CN102311721A - Formula and manufacturing method of low-temperature phase change ice storage tank - Google Patents
Formula and manufacturing method of low-temperature phase change ice storage tank Download PDFInfo
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- CN102311721A CN102311721A CN201110153624A CN201110153624A CN102311721A CN 102311721 A CN102311721 A CN 102311721A CN 201110153624 A CN201110153624 A CN 201110153624A CN 201110153624 A CN201110153624 A CN 201110153624A CN 102311721 A CN102311721 A CN 102311721A
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Abstract
The invention discloses a formula of a low-temperature phase change ice storage tank. The formula comprises the following components in percentage by weight: 10-30% of polyvinyl alcohol, 2-8% of sodium carboxymethylcellulose (CMCNa), 1-5% of polyacrylamide, 1-5% of sodium tetraborate and the balance of distilled water, wherein the sum of the weight percents of the components is 100%. The invention also discloses a manufacturing method of the low-temperature phase change ice storage tank. The method comprises the following steps of: heating the distilled water, adding polyvinyl alcohol in a corresponding proportion, and stirring until polyvinyl alcohol is dissolved; then adding sodium carboxymethylcellulose (CMCNa) and polyacrylamide, and evenly stirring and reacting; and then heating the mixed solution, adding polyacrylamide and stirring; and finally making a raw material case, and packaging to form the ice storage tank. The ice storage tank is equivalent to a storage battery, and the heat (cold) insulation effect of the ice storage tank can be enhanced on the whole, thus the ice-cooling time of the ice storage tank is prolonged.
Description
Technical field
The present invention discloses a kind of low temperature phase change ice bank prescription and preparation method thereof, belongs to cold-storage technology category, relates in particular to a kind of low temperature phase change ice bank, applicable to the commerce refrigeration and the fields such as medicine refrigeration and Cold Chain Logistics of beverage/food.
Background technology
Cold Chain Logistics general reference refrigerating class article are being produced, are being preserved transportation, selling; All the time be under the low temperature environment of regulation to consuming in each preceding link; To guarantee a systems engineering of article quality and performance, be to be the basis, to be the low temperature logistics process of means with the Refrigeration Technique with refrigerating process.Cold-storage apparatus has and keeps effect iced, fresh-keeping, that refrigerate, is that Cold Chain Logistics is transported and one of refrigeration instrument out of doors.
The inventor creates a new type low temperature phase transformation " ice bank " through being engaged in the Cold Chain Logistics many years of experience and combining the technological characteristics of cold-storage, is equivalent to＜store battery＞effect, so just there is the present invention to propose.
Summary of the invention
To the deficiency of prior art, the invention provides effective, safe and reliable low temperature phase change ice bank prescription of a kind of cold-storage and preparation method thereof.
For achieving the above object, the present invention realizes through following technical scheme:
A kind of low temperature phase change ice bank comprises following each component of the meter of mark by weight: Z 150PH 10～30%, and Xylo-Mucine (CMCNa) 2～8%, SEPIGEL 305 1～5%, sodium tetraborate 1～5%, surplus zero(ppm) water adds to 100%.
The making method of above-mentioned low temperature phase change ice bank comprises the steps:
One, zero(ppm) water is heated to 65～100 ℃, the Z 150PH of adding 10～30% is stirred to dissolving, preferred 65～75 ℃;
Two, 2～8% Xylo-Mucine CMCNa and 1～5% SEPIGEL 305 are joined in the above-mentioned solution stir;
Three, more than the above-mentioned mixed solution reaction 10min, preferred 10～15min;
Four, add 1～5% SEPIGEL 305 during heating mixed solution to 50～100 ℃, stir more than the 10min;
Five, will resist the low temperature material to adopt blow molding process to process the above-mentioned raw materials outer cover packaging and form ice bank, wherein said anti-low temperature material is PE, PET or metal or non-metallic material.
The present invention is through the ice bank of above-mentioned raw materials and prepared; Sturdy and durable, effect is equivalent to ' store battery ', can strengthen insulation (cold) effect of ice bank on the whole; Thereby prolonged its ice-cold time; Especially be fit to carry, transport all kinds of chilled goods or medicine under the outdoor non-transformer situation, can use separately or cooperate refrigerator car, have advantages such as safe and reliable, that the cold-storage effect is good.
Embodiment
Embodiment 1: a kind of low temperature phase change ice bank comprises following each component of the meter of mark by weight: Z 150PH 10%, and Xylo-Mucine (CMCNa) 2%, SEPIGEL 305 1%, sodium tetraborate 1%, surplus zero(ppm) water adds to 100%.
The making method of above-mentioned low temperature phase change ice bank comprises the steps:
One, zero(ppm) water is heated to 65～100 ℃, the Z 150PH of adding 10% is stirred to dissolving, preferred 65～75 ℃;
Two, 2% Xylo-Mucine CMCNa and 1% SEPIGEL 305 are joined in the above-mentioned solution stir;
Three, more than the above-mentioned mixed solution reaction 10min, preferred 10～15min;
Four, add 1% SEPIGEL 305 during heating mixed solution to 50～100 ℃, stir more than the 10min, preferably about 15 minutes;
Five, will resist the low temperature material to adopt blow molding process to process the above-mentioned raw materials outer cover packaging and form ice bank, wherein said anti-low temperature material is PE, PET or metal or non-metallic material.
Embodiment 2: a kind of low temperature phase change ice bank comprises following each component of the meter of mark by weight: Z 150PH 30%, and Xylo-Mucine (CMCNa) 8%, SEPIGEL 305 5%, sodium tetraborate 5%, surplus zero(ppm) water adds to 100%.
The making method of above-mentioned low temperature phase change ice bank with embodiment 1, repeats no more at this.
Embodiment 3: a kind of low temperature phase change ice bank comprises following each component of the meter of mark by weight: Z 150PH 20%, and Xylo-Mucine (CMCNa) 6%, SEPIGEL 305 4%, sodium tetraborate 3%, surplus zero(ppm) water adds to 100%.
The making method of above-mentioned low temperature phase change ice bank with embodiment 1, repeats no more at this.
Embodiment 4: a kind of low temperature phase change ice bank comprises following each component of the meter of mark by weight: Z 150PH 15%, and Xylo-Mucine (CMCNa) 4%, SEPIGEL 305 3%, sodium tetraborate 4%, surplus zero(ppm) water adds to 100%.
The making method of above-mentioned low temperature phase change ice bank with embodiment 1, repeats no more at this.
Embodiment 5: a kind of low temperature phase change ice bank comprises following each component of the meter of mark by weight: Z 150PH 25%, and Xylo-Mucine (CMCNa) 5%, SEPIGEL 305 2%, sodium tetraborate 3%, surplus zero(ppm) water adds to 100%.
The making method of above-mentioned low temperature phase change ice bank with embodiment 1, repeats no more at this.
The above record is merely the embodiment that utilizes this origination techniques content, anyly is familiar with modification, the variation that this creation of this art utilization is done, and all belongs to the claim of this creation opinion, and is not limited to embodiment announcement person.
Claims (5)
1. a low temperature phase change ice bank comprises following component, and each component is the mark meter by weight: Z 150PH 10～30%, and Xylo-Mucine CMCNa2～8%, SEPIGEL 305 1～5%, sodium tetraborate 1～5%, surplus zero(ppm) water adds to 100%.
2. the making method of claim 1 low temperature phase change ice bank comprises the steps:
One, zero(ppm) water is heated to 65～100 ℃, the Z 150PH of adding 10～30% is stirred to dissolving;
Two, 2～8% Xylo-Mucine CMCNa and 1～5% SEPIGEL 305 are joined in the above-mentioned solution stir;
Three, more than the above-mentioned mixed solution reaction 10min;
Four, add 1～5% SEPIGEL 305 during heating mixed solution to 50～100 ℃, stir more than the 10min;
Five, will resist the low temperature material to adopt blow molding process to process the above-mentioned raw materials outer cover packaging and form ice bank.
3. the making method of the described low temperature phase change ice bank of claim 2, it is characterized in that: described anti-low temperature material is PE, PET or metal or non-metallic material.
4. the making method of the described low temperature phase change ice bank of claim 2 is characterized in that: the zero(ppm) water described in the step 1 is heated to 65～75 ℃ of Z 150PH and dissolvings of adding corresponding proportionings.
5. the making method of the described low temperature phase change ice bank of claim 2 is characterized in that: mixed solution reaction 10～15min in the step 3.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201110153624A CN102311721A (en) | 2011-06-09 | 2011-06-09 | Formula and manufacturing method of low-temperature phase change ice storage tank |
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| CN201110153624A CN102311721A (en) | 2011-06-09 | 2011-06-09 | Formula and manufacturing method of low-temperature phase change ice storage tank |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102925116A (en) * | 2012-11-08 | 2013-02-13 | 沈阳建筑大学 | Fin-shaped phase change energy storage module |
| CN103194177A (en) * | 2013-03-26 | 2013-07-10 | 杭州普济医药技术开发有限公司 | Manufacturing method of ice bag for preserving biological products |
| CN103486793A (en) * | 2013-10-11 | 2014-01-01 | 崔德顺 | Production process of low temperature phase change cold accumulation ice box or ice bag |
| CN103725258A (en) * | 2013-12-16 | 2014-04-16 | 苏州安特实业有限公司 | Macromolecule coolant and preparation method thereof |
| CN103725260A (en) * | 2013-12-16 | 2014-04-16 | 苏州安特实业有限公司 | Coolant with good cold storage effect and long freezing time and preparation method thereof |
| CN103710003B (en) * | 2014-01-08 | 2016-06-01 | 黑龙江工程学院 | A kind of Low-temperature polymer-base phase change energy storage material and its preparation method |
| CN110129007A (en) * | 2019-05-20 | 2019-08-16 | 戴小红 | A kind of efficient stable cold-storage material |
| CN112852387A (en) * | 2021-02-23 | 2021-05-28 | 全球能源互联网研究院有限公司 | Phase change material and preparation method and application thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1101066A (en) * | 1993-09-29 | 1995-04-05 | 康来明 | Soft ice and preparation method |
| CN101921578A (en) * | 2009-06-10 | 2010-12-22 | 陆建新 | Coolant |
| CN101928550A (en) * | 2009-06-22 | 2010-12-29 | 林海英 | Ice bag of refrigerator |
-
2011
- 2011-06-09 CN CN201110153624A patent/CN102311721A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1101066A (en) * | 1993-09-29 | 1995-04-05 | 康来明 | Soft ice and preparation method |
| CN101921578A (en) * | 2009-06-10 | 2010-12-22 | 陆建新 | Coolant |
| CN101928550A (en) * | 2009-06-22 | 2010-12-29 | 林海英 | Ice bag of refrigerator |
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102925116A (en) * | 2012-11-08 | 2013-02-13 | 沈阳建筑大学 | Fin-shaped phase change energy storage module |
| CN102925116B (en) * | 2012-11-08 | 2015-09-09 | 沈阳建筑大学 | Rib-type phase-change accumulation energy module |
| CN103194177A (en) * | 2013-03-26 | 2013-07-10 | 杭州普济医药技术开发有限公司 | Manufacturing method of ice bag for preserving biological products |
| CN103194177B (en) * | 2013-03-26 | 2016-01-06 | 杭州普济医药技术开发有限公司 | For the manufacture method of the ice bag of preservation biological products |
| CN103486793A (en) * | 2013-10-11 | 2014-01-01 | 崔德顺 | Production process of low temperature phase change cold accumulation ice box or ice bag |
| CN103725258A (en) * | 2013-12-16 | 2014-04-16 | 苏州安特实业有限公司 | Macromolecule coolant and preparation method thereof |
| CN103725260A (en) * | 2013-12-16 | 2014-04-16 | 苏州安特实业有限公司 | Coolant with good cold storage effect and long freezing time and preparation method thereof |
| CN103725258B (en) * | 2013-12-16 | 2016-09-14 | 苏州安特实业有限公司 | A kind of Macromolecule coolant and preparation method thereof |
| CN103710003B (en) * | 2014-01-08 | 2016-06-01 | 黑龙江工程学院 | A kind of Low-temperature polymer-base phase change energy storage material and its preparation method |
| CN110129007A (en) * | 2019-05-20 | 2019-08-16 | 戴小红 | A kind of efficient stable cold-storage material |
| CN112852387A (en) * | 2021-02-23 | 2021-05-28 | 全球能源互联网研究院有限公司 | Phase change material and preparation method and application thereof |
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Application publication date: 20120111 |