CN102250684B - Treatment method before decolorizing in oil processing technique - Google Patents

Treatment method before decolorizing in oil processing technique Download PDF

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Publication number
CN102250684B
CN102250684B CN 201110161811 CN201110161811A CN102250684B CN 102250684 B CN102250684 B CN 102250684B CN 201110161811 CN201110161811 CN 201110161811 CN 201110161811 A CN201110161811 A CN 201110161811A CN 102250684 B CN102250684 B CN 102250684B
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China
Prior art keywords
oil
crude oil
decolorizing
enter
decolouring
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Expired - Fee Related
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CN 201110161811
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Chinese (zh)
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CN102250684A (en
Inventor
彭华
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HUNAN YINGCHENG GREASE INDUSTRY CO LTD
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HUNAN YINGCHENG GREASE INDUSTRY CO LTD
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Publication of CN102250684A publication Critical patent/CN102250684A/en
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Abstract

In order to overcome the problems that because the oil temperature is too low before decolorizing, the oil color is too deep, thus the production process is not continuous in the prior art, the invention provides a new treatment method before decolorizing by making full use of the existing equipment and pipelines and improving a decolorizing pipeline. The treatment method comprises the steps of: enabling crude oil to pass through a heater for heating, then premixing, enabling the pre-mixed crude oil to enter a decolorizing tower for decolorizing, enabling a part of the decolorized crude oil to enter a condenser for condensing and collecting the crude oil, and enabling the other part of the decolorized crude oil to enter a circulating pipeline for decolorizing again, wherein before the crude oil is decolorized, the oil in the circulating pipeline is conveyed to the heater to be heated for a period of time. By the treatment method, the oil temperature reaches a normal level before decolorizing, thereby maintaining continuous production.

Description

A kind for the treatment of method before decolorizing in oil processing technique
Technical field
The present invention relates to a kind of grease processing technique, a kind for the treatment of process before particularly the bleaching process in grease processing technique begins.
Background technology
At present, at the food oils production field, its production method generally all is to squeeze first, and extraction, operations such as decolouring, deodorization then are a kind of comparatively edible fat production technique of maturation again.But in present production technique, particularly in bleaching process, when the workshop stops to produce at every turn, oil is behind thorough circulation cleaning in the decolorization filtering machine, most of oil all must enter bleaching tower by the circulating line back-pressure to be treated to refilter when starting shooting next time, has certain low temperature oily thereby caused when each start is produced in the bleaching tower.When next time, start was produced, because the low temperature oil in the bleaching tower can not heat temperature raising, and the green oil temperature that enters in the bleaching tower is not high yet, after the former low temperature oil of depositing mixes, decolouring oil temperature to be filtered is lower, only have about 80 ℃, and the normal filtration oil temperature needs about 110 ℃, so carclazyte and separating of oil difficult when causing filter to filter, in the filter oil with micro-carclazyte, and micro-carclazyte can not enter subsequent processing in the oil, can only enter bleaching tower and continue circulation, and do not have heating unit in the bleaching tower, so whole filtration treats that limpid the expending time in of oil quite grow (4 to 5 hours) to such an extent as to oil is not in time exported, affect a upper operation alkali refining oil and can not input and be forced to stop a upper operation production.Owing to relating in the bleaching tower, technique can not add carclazyte again, must add by premixing tank, and after the filter filtration all there be not directly into the premixing tank pipeline all output channels, product control sampling is again at filter edible vegetable oil delivery port (seeing Fig. 1), but chemical examination check bleached oil color and luster is excessively dark, the dark oil of color and luster enters lower operation and just causes lower operation oil defective, does not enter lower operation and just can only enter the bleaching tower circulation.It is modified directly to add carclazyte at the tower internal recycle, also just can not solve its root problem, enters at last slops behind the deodorizing tower, has namely polluted deodorizing tower and has entered again again freshening of crude oil tank, greatly reduces production capacity, has increased production cost.
Summary of the invention
The present invention is excessively low for oil temperature before overcoming the decolouring that exists in the prior art, make the oil colours pool excessively dark, cause the problem that production process can not be continuous, by taking full advantage of existing installation, pipeline, the decolouring pipeline is improved, propose a kind of new front treatment process of decolouring, make the front oil temperature of decolouring reach normal level, keep producing continuously.
The present invention adopts following method to realize:
A kind for the treatment of method before decolorizing in oil processing technique, comprise and carry out premix after crude oil is by heater heats, decolour through entering bleaching tower behind the premix, enter condenser condenses through the decolouring rear portion and collect crude oil, a part enters circulating line and again decolours, when wherein decolouring, first the grease in the circulating line is transported to well heater and heats operation for some time.
Above-mentioned treatment method before decolorizing in oil processing technique, wherein circulating line is connected with the device for cleaning pipeline piping that enters before the well heater, when decolouring, make first connecting tube open-minded, making crude oil in the circulating line enter well heater heats, after heating operation for some time, connecting tube is closed, enter bleaching process.
Above-mentioned treatment method before decolorizing in oil processing technique wherein adopts opening and closing of control ball valve control linkage pipeline.
Adopt method of the present invention, killing two birds with one stone has solved the bleached oil oil temperature and has crossed low heating, and two problems of dark freshening are crossed in the oil colours pool, have satisfied the requirement of decolouring continuous production processes.Each start bleached oil enters filter to fuel-displaced limpid need of filter 1 hour, and the decolouring color and luster is crossed and deeply can in time be returned premixing tank and add the carclazyte freshening that again decolours, and falls color and luster and makes it to reach processing requirement, has greatly improved production efficiency, reduced production cost, convenient and practical.
Description of drawings
Fig. 1 is embodiment 1 described existing bleaching process schema in the treatment method before decolorizing in oil processing technique of the present invention, and 1 is well heater among the figure, and 2 is premixed device, and 3 is bleaching tower, and 4 is condenser;
Fig. 2 is the bleaching process schema after the embodiment 1 described improvement in the treatment method before decolorizing in oil processing technique of the present invention, and 1 is well heater among the figure, and 2 is premixed device, 3 is bleaching tower, and 4 is condenser, and 5 is circulating line, 6 for installing pipeline additional, and 7 and 8 are the control ball valve.
Embodiment
Embodiment 1
In the existing grease production technique about the decolouring general operation as shown in Figure 1, crude oil at first carries out premix through entering premixed device 2 after well heater 1 heating, decolour through entering bleaching tower 3 behind the premix, enter condenser 4 condensations through the decolouring rear portion and collect crude oil, a part enters circulating line 5 and again decolours.Now with circulating line 5 and enter device for cleaning pipeline before the well heater 1 and cross and install pipeline 6 additional and is connected, and install 7 controls of control ball valve additional and install opening or closing of pipeline 6 additional installing pipeline 6 additional, install additional at the bleaching tower flowline simultaneously and control ball valve 8, as shown in Figure 2.
Now adopt vegetable seed as raw material production rape oil, when decolouring program, first crude oil is heated, by well heater 1 the crude oil temperature is increased to 110 ℃.Then the ratio that with crude oil and the carclazyte of heating according to weight ratio is 1: 0.02 is mixed in premixed device 2, the premixed time is 8 minutes, entering bleaching tower 3 after the mixing decolours, then filter, get the decolouring oil sample and put into cell (133.4mm), measure by the Lovibond photoelectric color comparator, color colourity is R8.6, greater than R7.0, be substandard product.At this moment will control ball valve 7 and be in opening state, simultaneously the closing control ball valve 8, make in the pipeline crude oil enter well heater 1 and heat, and so circular flow is until product is qualified.After the product detection was qualified, closing control ball valve 7 was also opened control ball valve 8, formally enters bleaching process.
Embodiment 2
Now adopt cottonseed as raw material production rape oil, when decolouring program, first crude oil is heated, by well heater 1 the crude oil temperature is increased to 110 ℃.Then the ratio that with crude oil and the carclazyte of heating according to weight ratio is 1: 0.03 is mixed in premixed device 2, the premixed time is 8 minutes, entering bleaching tower 3 after the mixing decolours, then filter, get the decolouring oil sample and put into cell (133.4mm), measure by the Lovibond photoelectric color comparator, color colourity is R5.1, greater than R4.0, be substandard product.At this moment will control ball valve 7 and be in opening state, simultaneously the closing control ball valve 8, make in the pipeline crude oil enter well heater 1 and heat, and so circular flow is until product is qualified.After the product detection was qualified, closing control ball valve 7 was also opened control ball valve 8, formally enters bleaching process.

Claims (1)

1. treatment method before decolorizing in oil processing technique, comprise and carry out premix after crude oil is by heater heats, decolour through entering bleaching tower behind the premix, enter condenser condenses through the decolouring rear portion and collect crude oil, a part enters circulating line and again decolours, when it is characterized in that decolouring, first the grease in the circulating line is transported to well heater and heats operation for some time;
Above-mentioned fat processing method, wherein circulating line is connected with the device for cleaning pipeline piping that enters before the well heater, when decolouring, make first connecting tube open-minded, making crude oil in the circulating line enter well heater heats, after heating operation for some time, connecting tube is closed, enter bleaching process;
Above-mentioned fat processing method wherein adopts opening and closing of control ball valve control linkage pipeline;
Above-mentioned fat processing method when wherein decolouring, is transported to well heater with the grease in the circulating line first and heats, and reaches 110 ℃ to oil temperature.
CN 201110161811 2011-06-16 2011-06-16 Treatment method before decolorizing in oil processing technique Expired - Fee Related CN102250684B (en)

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Application Number Priority Date Filing Date Title
CN 201110161811 CN102250684B (en) 2011-06-16 2011-06-16 Treatment method before decolorizing in oil processing technique

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CN102250684A CN102250684A (en) 2011-11-23
CN102250684B true CN102250684B (en) 2013-10-16

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107308696B (en) * 2017-07-14 2022-10-28 浙江敦豪斯五金工业有限公司 Oil product continuous decoloring system and method

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201669081U (en) * 2010-04-23 2010-12-15 新疆金鑫生物科技发展有限公司 Heating stirring and mixing control device

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201669081U (en) * 2010-04-23 2010-12-15 新疆金鑫生物科技发展有限公司 Heating stirring and mixing control device

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
何东平.油脂精炼与加工工艺学.《油脂精炼与加工工艺学》.北京:化学工业出版社,2005,(第一版), *
王宏健,赵宇.一种新的油脂脱色工艺——预脱色与电子过滤.《中国油脂》.1999,第24卷(第5期), *
马传国.油脂加工工艺与设备.《油脂加工工艺与设备》.化学工业出版社,2004,(第一版), *

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