CN102218230A - Washing flow tank convenient for ester and saponin separation - Google Patents
Washing flow tank convenient for ester and saponin separation Download PDFInfo
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- CN102218230A CN102218230A CN2011100656892A CN201110065689A CN102218230A CN 102218230 A CN102218230 A CN 102218230A CN 2011100656892 A CN2011100656892 A CN 2011100656892A CN 201110065689 A CN201110065689 A CN 201110065689A CN 102218230 A CN102218230 A CN 102218230A
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- ester
- soap
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- settling tank
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Abstract
The invention discloses a washing flow tank which is convenient for ester and saponin separation. The tank which comprises a body is characterized in that: spraying devices are arranged on an upper part of the body, a window and joints for material discharge are arranged on a lower part of the body, and the window and the joints are in a same horizontal position. The tank has the advantages that a problem of secondary emulsification of ester caused by traditional stirring modes can be avoided and simultaneously the investment of the washing flow tank can be reduced and energy consumption in production processes can be decreased, because the spraying devices employed in the present invention allow water to be sprayed into a material system from the top of the washing flow tank; and the quality of products can be improved because a case that water impurities and saponin are introduced into ester during emptying ester, saponin and water impurity is avoided, the centrifugation difficulty is reduced, and the separation precision is improved.
Description
Technical field
The present invention relates to a kind of washing settling tank, particularly a kind of washing settling tank that makes things convenient for fat, soap to separate.
Background technology
In the production of biodiesel process to the separation of ester, soap, all adopt and to comprise the assorted material system of ester, soap and part water in the settling tank in washing and add water and mix, then adopt standing sedimentation that ester, soap, water are mixed and carry out layering, again three layers of material are carried out blowing respectively.At above separation process, existing washing settling tank device except tank body and associated components, also is equipped with mixing component, comprises motor, reductor, frame, shaft coupling, sealing, shaft, blade etc.In existing washing settling tank device, carry out above-mentioned separation process meeting and following problem occurs:
The one, because the existence of soap in the material system, when after adding water, stirring, emulsion can appear, even the ester saponification that part can directly be separated originally, and must be reclaimed by the ester of saponification, enter next process and generate the acid of ester fat, after separating, carry out esterification in deesterify workshop section, causing a large amount of energy wastes like this, reduce production capacity, is a problem of the many production of biodiesel of puzzlement enterprise;
The 2nd, in the separation process of ester, soap, because material printing opacity problem, can't see ester output, soap, the assorted separating interface of water by the visor on the equipment at all, existing processing technology routine all adopts in washing settling tank bottom and adds pipeline visor blowing respectively, promptly earlier soap is emitted, emitted then to water assortedly, emit ester at last, in this process,, water reaches the flowability problem of soap because mixing, a part is trapped in inner tank wall, when finally putting ester, be brought in the ester, thereby cause next step centrifugation precision to reduce, finally influence the quality of ester product.
Summary of the invention
Goal of the invention: at the problems referred to above, the purpose of this invention is to provide a kind of improved washing settling tank, emulsion does not appear in the existence that makes in the production of biodiesel process washing to ester, soap, separates because of soap, and by the clear wash rice of form as seen the layering that makes each storeroom simultaneously is convenient to separate.
Technical scheme: a kind of washing settling tank of being convenient to fat, soap separation, comprise tank body, described tank body top is equipped with spray equipment, and described tank body bottom is equipped with form and is used for the joint of discharges material, and described joint and described form are in same horizontal level.
Described spray equipment is a rotary-atomizing, washes material surface in the settling tank from the shower water of spray equipment ejection from comprehensive the covering of a plurality of angles.
Described spray equipment is the spray group with a plurality of atomizers, plays the spray effect of enhancing to material equally, covers the material surface equably.
Described atomizer is installed on the coil pipe, and coil arrangement is illegally occupied on tank body top, the spray effect of even shower water, and coil pipe also is the water channel to each atomizer simultaneously.
Described form has inside and outside two-layer eyeglass, can make operating personnel when observing the tank interior material by natural daylight or intense light source, the layering that can see material clearly.
Described joint is the joint group of being made up of a plurality of joints along described form length arrangement, at the material bed blowing that carries out of diverse location, or finds corresponding joint blowing by adjusting material bed position.
The present invention is characteristics of utilizing water and soap to mix, adopt spray equipment that water etc. is injected to the assorted material system of ester, soap, water from washing settling tank top uniformly, tiny water droplet has destroyed the structure of original system when entering into the material system, neat soap is pulled out from ester apace, utilize the sedimentation from the material system of water soap hybrid density simultaneously greater than the density of ester, separate by standing sedimentation, finally be divided into three layers, orlop is that water is assorted, sublevel is that soap, the superiors are ester.
Form is installed in the tank body bottom with the joint that is used for discharges material, i.e. the position of ester, soap, the assorted layering interfaces of water after the standing sedimentation layering makes operating personnel see ester, soap, the assorted layering interfaces of water clearly by form outside equipment; A plurality of joints of arranging along the form length direction can make the ester in the washing settling tank discharge, if micro-height tolerance appears in the position of ester layer and the position of certain joint, can adjust the interface by mixing, discharge ester by the joint of correspondence position again from tank base floss hole discharge section water.
Beneficial effect: compared with prior art, advantage of the present invention is to adopt spray equipment that water etc. is injected to the material system from washing settling tank top uniformly on the one hand, prevent the ester second emulsifying problem that causes because of traditional alr mode, reduce the input of washing settling tank body apparatus simultaneously, reduce the energy consumption in the production process; Avoided in the assorted blowing process of ester, soap, water that water is assorted, soap ribbon to go in the ester on the other hand, reduced the centrifugation difficulty, improved separation accuracy, thereby improve the quality of product.
Description of drawings
Fig. 1 is a front view of the present invention;
Fig. 2 is the A-A view among Fig. 1.
The specific embodiment
Below in conjunction with the drawings and specific embodiments, further illustrate the present invention, should understand these embodiment only is used to the present invention is described and is not used in and limit the scope of the invention, after having read the present invention, those skilled in the art all fall within the application's claims institute restricted portion to the modification of the various equivalent form of values of the present invention.
Shown in accompanying drawing 1,2, the present invention washes settling tank, tank body 1 top is provided with coil pipe 5, spray equipment 2 is installed on the coil pipe 5, and this spray equipment 2 is the hollow atomizer group of spiral, and coil pipe can be one group, also can be many groups, the supply of shower water is provided by water pump, sends into coil pipe 5 by water inlet pipe, and the water that sprays under certain pressure covers material system surface in the washing settling tank.The setting of spray equipment 2, will according to the different angles of the hollow atomizer of spiral rotation and apart from the material surface apart from calculating and setting, the best surface that the hollow atomizer of spiral is reached material covers, guarantee that shower water can cover whole material surface more equably, particularly water to washing the spray at settling tank inwall place, guarantee that the soap at inwall place can be removed by the outermost of the atomizing circle of rotary spray atomizing back formation.After these spray equipment 2 effects,, obtain ester, soap, the assorted layering interfaces of water with material system standing sedimentation.Orlop is that water is assorted, sublevel is that soap, the superiors are ester.
The form 3 that install washing settling tank tank body 1 bottom is inside and outside two-layer eyeglasses, and the distance between two-layer eyeglass is short, and approximately 10cm can make operating personnel when observing the tank interior material by natural daylight or intense light source, the layering that can see material clearly.Layering interfaces place after form 3 roughly is installed in material and leaves standstill is being positioned at same horizontal position with form, and vertical array has been installed one group of a plurality of joint 4 that is used for discharges material, cooperates from the observed layering interfaces of form, carries out the blowing operation.During concrete operations,, find out and ester, a most identical joint of soap interface,, open joint and can discharge ester with pipeline and this joint UNICOM by the position at form affirmation ester, soap interface.If the ester layer micro-height tolerance occurs with the most identical joint location, can by from tank base floss hole 6 discharge section water are assorted adjust interface location after, discharge ester by joint again; Discharge soap then in the same way, low amounts of water can be mixed during row's soap is discharged in the soap; Water is assorted discharges from tank base floss hole 6.The joint arrangement that one set of joints of arrange installing should guarantee the top is above ester, soap interface, and a joint arrangement of below is below soap, the assorted interface of water.
Claims (6)
1. be convenient to the washing settling tank that fat, soap separate for one kind, comprise tank body (1), it is characterized in that: described tank body (1) top is equipped with spray equipment (2), described tank body (1) bottom is equipped with form (3) and is used for the joint (4) of discharges material, and described joint (4) is in same horizontal level with described form (3).
2. the washing settling tank of being convenient to fat, soap separation according to claim 1, it is characterized in that: described spray equipment (2) is a rotary-atomizing.
3. the washing settling tank of being convenient to fat, soap separation according to claim 1, it is characterized in that: described spray equipment (2) is for having the spray group of a plurality of atomizers.
4. the washing settling tank of being convenient to fat, soap separation according to claim 3, it is characterized in that: described atomizer is installed on the coil pipe (5).
5. the washing settling tank of being convenient to fat, soap separation according to claim 1, it is characterized in that: described form (3) has inside and outside two-layer eyeglass.
6. according to claim 1ly be convenient to the washing settling tank that fat, soap separate, it is characterized in that: described joint (4) is the joint group of being made up of a plurality of joints along described form (3) length arrangement.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011100656892A CN102218230A (en) | 2011-03-18 | 2011-03-18 | Washing flow tank convenient for ester and saponin separation |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011100656892A CN102218230A (en) | 2011-03-18 | 2011-03-18 | Washing flow tank convenient for ester and saponin separation |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN102218230A true CN102218230A (en) | 2011-10-19 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2011100656892A Pending CN102218230A (en) | 2011-03-18 | 2011-03-18 | Washing flow tank convenient for ester and saponin separation |
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| Country | Link |
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| CN (1) | CN102218230A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105879821A (en) * | 2016-06-01 | 2016-08-24 | 唐山建华科技发展有限责任公司 | Solid-liquid separation device for high corrosion environment |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2001276536A (en) * | 2000-03-29 | 2001-10-09 | Hitachi Zosen Corp | Dry dust collecting apparatus for blast furnace |
| CN1761737A (en) * | 2003-03-20 | 2006-04-19 | 迈克尔·F·佩莱 | Method and apparatus for refining biodiesel |
| CN202036821U (en) * | 2011-03-18 | 2011-11-16 | 江苏恒顺达生物能源有限公司 | Washing precipitation tank convenient for separating grease from soap |
-
2011
- 2011-03-18 CN CN2011100656892A patent/CN102218230A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2001276536A (en) * | 2000-03-29 | 2001-10-09 | Hitachi Zosen Corp | Dry dust collecting apparatus for blast furnace |
| CN1761737A (en) * | 2003-03-20 | 2006-04-19 | 迈克尔·F·佩莱 | Method and apparatus for refining biodiesel |
| CN202036821U (en) * | 2011-03-18 | 2011-11-16 | 江苏恒顺达生物能源有限公司 | Washing precipitation tank convenient for separating grease from soap |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105879821A (en) * | 2016-06-01 | 2016-08-24 | 唐山建华科技发展有限责任公司 | Solid-liquid separation device for high corrosion environment |
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| C06 | Publication | ||
| PB01 | Publication | ||
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| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20111019 |