CN102359019A - Fibroin reinforcing method for fragile silk cultural relic - Google Patents
Fibroin reinforcing method for fragile silk cultural relic Download PDFInfo
- Publication number
- CN102359019A CN102359019A CN2011102379131A CN201110237913A CN102359019A CN 102359019 A CN102359019 A CN 102359019A CN 2011102379131 A CN2011102379131 A CN 2011102379131A CN 201110237913 A CN201110237913 A CN 201110237913A CN 102359019 A CN102359019 A CN 102359019A
- Authority
- CN
- China
- Prior art keywords
- fragile
- silk
- cultural relic
- historical relic
- fibroin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 108010022355 Fibroins Proteins 0.000 title claims abstract description 16
- 238000000034 method Methods 0.000 title claims abstract description 12
- 230000003014 reinforcing effect Effects 0.000 title abstract description 6
- KDXKERNSBIXSRK-UHFFFAOYSA-N Lysine Natural products NCCCCC(N)C(O)=O KDXKERNSBIXSRK-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000004472 Lysine Substances 0.000 claims abstract description 9
- HNDVDQJCIGZPNO-UHFFFAOYSA-N histidine Natural products OC(=O)C(N)CC1=CN=CN1 HNDVDQJCIGZPNO-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000000243 solution Substances 0.000 claims description 10
- 238000005728 strengthening Methods 0.000 claims description 8
- 239000012460 protein solution Substances 0.000 claims description 5
- 239000000463 material Substances 0.000 abstract description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 3
- 238000001035 drying Methods 0.000 abstract 1
- 239000012779 reinforcing material Substances 0.000 abstract 1
- 230000002787 reinforcement Effects 0.000 description 5
- 238000011160 research Methods 0.000 description 2
- 230000032683 aging Effects 0.000 description 1
- 239000003431 cross linking reagent Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
Landscapes
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
A fibroin reinforcing method for fragile silk cultural relics is characterized by comprising the following steps of: A) sprinkling fibroin solution with a mass percentage concentration of 0.01-0.1% on a surface of a fragile silk cultural relic uniformly until the fragile cultural relic until water drops from the fragile silk cultural relic; B) 10 min after completion of the step A), sprinkling a lysine solution with a mass percentage concentration of 0.1-2% on the surface of the fragile cultural relic until the fragile cultural relic until water drops from the fragile silk cultural relic; C) 10 min after completion of the step B), sprinkling a histidine solution with a mass percentage concentration of 0.1-2% on the surface of the fragile cultural relic until the fragile cultural relic until water drops from the fragile silk cultural relic and carrying out natural drying, so as to reinforce the fragile cultural relic. Compared with a prior art, the invention has advantages of 1) simple operation; 2) little influence caused by the reinforcing due to usage of reinforcing materials of fibroin, lysine and histidine and without other material.
Description
Technical field
What the present invention relates to is a kind of silk historical relic's protection method, particularly a kind of silk-fibroin method for strengthening of fragile silk historical relic.
Background technology
Silk is one of important symbol of Chinese civilization, and the silk historical relic is Ancient Times in China working people crystallization of wisdom especially, has very high scientific value, artistic value, historical value.Yet silk is a kind of natural hmw protein, and many silk historical relics seem intact, bright in colour when being unearthed, but in fact interior with the external acting in conjunction that waits various factors under, serious aging, embrittlement.How the silk historical relic that is on the verge of to damage is carried out effective reinforcement protection and handle, the reinforcement protection new method of research and development silk historical relic is urgent a, important research project of departments in charge of cultural and historical relics.
The silk-fibroin reinforcing project of being cooperated with the China Silk Museum by Institutes Of Technology Of Zhejiang has been developed fibroin albumen and has been reinforced the research of fragile silk goods, and obtains remarkable achievement.But people expect that also the reinforcement means that does not need crosslinking agent is arranged.
Summary of the invention
The object of the present invention is to provide a kind of silk-fibroin method for strengthening of fragile silk historical relic, select for use silk-fibroin and lysine, histidine, make reinforcing littler the influence of historical relic as reinforcement material.Outstanding advantage of the present invention is convenient, fast.
A kind of silk-fibroin method for strengthening of fragile silk historical relic is characterized in that adopting following steps:
A) be that 0.01～1% silk protein solution is sprayed on the fragile silk cultural artifact surface equably with mass percentage concentration, squirt till the fragile silk historical relic drips;
B) completing steps A) behind the 10min, be that 0.1%～2% lysine solution is sprayed on the fragile silk cultural artifact surface equably, squirt till the fragile silk historical relic drips mass percentage concentration;
C) completing steps B) behind the 10min, be that 0.1%～2% histidine solution is sprayed on the fragile silk cultural artifact surface equably, squirt till the fragile silk historical relic drips mass percentage concentration, air dry, the fragile silk historical relic obtains to reinforce.
Compare with prior art, advantage of the present invention is: 1) easy to operate; 2) reinforcement material does not have other material except that silk-fibroin and lysine, histidine, makes reinforcing littler to the influence of historical relic.
The specific embodiment
Embodiment 1:
A kind of silk-fibroin method for strengthening of fragile silk historical relic is characterized in that adopting following steps:
A) be that 0.01% silk protein solution is sprayed on the fragile silk cultural artifact surface equably with mass percentage concentration, squirt till the fragile silk historical relic drips;
B) completing steps A) behind the 10min, be that 2% lysine solution is sprayed on the fragile silk cultural artifact surface equably, squirt till the fragile silk historical relic drips mass percentage concentration;
C) completing steps B) behind the 10min, be that 0.1% histidine solution is sprayed on the fragile silk cultural artifact surface equably, squirt till the fragile silk historical relic drips mass percentage concentration, air dry, the fragile silk historical relic obtains to reinforce.
Embodiment 2:
A kind of silk-fibroin method for strengthening of fragile silk historical relic is characterized in that adopting following steps:
A) be that 1% silk protein solution is sprayed on the fragile silk cultural artifact surface equably with mass percentage concentration, squirt till the fragile silk historical relic drips;
B) completing steps A) behind the 10min, be that 0.01% lysine solution is sprayed on the fragile silk cultural artifact surface equably, squirt till the fragile silk historical relic drips mass percentage concentration;
C) completing steps B) behind the 10min, be that 2% histidine solution is sprayed on the fragile silk cultural artifact surface equably, squirt till the fragile silk historical relic drips mass percentage concentration, air dry, the fragile silk historical relic obtains to reinforce.
Embodiment 3:
A kind of silk-fibroin method for strengthening of fragile silk historical relic is characterized in that adopting following steps:
A) be that 0.5% silk protein solution is sprayed on the fragile silk cultural artifact surface equably with mass percentage concentration, squirt till the fragile silk historical relic drips;
B) completing steps A) behind the 10min, be that 1% lysine solution is sprayed on the fragile silk cultural artifact surface equably, squirt till the fragile silk historical relic drips mass percentage concentration;
C) completing steps B) behind the 10min, be that 1% histidine solution is sprayed on the fragile silk cultural artifact surface equably, squirt till the fragile silk historical relic drips mass percentage concentration, air dry, the fragile silk historical relic obtains to reinforce.
Claims (1)
1. the silk-fibroin method for strengthening of a fragile silk historical relic is characterized in that adopting following steps:
A) be that 0.01～1% silk protein solution is sprayed on the fragile silk cultural artifact surface equably with mass percentage concentration, squirt till the fragile silk historical relic drips;
B) completing steps A) behind the 10min, be that 0.1%～2% lysine solution is sprayed on the fragile silk cultural artifact surface equably, squirt till the fragile silk historical relic drips mass percentage concentration;
C) completing steps B) behind the 10min, be that 0.1%～2% histidine solution is sprayed on the fragile silk cultural artifact surface equably, squirt till the fragile silk historical relic drips mass percentage concentration, air dry, the fragile silk historical relic obtains to reinforce.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110237913 CN102359019B (en) | 2011-08-18 | 2011-08-18 | Fibroin reinforcing method for fragile silk cultural relic |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110237913 CN102359019B (en) | 2011-08-18 | 2011-08-18 | Fibroin reinforcing method for fragile silk cultural relic |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102359019A true CN102359019A (en) | 2012-02-22 |
| CN102359019B CN102359019B (en) | 2013-02-27 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201110237913 Expired - Fee Related CN102359019B (en) | 2011-08-18 | 2011-08-18 | Fibroin reinforcing method for fragile silk cultural relic |
Country Status (1)
| Country | Link |
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| CN (1) | CN102359019B (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104631119A (en) * | 2015-02-02 | 2015-05-20 | 浙江理工大学 | Catalytic reinforcement method for fragile silk fabric employing fibroinase |
| CN104631109A (en) * | 2015-02-02 | 2015-05-20 | 浙江理工大学 | Method for catalytic reinforcement of fragile silk fabric by employing aminoacidase |
| CN105671958A (en) * | 2016-01-21 | 2016-06-15 | 苏州纳百奥生物科技有限公司 | Reinforcing liquid and reinforcing method of antique silks and application of reinforcing liquid |
| CN107313253A (en) * | 2017-08-04 | 2017-11-03 | 浙江理工大学 | A kind of method for painting the reinforcing of class silk fabric cultural relics for fragile print |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101613937A (en) * | 2009-08-10 | 2009-12-30 | 浙江理工大学 | The bionical method for strengthening of silk-fibroin compound system of silk historical relic |
| CN101613938A (en) * | 2009-08-10 | 2009-12-30 | 浙江理工大学 | The preparation method of compound and biomimetic enhancing agent of silk protein of silk antiquity |
-
2011
- 2011-08-18 CN CN 201110237913 patent/CN102359019B/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101613937A (en) * | 2009-08-10 | 2009-12-30 | 浙江理工大学 | The bionical method for strengthening of silk-fibroin compound system of silk historical relic |
| CN101613938A (en) * | 2009-08-10 | 2009-12-30 | 浙江理工大学 | The preparation method of compound and biomimetic enhancing agent of silk protein of silk antiquity |
Non-Patent Citations (1)
| Title |
|---|
| 周旸等: "古代丝织品的丝素蛋白加固保护", 《文物保护与考古科学》 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104631119A (en) * | 2015-02-02 | 2015-05-20 | 浙江理工大学 | Catalytic reinforcement method for fragile silk fabric employing fibroinase |
| CN104631109A (en) * | 2015-02-02 | 2015-05-20 | 浙江理工大学 | Method for catalytic reinforcement of fragile silk fabric by employing aminoacidase |
| CN105671958A (en) * | 2016-01-21 | 2016-06-15 | 苏州纳百奥生物科技有限公司 | Reinforcing liquid and reinforcing method of antique silks and application of reinforcing liquid |
| CN105671958B (en) * | 2016-01-21 | 2017-11-28 | 苏州纳百奥生物科技有限公司 | The reinforcing liquid and reinforcement means of a kind of silk fabric cultural relics and application |
| CN107313253A (en) * | 2017-08-04 | 2017-11-03 | 浙江理工大学 | A kind of method for painting the reinforcing of class silk fabric cultural relics for fragile print |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102359019B (en) | 2013-02-27 |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20130227 Termination date: 20130818 |