CN102211054B - Process for sorting coarse coal slime by utilizing heavy medium liquid-solid fluidized bed - Google Patents

Process for sorting coarse coal slime by utilizing heavy medium liquid-solid fluidized bed Download PDF

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CN102211054B
CN102211054B CN 201110141345 CN201110141345A CN102211054B CN 102211054 B CN102211054 B CN 102211054B CN 201110141345 CN201110141345 CN 201110141345 CN 201110141345 A CN201110141345 A CN 201110141345A CN 102211054 B CN102211054 B CN 102211054B
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coal
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李延锋
刘炯天
陈文刊
冉进财
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China University of Mining and Technology CUMT
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Abstract

The invention provides a process for sorting coarse coal slime by utilizing a heavy medium liquid-solid fluidized bed. The process provided by the invention comprises the following steps: pouring a dilute medium of screenings screened by a clean coal medium-removing and dewatering screen and a part of the medium in a current divider box into a coarse coal slime sorting feed barrel; introducing a medium in a heavy medium system into the feedings of a liquid-solid fluidized bed coarse coal slime sorter; after the feedings are sorted by the liquid-solid fluidized bed coarse coal slime sorter, adding a magnetic separator recovery medium into overflows and underflows, wherein the added heavy medium can be used for weakening the influence of granularity to interference settlement, and strengthening the effect for sorting materials according to density, so that the sorting precision of the liquid-solid fluidized bed coarse coal slime sorter within a wide grain range can be improved, and the recovery ratio of coarse clean coals is greatly improved on the premise of ensuring the ash content of the coarse clean coals; simultaneously, the grain processing range of the liquid-solid fluidized bed coarse coal slime sorter is expanded; and the processing capacity of reselection is improved, and the flotation cost is reduced.

Description

重介质液固流化床分选粗煤泥工艺Separation of Coarse Coal Slime in Dense Medium Liquid-solid Fluidized Bed

技术领域 technical field

本发明涉及一种重介质液固流化床分选粗煤泥工艺,尤其适用于煤炭湿法分选工艺中的3-0.25mm粗煤泥的降灰脱硫。 The invention relates to a dense medium liquid-solid fluidized bed separation process for coarse coal slime, and is especially suitable for ash reduction and desulfurization of 3-0.25mm coarse coal slime in the coal wet separation process.

背景技术 Background technique

目前大多数选煤工艺采用不分级重选+粗煤泥分选+浮选相结合的工艺,粗煤泥根据国标GB/T7186-1998一般指2mm-0.25mm的煤粒,位于重选和浮选分选粒度界限(一般为0.5mm)的附近,这部分煤泥一般采用煤泥重介旋流器、螺旋分选机和液固流化床粗煤泥分选机分选,采用煤泥重介旋流器分选粗煤泥时,受大直径旋流器的工作状况影响大,分选效果差,并且设备入料压力大,设备磨损严重。螺旋分选机分选粗煤泥时,分选密度高并且不可调,分选出精煤灰分高。液固流化床粗煤泥分选机依靠分选密度低并且可以控制调节,对入料浓度要求一般不严格,动力消耗小的优势成为目前能够有效分选粗煤泥的设备之一。 At present, most coal preparation processes use a combination of non-graded gravity separation + coarse slime separation + flotation. According to the national standard GB/T7186-1998, coarse coal generally refers to coal particles of 2mm-0.25mm, which are located between gravity separation and flotation. In the vicinity of the separation particle size limit (generally 0.5mm), this part of the slime is generally separated by a slime dense medium cyclone, a spiral separator and a liquid-solid fluidized bed coarse slime separator. When the dense medium cyclone sorts coarse coal slime, it is greatly affected by the working conditions of the large-diameter cyclone, the separation effect is poor, and the feeding pressure of the equipment is high, and the equipment wears seriously. When the spiral separator sorts coarse coal slime, the sorting density is high and cannot be adjusted, and the sorted clean coal has a high ash content. The liquid-solid fluidized bed coarse slime separator relies on the low separation density and can be controlled and adjusted. The requirements for the feed concentration are generally not strict, and the advantages of low power consumption have become one of the equipments that can effectively separate coarse slime.

液固流化床粗煤泥分选机是一种利用上升水流使煤泥流态化,依托煤泥自身作为介质形成具有一定密度的床层,煤泥按照一定的干扰沉降速度实现分选。干扰沉降速度与颗粒的粒度、密度性质有关,当窄粒级分选时,干扰沉降速度受粒度影响较小,床层密度稳定,物料按密度实现分选,分选精度高。当宽粒级分选时,干扰沉降速度受粒度影响大,床层密度不稳定,物料不能严格按照密度分选,分选精度降低。生产实际中的一般液固流化流床粗煤分选工艺是重介分选工艺中的精煤磁选尾矿或与脱泥筛筛下物经过分级旋流器分级后进入液固流化床粗煤泥分选机,在该工艺中,分选机的分选上限是由重选工艺中的脱介筛和脱泥筛的筛孔决定的,分选下限是由分级旋流器决定的,由于分级旋流器的分级效率低,决定了该工艺的分选粒度范围比较宽。在宽粒级分选过程中,高密度细颗粒会进入溢流污染精煤,低密度粗颗粒会进入底流成为尾煤,造成精煤回收率低,精煤灰分高,分选精度低,分选效果差,同时,由于液固流化床分选机在宽粒级分选效果差,导致重选的处理量受到限制,浮选的成本大。 The liquid-solid fluidized bed coarse slime separator is a kind of coal slime fluidized by rising water flow, relying on the coal slime itself as a medium to form a bed with a certain density, and the coal slime is sorted according to a certain interference settlement speed. The interference settling velocity is related to the particle size and density properties of the particles. When the narrow particle size is sorted, the interference settling velocity is less affected by the particle size, the bed density is stable, the material is sorted according to the density, and the sorting accuracy is high. When sorting with a wide particle size, the disturbing sedimentation velocity is greatly affected by the particle size, the bed density is unstable, the materials cannot be sorted strictly according to the density, and the sorting accuracy is reduced. The general liquid-solid fluidized fluidized bed coarse coal separation process in actual production is that the clean coal magnetic separation tailings or the undersize of the desliming screen in the dense medium separation process enter the liquid-solid fluidization after being classified by a classifying cyclone. Bed coarse coal slime separator, in this process, the upper limit of the separator is determined by the sieve holes of the desliming sieve and the desliming sieve in the gravity separation process, and the lower limit of the separation is determined by the classifying cyclone Yes, due to the low classification efficiency of the classifying cyclone, the separation particle size range of this process is relatively wide. In the process of wide particle size separation, high-density fine particles will enter the overflow to pollute the clean coal, and low-density coarse particles will enter the underflow to become tailing coal, resulting in low recovery rate of clean coal, high ash content of clean coal, low separation accuracy, and low separation accuracy. At the same time, due to the poor separation effect of the liquid-solid fluidized bed separator in wide particle size, the processing capacity of re-election is limited, and the cost of flotation is high.

技术内容technical content

技术问题:本发明的目的是克服已有技术中的不足之处,提供一种在分选3mm-0.25mm的粗煤泥时,精煤灰分低,分选精度高,分选效果好的重介质液固流化床分选粗煤泥工艺。 Technical problem: the purpose of the present invention is to overcome the deficiencies in the prior art, and to provide a kind of heavy coal with low clean coal ash content, high sorting precision and good sorting effect when sorting 3mm-0.25mm coarse coal slime. Medium liquid-solid fluidized bed separation process for coarse coal slime.

技术方案:本发明的重介质液固流化床分选粗煤泥工艺:包括对原煤进行脱泥或不脱泥,脱泥后原煤或不脱泥的原煤和介质桶中的介质进入三产品重介旋流器中进行分选,分选出的精煤、中煤和矸石分别进行脱介脱水,其中精煤进入精煤弧形筛进行预先脱介,预先脱介后的筛上混合物进入精煤脱介脱水筛脱介脱水,筛下物介质进入分流箱中分流,精煤脱介脱水筛筛上物的精煤进入精煤脱水设备脱水后排出,精煤脱介脱水筛筛下物的合格介质和分流箱中的一部分介质Ⅰ一并进入合介桶; Technical solution: The dense medium liquid-solid fluidized bed separation process for coarse coal slime of the present invention: including desliming or not desliming the raw coal, the raw coal after desliming or the raw coal without desliming and the medium in the medium barrel enter the three products Sorting is carried out in the dense medium cyclone, and the separated clean coal, medium coal and gangue are separated and dehydrated respectively. The clean coal dehydration screen is dewatered, and the medium under the screen enters the shunt box for diversion. The clean coal on the clean coal dehydration screen enters the clean coal dehydration equipment for dehydration and is discharged. The clean coal dehydration screen undersize The qualified medium and a part of the medium Ⅰ in the split box enter the combined media barrel together;

所述的精煤脱介脱水筛筛下物的稀介质和分流箱中的另一部分介质Ⅱ一并进入粗煤泥分选入料桶;粗煤泥分选入料桶的煤介混合物进入分级旋流器中进行分级; The thin medium of the undersieve of the clean coal de-intermediation and dehydration screen and another part of the medium II in the split box enter the coarse coal slime sorting into the bucket; the coarse coal slime sorting into the coal medium mixture into the bucket enters the classification Classification in a cyclone;

经分级旋流器分级出的溢流细颗物料进入磁选机磁选,磁选机磁选后的精矿进入合介桶,磁选后的尾矿进入浮选设备浮选; The overflow fine material classified by the grading cyclone enters the magnetic separator for magnetic separation, the concentrate after magnetic separation of the magnetic separator enters the mixing barrel, and the tailings after magnetic separation enters the flotation equipment for flotation;

经分级旋流器分级出的底流粗颗物料进入液固流化床粗煤泥分选机分选,液固流化床粗煤泥分选机分选出的溢流进入精煤磁选机磁选,磁选精矿进入合介桶,磁选尾矿经精煤煤泥分级脱水设备脱水,脱水后的精煤排出,精煤煤泥水进入浮选设备浮选; The underflow coarse material classified by the classifying cyclone enters the liquid-solid fluidized bed coarse slime separator for separation, and the overflow from the liquid-solid fluidized bed coarse slime separator enters the clean coal magnetic separator Magnetic separation, the magnetic separation concentrate enters the mixing barrel, the magnetic separation tailings are dehydrated by the clean coal slime classification dehydration equipment, the dehydrated clean coal is discharged, and the clean coal slime water enters the flotation equipment for flotation;

液固流化床粗煤泥分选机分选出的底流进入中煤磁选机磁选,磁选精矿进入合介桶,磁选尾矿经中煤煤泥分级脱水设备脱水,脱水后的中煤排出,中煤煤泥水进入浓缩压滤设备进行浓缩压滤。 The underflow from the liquid-solid fluidized bed coarse slime separator enters the China Coal Magnetic Separator for magnetic separation, and the magnetically separated concentrate enters the media barrel. The medium coal is discharged, and the medium coal slime water enters the concentrated filter press equipment for concentrated filter press.

有益效果:将精煤脱介脱水筛筛下物的稀介质和分流箱中的部分介质一并进入粗煤泥分选入料桶,通过在液固流化床粗煤泥分选机的入料中引入重介系统中的介质,经液固流化床分选后,相应在液固流化床粗煤泥分选机的溢流和底流增加磁选回收介质,由于加入的重介质削弱粒度对干扰沉降的影响,强化物料按密度分选作用,减少了高密度细颗粒和低密度粗颗粒的错配,可提高液固流化床粗煤泥分选机在宽粒级范围内的分选精度,在保证粗精煤灰分的前提下,大大提高了粗精煤的回收率。同时也延伸了液固流化床粗煤泥分选机的处理粒度范围,采用选前预脱泥时,可以增大脱泥筛的筛孔,提高脱泥效率和三产品重介旋流器的处理量,采用选前不脱泥时,可以增大脱介筛的筛缝,降低其介耗;液固流化床粗煤泥分选机对细颗粒的分选效果提高,可以降低浮选分选的有效分选粒度上限,减少进入浮选的煤泥量,降低浮选成本。 Beneficial effects: the dilute medium of the clean coal de-intermediation and dewatering screen undersize and part of the medium in the splitter box enter the coarse coal slime sorting and feeding barrel, and pass through the liquid-solid fluidized bed coarse coal slime sorting machine. The medium in the dense medium system is introduced into the feed, and after liquid-solid fluidized bed separation, the corresponding overflow and underflow of the liquid-solid fluidized bed coarse slime separator increase the magnetic separation recovery medium, because the added heavy medium weakens the The effect of particle size on disturbing settlement, strengthening the separation of materials according to density, reducing the mismatch of high-density fine particles and low-density coarse particles, can improve the performance of liquid-solid fluidized bed coarse coal slime separator in a wide range of particle sizes The separation accuracy greatly improves the recovery rate of coarse and clean coal under the premise of ensuring the ash content of coarse and clean coal. At the same time, the processing particle size range of the liquid-solid fluidized bed coarse coal slime separator is extended. When the pre-sliming is used, the sieve hole of the desliming screen can be increased, and the desliming efficiency and the three-product dense medium cyclone can be improved. When using no desliming before selection, the sieve of the desliming sieve can be increased to reduce its media consumption; the liquid-solid fluidized bed coarse coal slime separator can improve the separation effect of fine particles, which can reduce the floating The upper limit of the effective separation particle size of the separation separation can reduce the amount of slime entering the flotation and reduce the cost of flotation.

附图说明 Description of drawings

图1是本发明的工艺流程示意图。 Fig. 1 is a process flow diagram of the present invention.

具体实施方式 Detailed ways

   下面结合附图对本发明的实施例作进一步的描述: Embodiments of the present invention will be further described below in conjunction with the accompanying drawings:

实施一、当原煤中粒度小于0.5mm、含量低于20%时,无需对原煤1进行脱泥,其分选工艺步骤如下: Implementation 1. When the particle size of the raw coal is less than 0.5mm and the content is lower than 20%, it is not necessary to deslim the raw coal 1. The separation process steps are as follows:

a.不脱泥的原煤和介质桶22中的介质一并进入三产品重介旋流器3中进行分选,分别选出精煤、中煤和矸石,分选出的中煤进入中煤脱介脱水设备4,分选的矸石进入矸石脱介脱水设备7; a. The raw coal that is not deslimed and the medium in the medium barrel 22 enter the three-product dense medium cyclone 3 for separation, and clean coal, medium coal and gangue are selected respectively, and the medium coal that is sorted out enters the medium coal de-medium Dehydration equipment 4, the sorted gangue enters the gangue dehydration equipment 7;

b.三产品重介旋流器3分选出的精煤进入精煤弧形筛5预先脱介,弧形筛5的筛上混合物进入精煤脱介脱水筛7脱介脱水,筛下物介质进入分流箱8中分流; b. The clean coal selected by the three-product dense medium cyclone 3 points into the clean coal arc screen 5 for pre-demediation, and the mixture on the arc screen 5 enters the clean coal de-intermediation and dehydration screen 7 for de-intermediation and dehydration, and the under-screen medium enters Shunt in the shunt box 8;

c.精煤脱介脱水筛7的筛上物精煤经精煤脱水设备9脱水排出,.精煤脱介脱水筛7的筛下物合格介质和分流箱8下的一部分介质Ⅰ进入合介桶22内,精煤脱介脱水筛7的筛下物合格介质和分流箱8下的另一部分介质Ⅱ进入粗煤泥分选入料桶10内; c. The clean coal on the screen of the clean coal dehydration screen 7 is dehydrated and discharged by the clean coal dehydration equipment 9. The qualified medium of the undersize of the clean coal dehydration screen 7 and a part of the medium I under the splitter box 8 enter the mediation barrel 22 Inside, the qualified undersize medium of the clean coal de-mediation and dehydration screen 7 and another part of the medium II under the shunt box 8 enter the coarse coal slime sorting into the material barrel 10;

d.粗煤泥分选入料桶10内的煤介混合物经过泵输送到分级旋流器11中进行分级; d. Coarse slime is sorted into the coal-medium mixture in the material tank 10 and transported to the classifying cyclone 11 through the pump for classification;

f.分级旋流器11分级溢流出的细颗粒进入磁选机15磁选,磁选出的精矿进入合介桶22,磁选出的尾矿进入浮选设备21浮选; f. The fine particles from the classification overflow of the classifying cyclone 11 enter the magnetic separator 15 for magnetic separation, the magnetically separated concentrate enters the joint barrel 22, and the magnetically separated tailings enter the flotation device 21 for flotation;

g.分级旋流器11分级溢流出的细颗粒进入液固流化床粗煤泥分选机12分选以后,在干扰沉降作用下,低密度颗粒上升成为溢流,进入精煤磁选机14中磁选,精煤磁选机14的磁选精矿流回合介桶22内,磁选尾矿进入精煤煤泥分级脱水设备17脱水后排出精煤20,脱水后的精煤煤泥水进入浮选设备21 中浮选; g. The fine particles from the classification overflow of the classifying cyclone 11 enter the liquid-solid fluidized bed coarse coal slime separator 12 for separation, and under the action of disturbing sedimentation, the low-density particles rise to overflow and enter the clean coal magnetic separator 14 Magnetic separation, the magnetic separation concentrate of the clean coal magnetic separator 14 flows back into the media barrel 22, the magnetic separation tailings enter the clean coal slime classification dehydration equipment 17 and discharge the clean coal 20 after dehydration, and the dehydrated clean coal slime water enters the buoy Flotation in the selection equipment 21;

h.分级旋流器11分级底流中的细颗粒进入液固流化床粗煤泥分选机12分选以后,在干扰沉降作用下,低密度颗粒沉降成为底流,进入中煤磁选机13中磁选,经中煤磁选机13磁选的尾矿流回到合介桶22,磁选尾矿进入中煤煤泥分级脱水设备16脱水后,排出中煤18,脱水后的中煤煤泥水进入浓缩压滤设备21中进行浓缩压滤。 h. After the fine particles in the classified underflow of the classifying cyclone 11 enter the liquid-solid fluidized bed coarse slime separator 12 for separation, under the action of disturbing sedimentation, the low-density particles settle and become the underflow, and enter the medium magnetic separator 13. The tailings through the medium coal magnetic separator 13 magnetic separation flow back to the joint barrel 22, and the magnetic separation tailings enter the medium coal slime classification dewatering equipment 16 for dehydration, and then discharge the medium coal 18, and the medium coal slime water after dehydration Enter the concentrated filter press equipment 21 to carry out concentrated filter press.

实施二、当原煤中粒度小于0.5mm、含量大于20%时,需对原煤1进行脱泥。先将原煤1引入脱泥筛2中进行脱泥,脱泥后的筛上物原煤进入三产重介旋流器3进行分选,脱泥后的筛下物煤泥水进入粗煤泥分选入料桶10内;后续的工艺与实施一相同,省略。 Implementation 2. When the particle size of the raw coal is less than 0.5mm and the content is greater than 20%, the raw coal 1 needs to be deslimed. Firstly, the raw coal 1 is introduced into the desliming screen 2 for desliming, and the raw coal on the sieve after desliming enters the tertiary heavy medium cyclone 3 for separation, and the undersieve coal slime water after desliming enters the coarse coal slime separation Enter in the material bucket 10; Subsequent technology is identical with implementation one, omits.

Claims (1)

1.一种重介质液固流化床粗煤泥分选工艺,包括对原煤(1)进行脱泥或不脱泥,当原煤中粒度小于0.5mm、含量低于20%时,无需对原煤(1)进行脱泥,当原煤中粒度小于0.5mm、含量大于20%时,需对原煤(1)进行脱泥;脱泥后原煤或不脱泥的原煤和介质桶(22)中的介质一并进入三产品重介旋流器(3)中进行分选,分选出的精煤、中煤和矸石分别进行脱介脱水,其中精煤进入精煤弧形筛(5)进行预先脱介,预先脱介后的筛上混合物进入精煤脱介脱水筛(7)脱介脱水,筛下物介质进入分流箱(8)中分流,精煤脱介脱水筛(7)筛上物的精煤进入精煤脱水设备(9)脱水后排出,精煤脱介脱水筛(7)筛下物的合格介质和分流箱(8)中的一部分介质Ⅰ一并进入合介桶(22);其特征在于: 1. A dense medium liquid-solid fluidized bed coarse coal slime separation process, including desliming or not desliming the raw coal (1), when the particle size of the raw coal is less than 0.5mm and the content is less than 20%, there is no need to deslim the raw coal (1) Desliming. When the particle size of the raw coal is less than 0.5mm and the content is greater than 20%, the raw coal (1) needs to be deslimed; the raw coal after desliming or the raw coal without desliming and the medium in the medium barrel (22) They enter the three-product dense-medium cyclone (3) for separation, and the separated clean coal, medium coal and gangue are separated and dehydrated respectively, and the clean coal enters the clean coal curved screen (5) for pre-dehydration. medium, the mixture on the sieve after de-intermediation in advance enters the clean coal de-intermediation and dehydration screen (7) for de-intermediation and dehydration, and the medium under the sieve enters the shunt box (8) for diversion, and the clean coal de-intermediation and dehydration screen (7) sieve The clean coal enters the clean coal dehydration equipment (9) and is discharged after dehydration, and the qualified medium of the undersize of the clean coal dehydration screen (7) and a part of medium I in the splitter box (8) enter the combined media barrel (22); It is characterized by: 所述的精煤脱介脱水筛(7)筛下物的稀介质和分流箱(8)中的另一部分介质Ⅱ一并进入粗煤泥分选入料桶(10); The dilute medium of the undersize of the clean coal de-intermediation and dehydration screen (7) and another part of the medium II in the split box (8) enter the coarse coal slime into the material bucket (10); 粗煤泥分选入料桶(10)的煤介混合物进入分级旋流器(11)中进行分级;经分级旋流器(11)分级出的溢流细颗物料进入磁选机(15)磁选,磁选机(15)磁选后的精矿进入合介桶(22),磁选后的尾矿进入浮选设备(21)浮选; Coarse slime sorted into the material tank (10) and the coal-medium mixture enters the classifying cyclone (11) for classification; the overflow fine material classified by the classifying cyclone (11) enters the magnetic separator (15) Magnetic separation, the concentrated ore after magnetic separation by the magnetic separator (15) enters the joint barrel (22), and the tailings after the magnetic separation enters the flotation device (21) for flotation; 经分级旋流器(11)分级出的底流粗颗物料进入液固流化床粗煤泥分选机(12)分选,液固流化床粗煤泥分选机(12)分选出的溢流进入精煤磁选机(14)磁选,磁选精矿进入合介桶(22),磁选尾矿经精煤煤泥分级脱水设备(17)脱水,脱水后的精煤排出,精煤煤泥水进入浮选设备(21)浮选; The underflow coarse material classified by the classifying cyclone (11) enters the liquid-solid fluidized bed coarse slime separator (12) for separation, and the liquid-solid fluidized bed coarse slime separator (12) separates The overflow of the overflow enters the clean coal magnetic separator (14) for magnetic separation, the magnetic separation concentrate enters the joint barrel (22), the magnetic separation tailings are dehydrated by the clean coal slime classification dehydration equipment (17), and the dehydrated clean coal is discharged , the clean coal slime water enters the flotation equipment (21) for flotation; 液固流化床粗煤泥分选机(12)分选出的底流进入中煤磁选机(13)磁选,磁选精矿进入合介桶(22),磁选尾矿经中煤煤泥分级脱水设备(16)脱水,脱水后的中煤排出,中煤煤泥水进入浓缩压滤(19)设备进行浓缩压滤。 The underflow from the liquid-solid fluidized bed coarse slime separator (12) enters the medium coal magnetic separator (13) for magnetic separation, and the magnetically separated concentrate enters the mixing tank (22), and the magnetic separation tailings pass through the medium coal The coal slime graded dehydration equipment (16) dehydrates, and the dehydrated medium coal is discharged, and the medium coal slime water enters the concentrated filter press (19) equipment for concentrated filter press.
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