaches the second box frame 7 coplanar with the first box frame, 49 parts, described light-management members is positioned at the first box frame 49, the light partition member is positioned at the second box frame 7, see Fig. 7, the described second box frame 7 is provided with reception and disperses end through optical receiving end (this optical receiving end can be as the described light-receiving of this embodiment hole 47) and the dispersion of the light of light-management members processing through the light of the light of light partition member processing.See Fig. 4, the side of light partition member is provided with the light entrance port 9 relative with the described second box frame 7 light-receiving holes 47, and disperses the relative light of end to divide raw edge with the described second box frame, 7 light respectively.
It is a plurality of that described light disperses end to have, the dispersion direction that it arranges orientation and number after can handling according to the light partition member and be arranged on light in the light partition member and cut apart the type of mirror and decide, and the concrete form that described light disperses to hold also can be dispersion hole.
For example, for this embodiment, it can be that as shown in Figure 5 semi-permeable and semi-reflecting mirror 11 is (namely after this mirror is handled that described light is cut apart mirror, be divided into two kinds of light that disperse direction, half light reflection, half light transmission), at this moment, see Fig. 3, the light of the second box frame 7 disperses end to comprise light transmission end (being arranged on the second box frame 7 with respect to the light beam orifice 51 of the second box frame optical receiving end, one side) and light reflection end (being arranged on the second box frame 7 with respect to the light reflection hole 50 of Luminescent cases 2 one sides), see Fig. 4 equally, the side of light partition member is provided with respectively light-transmissive port 10 and the light reflex port 8 relative with the described second box frame, 7 smooth beam orifices 51 and light reflection hole 50.After light enters from light entrance port 9, will penetrate (referring to the dotted line of Fig. 5) from light-transmissive port 10 and light reflex port 8.
Second kind of technical scheme carried out further restriction to first kind of technical scheme, and namely the light partition member is a cavity; This dispersion direction that just means light can also be the cavity hatch direction except transmission direction and reflection direction.
When described light is cut apart mirror and is also selected semi-permeable and semi-reflecting mirror for use, just there are two kinds of light deployment conditions: see Fig. 4, first kind of light deployment conditions is that light enters from light entrance port 9, penetrate (referring to the dotted line of Fig. 6) from light-transmissive port 10 and cavity hatch bore 52 respectively, described semi-permeable and semi-reflecting mirror is semi-permeable and semi-reflecting mirror 12 as shown in Figure 6; Second kind of light deployment conditions is that light enters from light entrance port 9, penetrates (the placement situation of semi-permeable and semi-reflecting mirror is not shown) from light reflex port 8 and cavity hatch bore 52 respectively.
Two kinds of technical schemes introducing above all can improve the detection efficiency of monochromator at least, because dividing the light that sheds all is parts of the former light before light is cut apart, the ratio of its shared former light can be cut apart modes such as mirror by change and regulates, so operating personnel can carry out multiple detection simultaneously on the described monochromator of this embodiment, and such detection is because the character of employed light is identical, shared former light ratio example is determined, so testing result has the contrast reference value, analysis ability significantly rises.
Two kinds of technical schemes introducing above also have such beneficial effect, namely can replace light to cut apart mirror with testing sample, and this moment, described smooth partition member was the orthobaric volume micro-example chamber of placing sample, and described monochromator can directly detect it.
This embodiment is selected monochromatic wavelength coverage, thereby the light wave scope of monochromatic light bright dipping is fallen within on technician's necessary wavelength scope, guarantees the quality of bright dipping.The method that realizes normally (is seen Figure 11 with light by grating, the concrete course of work is introduced below), adjust the angle of grating, can obtain having the light of different wavelength range, in order to make the technician can accurately adjust the angle of grating easily, this embodiment provides two kinds of technical schemes for technician's selection:
First kind is the angle that adopts electronic mode to regulate grating, specifically can be achieved like this (referring to Fig. 8):
Described light-management members comprises light-reflecting components and the grating that the light through the light-reflecting components reflection is screened, and described grating comprises grating body 53 and grating seat 40 (seeing Figure 12), and described grating body 53 is installed on the grating seat 40;
Described light reflection box 3 also comprises the Vidacare corp that drives 40 rotations of grating seat, described Vidacare corp comprises screw mandrel 23, guide rod 19, is arranged on screw mandrel 23 and the guide rod 19, walking slide block 22, lever arm 27, grating seat rotating shaft 54 (see figure 9)s that are connected with grating seat 40 that move at screw mandrel 23 and guide rod 19 with the rotation of screw mandrel 23 and the drive motor 18 that is connected with screw mandrel 23 1 ends;
One end of lever arm 27 is connected with grating seat rotating shaft 54, and the end of lever arm 27 other ends is the contact block 20 that contacts with walking slide block 22, and described grating seat rotating shaft 54 is provided with time power torsion spring that resets for the rotating shaft of grating seat.
Start drive motor 18, just can adjust the angle of grating by walking piece 22, lever arm 27 and grating seat rotating shaft 54, on this basis, be in adjusting the requirement of precision, the described Vidacare corp of this embodiment also comprises potentiometer 24, control circuit and display screen 26, screw mandrel 23 is connected by gear set 25 with potentiometer 24 with respect to an end that is connected with drive motor 18, and potentiometer 24 is connected with display screen 26 by control circuit, and drive motor 18 is connected with control circuit.
Second kind is the angle that adopts manual mode to regulate grating, specifically can be divided into two kinds of situations, and first kind of situation shows wavelength by index dial, specifically can be achieved like this:
Described light-management members comprises light-reflecting components and the grating that the light through the light-reflecting components reflection is screened, and described grating comprises grating body 53 and grating seat 40 (seeing Figure 12), and described grating body 53 is installed on the grating seat 40;
Described light reflection box 3 also comprises the manual driving device that drives 40 rotations of grating seat, see Figure 11, described manual driving device comprises the rotating disk 31 that is connected with the rotating shaft of grating seat, be located in the manual dish 29 at the bottom of the described light reflection box box and be surrounded on rotating disk 31 and manually coil driving-belt 32 on 29.
This manual driving device generally should be arranged on the place of being convenient to technician's operation, for example can be arranged on the top of light reflection box 3, manually need to mark the scale that is carved with wavelength coverage on the dish 29 simultaneously, when the technician needs the monochromatic light of a certain wavelength coverage, only needing manually to coil respective wavelength on 29 pushes assigned address and get final product and (need an indicator dog 33 be set manually coiling 29 usually, thereby when the scale of a certain wavelength coverage pushes on the indicator dog, i.e. explanation is adjusted to monochromatic wavelength coverage on this wavelength coverage).
Second kind of situation shows wavelength (referring to Figure 10, not shown display screen) by display screen, only changes manual pulley into by driving the drive motor 18 that the rotating shaft of grating seat realizes the Vidacare corp that grating seat 40 rotates with this embodiment is described.
This embodiment has also realized the function of fixed slit, (see figure 7) specific as follows:
The first crack sheet 44 that described light reflection box 3 and the junction of Luminescent cases 2 are provided with first light hole 42 (referring to Figure 13) and are made up of the first printing opacity crack part 16 relative with first light hole 42 and first shading light part 15, the width of the described first printing opacity crack part 16 is smaller or equal to first light hole, 42 width;
For ease of explanation, the described second box frame, 7 light disperse end can to have (for example being the second box frame, 7 smooth beam orifices 51) with the form of light dispersion hole, described light reflection box 3 is provided with the second crack sheet of being made up of the second printing opacity crack part 55 relative with light beam orifice 51 and second shading light part 56 44 (the second crack sheet is the first crack sheet 44 in this embodiment), and the width of the described second printing opacity crack part 55 is smaller or equal to light dispersion hole width.
Further, this embodiment has also realized the function of variable gap, the realization of this function can be on the basis that the fixed slit function realizes, printing opacity crack part 16 at crack sheet 44 is sticked a kind of euphotic zone (Fig. 7 is not shown), such euphotic zone should have different printing opacity width in the direction of euphotic zone, thereby as long as move the real-time variation of width generation that can make the transmissive slit part 16 that is positioned on the light hole 42 along the direction of euphotic zone, general such euphotic zone is exactly euphotic zone as shown in figure 14, the dash area of euphotic zone is light tight, the blank parts printing opacity), the device of certain mobile crack sheet 44 also should be indispensable, so the described light reflection of this embodiment box also comprises first driving mechanism of the mobile first crack sheet and second driving mechanism of the mobile second crack sheet.
See Fig. 7, described first driving mechanism comprises first screw mandrel 13, first guide rod 17 and the first crack sheet motor 14 that is set in parallel in the light reflection box frame 47, the described first crack sheet 44 is installed in respectively on first screw mandrel 13 and first guide rod 17 by first feed screw nut 57 and first guide rod hole 45 that is arranged on the first crack sheet 44, and first screw mandrel, 13 1 ends are connected with the first crack sheet motor, 14 output shafts.
Described second driving mechanism also can adopt and the similar structure of first driving mechanism, described second driving mechanism of this embodiment is consistent with the structure of first driving mechanism, concrete, described second driving mechanism comprises second screw mandrel that is set in parallel in the light reflection box frame 47, second guide rod and the second crack sheet motor, the described second crack sheet is installed in respectively on second screw mandrel and second guide rod by second feed screw nut and second guide rod hole that is arranged on the second crack sheet, one end of described second screw mandrel is connected (described second screw mandrel with the output shaft of the described second crack sheet motor, second guide rod, the second crack sheet motor, second feed screw nut and second guide rod hole are first screw mandrel respectively, first guide rod, the first crack sheet motor, therefore first feed screw nut and first guide rod hole do not have label).
For accurately regulating the purpose of design that crack sheet 44 moves, crack sheet motor 14 preferably is connected with the control assembly of monochromator, and such control assembly can be control circuit (as single-chip microcomputer etc.).
Embodiment
After having introduced every technical scheme of this embodiment, embodiment also will do detailed introduction to the running of monochromator.
For convenience of description, present embodiment is used the employed accompanying drawing of embodiment, should be noted that, only using for convenience of description like this, therefore, the situation that two kinds of titles appear in same label may occur, but can't cause technician's misunderstanding.
Referring to Fig. 1, a kind of monochromator comprises at least by 4 Luminescent cases of forming 2 at the bottom of light-emitting device, Luminescent cases frame 48 and the Luminescent cases; And at least by the 5 light reflection boxes of forming 3 at the bottom of light reflecting device, light reflection box frame 47 and the light reflection box, Luminescent cases 2 is connected with light reflection box 3, referring to Fig. 2, at the bottom of the described Luminescent cases 4 and light reflection box at the bottom of 5 the corresponding mirror image of end face and bottom surface be symmetrically arranged with mounting light emitting device and Luminescent cases frame 48; And the installation position of light reflecting device and light reflection box frame 47.
One, transmission and the light reflection box of light in Luminescent cases designs with shading between Luminescent cases and the sample box
As shown in figure 12, light-emitting device in the Luminescent cases 2 comprises tungsten lamp 35, deuterium lamp 34 and Luminescent cases catoptron 36, and the light that tungsten lamp 35 and deuterium lamp 34 send all can be injected the light hole 42 (referring to Figure 13) that is positioned at Luminescent cases 2 and light reflection box 3 junctions by Luminescent cases catoptron 36.
Referring to Fig. 7 (light hole 42 is not shown), be provided with crack sheet 44 in the light reflection box 3, the printing opacity crack part 16 of this crack sheet 44 be row's size smaller or equal to the square opening of light hole 42, what the light that is penetrated from light hole 42 by Luminescent cases 2 can part be covered by shading light part 15.
Why present embodiment will be arranged to transmissive slit part 16 row's (four) square opening, its purpose is the movement by crack sheet 44, different square openings can be moved on the light hole 42, thereby can adjust the transmittance that light penetrates light reflection box 3, and the final design proposal of present embodiment is to make the size of square opening consistent, and stick as shown in figure 15 the euphotic zone that is provided with the open-work corresponding with four square openings at described row's square opening, same like this can achieving the above object, and also reduced production cost.
For the movement of crack sheet, present embodiment is to realize that by the driving that is arranged on the crack sheet motor 14 on the light reflection box 3 concrete structure is such:
Crack sheet 44 is provided with guide rod hole 45 and the feed screw nut 57 who passes for the guide rod 17 that is arranged in the light reflection box 3, crack sheet motor 14 is connected with feed screw nut 57 by screw mandrel 13, and guide rod 17 and screw mandrel 13 are all parallel with the square opening orientation of printing opacity crack part 16.
Light in the light reflection box 3 finally light dispersion hole by being positioned at light reflection box 3 and the junction of sample box 1 (also i.e. the second box frame, 7 smooth beam orifices 51) enters sample box 1 (referring to Figure 13), as shown in Figure 7, the described crack sheet 44 of present embodiment also light beam orifice 51 be provided be positioned at light hole 42 on the identical printing opacity crack of the structure of printing opacity crack part 16, to realize identical purpose of design.
In order to make crack sheet 44 mobile accurately along guide rod 17, in order to adjust the transmitance of light accurately, crack sheet motor 14 can be connected with control circuit (for example single-chip microcomputer etc.).Yet such design also has perfect inadequately place, for example the described crack sheet 44 of present embodiment is an one-piece construction, this just means and can only carry out simultaneously the adjustment of the transmitance of light (present embodiment relates to Luminescent cases 2 and light reflection box 3, and the light transmission rate of light reflection box 3 and sample box 1).Improved a kind of method can be that crack sheet 44 is splitted into two halves, and uses the movement of two Electric Machine Control crack sheets 44 respectively.
Two, the transmission of light in light reflection box and sample box
Referring to Figure 12, light reflecting device comprises light-management members and light partition member, described light-management members comprises light reflection box catoptron 39, collimating mirror 41, grating and optical filter 46, inject the light of light reflection box 3 through light hole 42 (referring to Figure 13) and at first inject light reflection box catoptron 39, through first reflection, inject collimating mirror 41, with by injecting the grating that is positioned at grating seat 40 second time of collimating mirror 41, this grating will meet the light of setting wavelength coverage and inject collimating mirror 41 again, and will meet the light of setting wavelength coverage and inject optical filter 46 through reflection for the third time by collimating mirror 41, inject again be used to the second box frame 7 (referring to Fig. 7) that holds the light partition member from the light that optical filter 46 penetrates, the light partition member is that orthobaric volume micro-example chamber 6 (also is a cavity in the present embodiment, referring to Fig. 7), this orthobaric volume micro-example chamber 6 can realize that all functions of the light partition member that embodiment is partly introduced are (referring to Fig. 4-Fig. 6), also namely in orthobaric volume micro-example chamber 6, place different semi-permeable and semi-reflecting mirror (for example label 11 and 12 among Fig. 5-6), after the light-receiving hole of the second box frame 7 47 (see figure 7)s are injected, light namely enters the light entrance port 9 of orthobaric volume micro-example chamber 6, and any two directions ejaculations from three directions, described three directions are 90 ° of levels (i.e. the direction that penetrates through light reflex port 8) for injecting direction with light, inject direction with light and be vertical 90 ° (i.e. the directions that 6 cavity hatch bores 52 penetrate through orthobaric volume micro-example chamber), inject direction identical (i.e. the direction that penetrates through light-transmissive port 10) with light.
The light that penetrates from light-transmissive port 10 is injected lens 38 in the sample box through the light beam orifice 43 of crack sheet 44 and the second box frame, and penetrates from lens 37 through sample cell (Figure 12 is not shown).
Three, the installation of each parts of monochromator
In the detailed introduction of embodiment part how to make the rotation of grating, obtaining meeting the light of setting wavelength coverage, a kind of is to adopt manual mode to drive the rotation of grating, and the another kind of higher electronic mode of degree of accuracy that adopts drives the grating rotation.The accurate rotation that realizes grating needs the higher grating drive unit of design precision on the one hand, on the other hand, also needs grating is in place.
In fact, because the described monochromator of present embodiment is an exact instrument, all can increase the light quality that of monochromator greatly any human error who installs, the outfit that present embodiment is supporting with each parts in the monochromator element seat, for example, for grating, corresponding grating seat is arranged, for the catoptron in the Luminescent cases, corresponding mirror unit etc. is arranged, and the installation position of corresponding component seat is all arranged in Luminescent cases and light reflection box, and all element seat and installation position all are mould standard production, therefore, can guarantee the compactedness of instrument, when the present embodiment monochromator is installed simultaneously, as long as parts are put into corresponding element seat, again element seat is installed to the installation that corresponding installation position can be finished monochromator fast and accurately, and does not need debugging.Introduction by the embodiment part, after the described monochromator of present embodiment can be realized disposable input, satisfy the detection method demand that single beam ultraviolet-visual spectrometer, twin-beam ultraviolet-visual spectrometer, ratio is monitored the twin-beam ultraviolet-visual spectrometer, satisfy the operating habit according to device operator, the demand of the personalized relative position that Luminescent cases and light reflection box are set; Satisfied the operation individual demand that automatic wavelength setting (length scanning) or manual wavelength arrange; Satisfied the differentiated demand that digital demonstration and index dial show; Satisfied parts the demand of exempting to debug is installed, efficiency improves more than 100 times; Having satisfied the user changes light source and exempts from instrument, non-regulating function and life science, biochemical analysis to the requirement of trace test (realizing by orthobaric volume micro-example chamber).

Claims (13)

1. a monochromator comprises at least by the Luminescent cases of forming at the bottom of light-emitting device, Luminescent cases frame and the Luminescent cases; And at least by the light reflection box of forming at the bottom of light reflecting device, light reflection box frame and the light reflection box, Luminescent cases and light reflection box is connected, it is characterized in that end face at the bottom of the described Luminescent cases and bottom surface at least mirror image be symmetrically arranged with the installation position of mounting light emitting device and Luminescent cases frame;
End face at the bottom of the described light reflection box and bottom surface mirror image at least are symmetrically arranged with the installation position that light reflecting device and light reflection box frame are installed.
2. a kind of monochromator according to claim 1 is characterized in that described light reflecting device comprises light-management members and the light partition member that will cut apart in proportion through the light that light-management members is handled;
Described light reflection box frame comprises the first box frame and the second box frame that is connected with the first box frame, described light-management members is positioned at the first box frame, the light partition member is positioned at the second box frame, and the described second box frame is provided with reception and disperses end through optical receiving end and the dispersion of the light of light-management members processing through the light of the light of light partition member processing.
3. a kind of monochromator according to claim 2 is characterized in that the side of described smooth partition member is provided with the light entrance port relative with the described second box frame optical receiving end, and disperses the relative light of end to divide raw edge with the described second box frame light; Be provided with in the described smooth partition member light is injected through described smooth entrance port, and cut apart mirror from the light that light divides raw edge to penetrate.
4. a kind of monochromator according to claim 3 is characterized in that described light disperses end to comprise that light transmission end and light reflection end, described light divide raw edge to comprise light-transmissive port and light reflex port, and it is semi-permeable and semi-reflecting mirror that described light is cut apart mirror.
5. a kind of monochromator according to claim 3 is characterized in that the light partition member is a cavity; Described light disperses end to comprise light transmission end and light reflection end; Described light disperses end to exist with the form of light dispersion hole, and described smooth dispersion hole comprises light beam orifice and cavity hatch bore, perhaps light reflection hole and cavity hatch bore; It is semi-permeable and semi-reflecting mirror that described light is cut apart mirror.
6. a kind of monochromator according to claim 2, it is characterized in that described light-management members comprises light-reflecting components and the grating that the light through the light-reflecting components reflection is screened, described grating comprises grating body and grating seat, and described grating body is installed on the grating seat;
Described light reflection box also comprises the Vidacare corp that drives the rotation of grating seat, described Vidacare corp comprises screw mandrel, guide rod, is arranged on screw mandrel and the guide rod, with the rotation of screw mandrel at mobile walking slide block, lever arm, the grating seat rotating shaft that is connected with the grating seat of screw mandrel and guide rod and the drive motor that is connected with screw mandrel one end;
One end of lever arm is connected with the rotating shaft of grating seat, and the end of the lever arm other end is the contact block that contacts with the walking slide block, establishes resilient torsion spring in the rotating shaft of described grating seat.
7. a kind of monochromator according to claim 6, it is characterized in that described Vidacare corp also comprises potentiometer, control circuit and display screen, described screw mandrel is connected by gear set with potentiometer with respect to the end that drive motor connects, potentiometer is connected with display screen by control circuit, and drive motor is connected with control circuit.
8. a kind of monochromator according to claim 2, it is characterized in that described light-management members comprises light-reflecting components and the grating that the light through the light-reflecting components reflection is screened, described grating comprises grating body and grating seat, and described grating body is installed on the grating seat;
Described light reflection box also comprises and drives the manual driving device that the grating seat rotates, and described manual driving device comprises the rotating disk that is connected with the rotating shaft of grating seat, be located in the manual dish at the bottom of the described light reflection box box and the driving-belt that is surrounded on rotating disk and manually coils.
9. a kind of monochromator according to claim 8 is characterized in that manually being carved with wave length calibration on the dish, manually coils a side and is provided with wave length calibration indicator dog on installing at the bottom of the described light reflection box box.
10. a kind of monochromator according to claim 2, it is characterized in that the first crack sheet that described light reflection box and the junction of Luminescent cases are provided with first light hole and are made up of the first printing opacity crack part relative with first light hole and first shading light part, the width of described first printing opacity crack part is smaller or equal to the first light hole width.
11. a kind of monochromator according to claim 10, it is characterized in that described light reflection box also comprises first driving mechanism of the mobile first crack sheet, first driving mechanism comprises first screw mandrel, first guide rod and the first crack sheet motor that is set in parallel in the light reflection box frame, the described first crack sheet is installed in respectively on first screw mandrel and first guide rod by first feed screw nut and first guide rod hole that is arranged on the first crack sheet, and second screw mandrel, one end is connected with the first crack sheet motor output shaft.
12. a kind of monochromator according to claim 2, it is characterized in that described light disperses end to be the light dispersion hole, described light reflection box is provided with the second crack sheet of being made up of the second printing opacity crack part relative with the light dispersion hole and second shading light part, and the width of described second printing opacity crack part is smaller or equal to light dispersion hole width.
13. a kind of monochromator according to claim 12, it is characterized in that described light reflection box also comprises second driving mechanism of the mobile second crack sheet, second driving mechanism comprises second screw mandrel, second guide rod and the second crack sheet motor that is set in parallel in the light reflection box frame, the described second crack sheet is installed in respectively on second screw mandrel and second guide rod by second feed screw nut and second guide rod hole that is arranged on the second crack sheet, and an end of described second screw mandrel is connected with the output shaft of the described second crack sheet motor.
CN 201010249947 2010-08-10 2010-08-10 Monochrometer Expired - Fee Related CN102374898B (en)

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