CN102243160B - Method for detecting suction resistance of cigar - Google Patents

Method for detecting suction resistance of cigar Download PDF

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CN102243160B
CN102243160B CN 201110108836 CN201110108836A CN102243160B CN 102243160 B CN102243160 B CN 102243160B CN 201110108836 CN201110108836 CN 201110108836 CN 201110108836 A CN201110108836 A CN 201110108836A CN 102243160 B CN102243160 B CN 102243160B
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cigar
sample
measuring head
resistance
suction
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CN102243160A (en
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陈欢
庞永强
姜兴益
陈再根
唐纲岭
周德成
闪红光
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Zhengzhou Tobacco Research Institute of CNTC
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Zhengzhou Tobacco Research Institute of CNTC
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Abstract

The invention provides a method for detecting suction resistance of a cigar, which can accurately detect the suction resistance of a cigar without destruction and is suitable for detecting cigar samples in different appearance specifications. The invention also provides a method for calculating air flow rate in the suction resistance detection process. The method for detecting the suction resistance of a cigar is characterized by comprising the following steps: a, preparing a cigar sample; b, preparing a cigar test head; c, calculating the air flow rate; and d, detecting the suction resistance of the cigar. By using the method, related operations for suction resistance detection of the cigar are specified, and accuracy, repeatability and reproducibility of the suction resistance detecting results of the cigar are well guaranteed.

Description

Method for detecting suction resistance of cigar
Technical field
The present invention relates to cigar flue gas analysis technology, relate to specifically a kind of method for detecting suction resistance of cigar that is applicable to.
Background technology
When carrying out the cigar flue gas analysis, need to carry out in advance the mensuration of cigar resistance to suction.Therefore but in the prior art, still lack the assay method of cigar resistance to suction, set up that method for detecting suction resistance of cigar is extremely important concerning the cigar flue gas analysis accurately and reliably.But the profile specification limit of cigar is very wide, and length variations is approximately from 65 mm to 250 mm, weight change from less than 1 g to greater than 15 g, vary in diameter is approximately from 6 mm to 25 mm.The shape that cigar rolls is also very inconsistent, some near cylindrical, and some approximate circle tapers, especially the shape difference of cigar holder end is very large.Therefore, the assay method of cigar resistance to suction is different from the Cigarette Draw Resistance assay method, needs to set up the resistance to suction assay method of the cigar that is applicable to different form factors.In addition, the resistance to suction of cigarette is relevant with the air flow rate by cigarette, and when carrying out the cigar flue gas analysis, diameter regardless of cigar, should guarantee that all air-flow passes through the cigar xsect with the constant flow rate of 11.8 cm/s, therefore, when measuring the cigar resistance to suction, the air flow rate by cigar should calculate according to the diameter of cigar and set.
Summary of the invention
For the deficiencies in the prior art, the invention provides and a kind ofly can be applicable to the method for measuring of cigar resistance to suction.The method can be applicable to the resistance to suction of the cigar of different form factors and measure, and the computing method of air flow rate when providing resistance to suction to measure.
The objective of the invention is to be achieved through the following technical solutions: the assay method of cigar cigarette resistance to suction of the present invention may further comprise the steps:
The preparation of 1 cigar sample:
1.1 regulate the cigar sample:
Adjusting ambient is: temperature: 22 ℃ ± 1 ℃; Relative humidity: (60 ± 2) %; Atmospheric pressure: 96kPa ± 10kPa.The adjusting time is no less than 72 hours.
1.2 the cigar sample is carried out mark:
The cigar of mouth end sealing should excise mouth end 5 mm, and mark lengths does not comprise the part of excision.
Carry out mark with a soft head insertion depth (apart from cigar holder end 28 mm places) to cigar, be accurate to 0.5 mm.
The preparation of cigar measuring head:
Select the measuring head of corresponding size according to the diameter range of cigar.And according to the diameter of cigar apart from mouth end 15 mm places, emulsion tube sleeve, emulsion tube and sealing gasket in measuring head base and the measuring head are carried out optimal selection.Measuring head should coat cigarette 28 mm from the cigar stub is terminal, and flue gas composition and air are all had impenetrability, avoids leaking gas between cigar and the measuring head.
The setting of air flow rate:
Be 11.8 cm/s in order to keep the gas velocity by cigar cigarette xsect, diameter should be obtained apart from the diameter at mouth end 33 mm places according to cigar greater than the air flow rate of 12.0 mm cigars.The air flow rate that diameter is less than or equal to 12.0 mm cigars should be set as 800.0 mL/min.
The mensuration of cigar resistance to suction
4.1 test atmosphere
Temperature: 22 ℃ ± 2 ℃ relative humidity: (60 ± 5) %
4.2 the resistance to suction instrument is proofreaied and correct:
Before proper testing, should adopt Transfer Standards spare calibration, if temperature variation surpasses 2 ℃ or relative humidity variations surpasses 5%, all should recalibrate every day at least one times.
4.3 the diameter according to the cigar sample calculates and sets the corresponding air flow flow;
4.4 after measuring head is positioned over sense channel, with the zero clearing of resistance to suction value;
4.5 insert cigar sample to be measured, and the resistance to suction value of record sample.(degree of depth that cigar inserts measuring head is 28 mm)
The invention has the advantages that: can accurately, without damage measure the cigar resistance to suction, be applicable to the cigar sample tests of different form factors, and the computing method of air flow rate when providing resistance to suction to measure.This method standard the associative operation measured of cigar resistance to suction, ensured better accuracy, the Repeatability and Reproducibility of cigar resistance to suction measurement result.
Description of drawings
Fig. 1 is the structural representation of cigar measuring head among the present invention.(this measuring head is joined common components by smoking machine in the prior art)
Fig. 2 is measuring head understructure schematic diagram among Fig. 1.
Fig. 3 is cigarette retained part assembling explosive view among Fig. 1.
Among the figure: 1, measuring head base, 2, the cigarette retained part, 2-1, emulsion tube sleeve, 2-2, emulsion tube, 2-3, sealing gasket.
Embodiment
The concrete technological process of the present invention is described in further detail as follows:
The preparation of 1 cigar sample:
1.1 the adjusting of cigar sample:
1.1.1 Gas regulation:
Temperature: 22 ℃ ± 1 ℃ relative humidity: (60 ± 2) %
Annotate: atmospheric pressure should be within 96kPa ± 10kPa.Atmospheric pressure should be tested and be embodied in the test report.
1.1.2 the adjusting time
Under forced draft, the cigar balance needs 72 hours at least.
1.1.3 the check of balance
Meet the cigar sample of one of following condition, be considered to obtain balance:
A) in 24 h, the quality of cigar relatively variation is not more than 0.1%;
B) in cigar is placed on the closed container suitable with its volume, the relative humidity in this container is identical with the relative humidity of the Gas regulation of regulation.
1.2 cigarette mark
The cigar of mouth end sealing should excise mouth end 5 mm, and mark lengths does not comprise the part of excision.
Carry out mark with a soft head insertion depth (apart from cigar holder end 28 mm places) to cigar, be accurate to 0.5 mm.
Should avoid damaging cigarette during mark.The cigarette of accidental damage or labeling process find that defective cigarette should discard, and replace with cigarette for subsequent use.
The selection of cigar measuring head
When carrying out the cigar analysis, need to be according to the concrete suitable measuring head of apparent parameter assembling of cigar.Select emulsion tube sleeve, emulsion tube and sealing gasket in measuring head base and the measuring head according to cigar apart from the diameter at mouth end 15 mm places.As shown in Figure 1, the cigar measuring head comprises that the two large divisions forms: measuring head base portion and cigarette retained part.Figure 2 shows that measuring head base schematic diagram, as shown in Figure 2, the measuring head base only has two kinds of models to select, the difference of these two kinds of models is that the diameter with cigarette retained part junction is 26mm or 32mm, and the base of these two kinds of models is applicable to respectively the cigar that diameter range is 6.5 mm-16.49 mm and 16.5 mm-22.5 mm.Figure 3 shows that the part that is used for the cigarette clamping in the cigar measuring head.Because the size of cigar differs, therefore need according to the diameter of cigar emulsion tube sleeve and emulsion tube in the measuring head to be selected according to table 1, sealing gasket is selected according to cigar holder end shape by the operator, should avoid the fold of cigar, leaks gas in the test process preventing.The measuring head of standard should coat cigarette 28 mm from the cigar holder end, and flue gas composition and air are all had impenetrability, avoids leaking gas between cigar and the measuring head.
Figure 201110108836X100002DEST_PATH_IMAGE001
The setting of air flow rate
Be 11.8 cm/s in order to keep the gas velocity by the cigar xsect, diameter greater than the air flow rate of 12.0 mm cigars should according to cigar be obtained apart from the diameter at mouth end 33 mm places.Air flow rate is tried to achieve according to the diameter according to the form below 2. of cigar:
Table 2. is set the relation of air flow rate and cigar diameter
Cigar diameter x(mm) Air flow rate V (mL/min)
≤ 12.0 800.0
≥ 12.1 y= 5.56 * x 2
Wherein: air flow rate y is accurate to 0.1 mL/min; Diameter x is accurate to 0.1 mm
Annotate: formula [y=5.56 * x 2] be based on the principle of 11.8 cm/s constant flow rates
4. the mensuration of cigar resistance to suction:
4.1 test atmosphere:
Temperature: 22 ℃ ± 2 ℃ relative humidity: (60 ± 5) %
4.2 resistance absorbing instrument is proofreaied and correct:
Before proper testing, should adopt Transfer Standards spare calibration, if temperature variation surpasses 2 ℃ or relative humidity variations surpasses 5%, all should recalibrate every day at least one times.
4.2.1 pressure drop Transfer Standards spare is equilibrated to ambient air temperature;
4.2.2 adjust liquid level to zero graduation, insert standard component, after fluid column is stable, adjust flow controller until pressure drop shows the nominal value of Transfer Standards spare.
4.3 the diameter according to the cigar sample is set the corresponding air flow flow;
4.4 after measuring head is positioned over sense channel, with the zero clearing of resistance to suction value;
4.5 insert cigar sample to be measured, the degree of depth that cigar inserts measuring head is 28mm, the resistance to suction value of record sample;
Below in conjunction with embodiment assay method of the present invention is described further, but is not restriction the present invention.Adopt the present invention that the resistance to suction of three kinds of cigar samples is measured, measurement result is as shown in table 3.Wherein sample A and B are by hand and roll cigar, and the resistance to suction otherness is larger between the cigarette, and sample C is machine-processed cigar, therefore resistance to suction difference is less between the cigarette.
The resistance to suction test result of table 3. cigar sample A, B, C: (unit: mmWG)
Sample A Sample B Sample C
96 63 94
103 43 93
109 54 94
89 80 92
144 51 93
102 45 92
87 52 94
115 40 92

Claims (1)

1. one kind is applicable to the method for measuring of cigar resistance to suction, it is characterized in that: comprise following determination step:
A. the preparation of cigar sample:
Regulate the cigar sample, and carry out the cigarette mark,
The adjusting ambient of regulating the cigar sample is: temperature: 22 ℃ ± 1 ℃; Relative humidity: (60 ± 2) %; Atmospheric pressure: 96kPa ± 10kPa, the adjusting time is no less than 72 hours;
When the cigar sample was carried out mark, the cigar of mouth end sealing should excise mouth end 5 mm, and mark lengths does not comprise the part of excision, with a soft head insertion depth to cigar, carry out mark apart from cigar holder end 28 mm places;
B. the preparation of cigar measuring head:
According to the diameter of cigar apart from mouth end 15 mm places, emulsion tube sleeve, emulsion tube and sealing gasket in measuring head base and the measuring head are selected, measuring head should be from terminal cigar 28 mm that coat of cigar holder, and flue gas composition and air all had impenetrability, avoid leaking gas between cigar and the measuring head;
C. the calculating of air flow rate:
In order to guarantee that the gas velocity by the cigar xsect is the constant flow rate of 11.8 cm/s, diameter should calculate according to the diameter of cigar apart from mouth end 33 mm places greater than the air flow rate of the cigar of 12.0 mm;
D. the mensuration of cigar resistance to suction:
Air flow rate corresponding to cigar sample to be measured proofreaied and correct and set to the resistance to suction instrument, measuring head is positioned over sense channel after, carry out zero clearing, insert cigar sample to be measured, the degree of depth that cigar inserts measuring head is 28 mm, the resistance to suction value of record sample.
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102390318A (en) * 2011-10-22 2012-03-28 成都市翻鑫家科技有限公司 Automobile tail lamp circuit
CN105241601A (en) * 2015-11-13 2016-01-13 深圳市新宜康科技有限公司 Electronic cigarette atomization core and atomizer air resistance production line detection method and detection device
CN106018168B (en) * 2016-05-16 2018-07-31 江苏中烟工业有限责任公司 A kind of method of on-line measurement Cigarette Draw Resistance
CN108169061A (en) * 2017-11-28 2018-06-15 山东中烟工业有限责任公司 A kind of craft whole-tobacco leaves roll cigar resistance to suction detection method
CN112229757B (en) * 2020-10-10 2024-03-29 中国烟草总公司郑州烟草研究院 Method for evaluating quick conformity of pressure drop of cigarette and filter stick

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101839835A (en) * 2010-02-04 2010-09-22 河南中烟工业有限责任公司 Method for fast comparing suction resistance between cigarette suction resistance instruments
CN101943651A (en) * 2010-09-20 2011-01-12 中国烟草总公司郑州烟草研究院 Filter stick suction resistance on-line measuring device
CN201716091U (en) * 2010-06-30 2011-01-19 中国科学院沈阳科学仪器研制中心有限公司 Five-physical index detection system for cigarettes

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101839835A (en) * 2010-02-04 2010-09-22 河南中烟工业有限责任公司 Method for fast comparing suction resistance between cigarette suction resistance instruments
CN201716091U (en) * 2010-06-30 2011-01-19 中国科学院沈阳科学仪器研制中心有限公司 Five-physical index detection system for cigarettes
CN101943651A (en) * 2010-09-20 2011-01-12 中国烟草总公司郑州烟草研究院 Filter stick suction resistance on-line measuring device

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