CN102182101B - Paper for high-filler culture and production method thereof - Google Patents
Paper for high-filler culture and production method thereof Download PDFInfo
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- CN102182101B CN102182101B CN 201110084721 CN201110084721A CN102182101B CN 102182101 B CN102182101 B CN 102182101B CN 201110084721 CN201110084721 CN 201110084721 CN 201110084721 A CN201110084721 A CN 201110084721A CN 102182101 B CN102182101 B CN 102182101B
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Abstract
The invention provides paper for high-filler culture and a production method thereof. The method comprises the following steps of: beating and dispersing 25 to 60 weight parts of wood pulp, and then mixing the wood pulp and 40 to 75 weight parts of calcium silicate filler to obtain paper pulp; diluting the paper pulp by adding water to obtain mixed pulp A, wherein the paper pulp accounts for 5 to12 mass percent of the mixed pulp A; beating the mixed pulp A, and diluting the beaten pulp by adding water to obtain mixed pulp B, wherein the paper pulp accounts for 3 to 7 mass percent of the mixed pulp B; removing residue from the mixed pulp B, and then adding a reinforcing agent, a dispersant and a retention and filtration aid to obtain mixed pulp C; diluting the mixed pulp C by adding waterto obtain mixed pulp D, wherein the paper pulp accounts for 0.3 to 4 mass percent of the mixed pulp D; and manufacturing the paper for the culture with the mixed pulp D by using a papermaking machine. The paper for the high-filler culture solves the problem of low filler adding amount in the prior art.
Description
Technical field
The invention belongs to pulp technology for making paper, relate in particular to a kind of high filler cultural paper and production method thereof.
Background technology
Present cultural paper commonly used based on a large amount of string paper pulp, adds mineral filler such as 10%~20% calcium carbonate or talcum powder and a spot of chemical assistant again and makes.Yet it is bigger to be accompanied by environmental pollution and plant material consumption that pulping process brings, and water consumption is big, and the problem that energy resource consumption is big needs to consider to reduce the string consumption but must guarantee the paper technology of the performance of paper own.
A kind of product that is called as stone paper is arranged at present, be to make with the processing method that Paris white and plastics mix film forming, this method is the calcium carbonate powder with 50%~80%, granularity is that 800 orders are to 1200 orders, earlier with PE (polyethylene) plastics and the mixing particle that manufactures of adhesive, the film that manufactures as papermaking with the plastic molding press of blown film or press mold is stone paper again.The quality of this stone paper has very big difference with commonly used sheet properties, mainly has difficult degradation, difficult printing, and usable floor area little (weight is big), and reclaim problem such as difficulty, do not satisfy the requirement of cultural paper.Can't realize the production of high filler cultural paper thus in the prior art.
Summary of the invention
The invention provides a kind of high filler cultural paper and production method thereof, be intended to realize improving the filler addition of cultural paper, and paper performance satisfies concerned countries standard or industry standard.
The invention provides a kind of production method of high filler cultural paper, may further comprise the steps:
Disperse back the mixing with the calcium silicate filling material of 40~75 weight portions to obtain paper pulp the wood pulp size degradation of 25-60 weight portion; Described paper pulp thin up is obtained mixed slurry A, and the mass percent that makes described paper pulp account for described mixed slurry A is 5~12%;
After mixed slurry A making beating, thin up obtains mixed slurry B, and the mass percent that makes described paper pulp account for described mixed slurry B is 3-7%; Wherein, for example mixed slurry A can the be pulled an oar beating degree of 35 ° of SR~80 ° SR;
After mixed slurry B slagging-off, add reinforcing agent, dispersant and retention and drainage aid agent, obtain mixed slurry C;
Thin up obtains mixed slurry D in the described mixed slurry C, and the mass percent that makes described paper pulp account for described mixed slurry D is 0.3-4%;
With paper machine with the described mixed slurry D cultural paper of manufacturing paper with pulp out.Further, behind the cultural paper of manufacturing paper with pulp out, the coating latex that can also to add relative pulp quality percentage be 1.5-5.5% carries out dip coated, evenly is coated with can make between the fiber of forming paper behind the latex to combine closely, and forms the paper that has than high-tensile strength and water proofing property.
Wherein, described calcium silicate filling material is the active silicic acid calcium powder, and this active silicic acid calcium powder is loose porous white powder, whiteness 〉=80%, and further whiteness 〉=85%, whiteness 〉=90% further, bulk density is 0.10-0.50g/cm
3, further bulk density is 0.15-0.40g/cm
3, further bulk density is 0.17-0.30g/cm
3, particle diameter is 3-40 μ m, and further particle diameter is 5-30 μ m, and further particle diameter is 8-25 μ m.Active silicic acid calcium powder among the present invention can utilize flyash or other industrial solid castoffs to produce.
Further, wood pulp is the 30-50 weight portion, and calcium silicate filling material is the 50-70 weight portion.
Further, wood pulp is the 36-47 weight portion, and calcium silicate filling material is the 53-64 weight portion.
In a preferred embodiment, it is 1-5% that the addition of described reinforcing agent accounts for described pulp quality percentage, and described reinforcing agent is water miscible PVA fiber.
In a preferred embodiment, it is 0.5-1.5% that the addition of described dispersant accounts for described pulp quality percentage, and described dispersant is polyethylene glycol oxide.
In a preferred embodiment, it is 0.3-3% that the addition of described retention and drainage aid agent accounts for described pulp quality percentage, and described retention and drainage aid agent is high molecular polymer.
The present invention also provides a kind of high filler cultural paper that uses method provided by the invention to make.
High filler cultural paper provided by the invention and production method thereof, calcium silicates with 40~75% is filler, plant fiber material with 25~60% is skeleton, utilizes paper technology to produce cultural paper, can also make paper possess higher pulling force and water proofing property after water-fast latex dipping coating.High filler cultural paper provided by the invention can reach the every index that has cultural paper now, has solved the lower problem of the addition of filler in the prior art.High filler cultural paper provided by the invention, when keeping existing cultural paper character, can save the plant wood pulp fibre significantly, reduce the consumption of plant material, and the calcium silicate filling material among the present invention can utilize trade waste to obtain, thereby makes raw material economics and environmental protection.
The specific embodiment
Below in conjunction with concrete embodiment the present invention is described in further detail.
The production method of high filler cultural paper provided by the invention can may further comprise the steps:
Step 1, the wood pulp size degradation of certain part by weight disperseed to mix with the calcium silicate filling material of certain part by weight obtain paper pulp; Described paper pulp thin up is obtained mixed slurry A;
Be specifically as follows: send into after the wood pulp of certain part by weight is disperseed with the hydrabrusher size degradation and kowtow preceding pulp storage tank, the calcium silicate filling material that adds certain part by weight this is kowtowed before in the pulp storage tank obtains paper pulp, adds the water adjusting in this paper pulp then and obtains mixed slurry A; Wherein, wood pulp can be bleached wood pulp.
Step 2, with after the mixed slurry A that obtains in the step 1 making beating, thin up obtains mixed slurry B;
Be specifically as follows: with disc mill the mixed slurry A that obtains in the step 1 is pulled an oar after certain beating degree, thin up obtains mixed slurry B, mixed slurry B is sent into kowtow the back pulp storage tank then.
Step 3, the mixed slurry B that obtains in the step 2 purified slagging-off after, add reinforcing agent, dispersant and retention and drainage aid agent, obtain mixed slurry C;
Be specifically as follows: the mixed slurry B that obtains in the step 2 is sent into the pond of sizing mixing after pulp screen and desander purification; In the pond of sizing mixing, add a certain amount of reinforcing agent then, stir and mix; In the pond of sizing mixing, add certain amount of dispersant again, stir and mix; Add a certain amount of retention and drainage aid agent as required again, obtain mixed slurry C.Wherein, the addition sequence of reinforcing agent, dispersant and retention and drainage aid agent can be decided according to the actual requirements, and the present invention does not limit.
Thin up obtains mixed slurry D among step 4, the mixed slurry C that obtains in the step 3, mixed slurry D can be sent into then and copy preceding stock tank.
Step 5, with paper machine with the mixed slurry D that obtains in the step 4 cultural paper of manufacturing paper with pulp out;
Concrete, can use the paper machine required quantitative cultural paper of manufacturing paper with pulp out as required, for example: can be by the speed of a motor vehicle of control head box flow velocity and the paper machine required quantitative cultural paper of manufacturing paper with pulp out; Behind the cultural paper of manufacturing paper with pulp out, can add a certain amount of latex coating again and carry out dip coated.
Wherein, reinforcing agent is water miscible PVA (polyvinyl alcohol) fiber, and reinforcing agent can directly add in the mixed slurry and mixes with paper pulp fiber, copies when dry behind the paper to be combined the generation humidification with paper pulp fiber.
Dispersant is polyethylene glycol oxide (PEO), and to become mass fraction be 0.5~6% solution to thin up during use, adds in the mixed slurry fiber is evenly disperseed, and guarantees the evenness of paper.
Retention and drainage aid agent is for example PAM (polyacrylamide) of high molecular polymer, and the purpose that adds retention and drainage aid agent is the drainage rate when accelerating the shaping of l Water Paper page or leaf.
The mixing material that latex coating is made up of starch, active silicic acid calcium micro mist, AKD (alkyl ketene dimer), latex etc. is attached to paper surface uniformly, forms level and smooth bright and clean surface; Perhaps, also available carboxylic styrene butadiene latex of latex coating; To be coated with latex is coated on can increase paper in the page surface strength with infusion process, and prevent the paper layering and give paper anti-water humidity resistance.
Embodiment one
Use following method to produce high filler cultural paper:
Send into after step 101, the bleached sulphate needlebush pulpboard water power pulper size degradation dispersion with 50 weight portions and kowtow preceding pulp storage tank, the calcium silicate filling material that adds 50 weight portions before this is kowtowed in the pulp storage tank obtains paper pulp; Add the water adjusting and obtain mixed slurry A in paper pulp, the mass percent that makes paper pulp account for mixed slurry A is 6.0%;
Wherein, the whiteness of the calcium silicate filling material in this step is 92%, and bulk density is 0.30g/cm
3, average grain diameter is 20 μ m;
Step 102, with disc mill the mixed slurry A that obtains in the step 101 is pulled an oar after the beating degree of 40 ° of SR, thin up obtains mixed slurry B, and the mass percent that makes paper pulp account for mixed slurry B is 4.0%; And with mixed slurry B send into kowtow the back pulp storage tank;
Step 103, the mixed slurry B that step 102 is obtained send into the pond of sizing mixing after pulp screen and desander purification;
Step 104, add that to account for pulp quality percentage be 1.0% reinforcing agent in the pond of sizing mixing, stir and mix;
Step 105, add that to account for pulp quality percentage be 0.5% dispersant and to account for pulp quality percentage be 0.3% retention and drainage aid agent in the pond of sizing mixing again, obtain mixed slurry C;
Step 106, add water regulate and to obtain mixed slurry D in mixed slurry C, the mass percent that makes paper pulp account for mixed slurry D is 1.0%; And mixed slurry D sent into copy preceding stock tank;
Step 107, with the paper machine required quantitative paper of manufacturing paper with pulp out;
According to different demands, the speed of a motor vehicle of control head box flow velocity and the paper machine required dissimilar cultural paper of manufacturing paper with pulp out is the performance of the dissimilar cultural papers that make below:
Offset printing paper, quantitatively 67.7g/m
2, whiteness 78.7%, opacity 98.7%, satisfy the requirement of QB/T1012-1991;
Light-duty printing paper, quantitatively 67.7g/m
2, brightness 78.7%, opacity 98.7%, tensile index 32.05N.m/g, satisfy the requirement of QB/T2809-2006;
Copy paper, quantitatively 70.9g/m
2, thickness 176 μ m, whiteness 92.1%, opacity 98.57%, satisfy the requirement of QB/T2342-2006;
Writing paper, quantitatively 58.4g/m
2, tightness 0.85g/m
2, whiteness 85.5%, opacity 93.4%, satisfy the requirement of GB/T12654-2008;
Newsprint, quantitatively 49.8g/m
2, brightness 78.1%, opacity 98.57%, satisfy the requirement of GB/T1910-1999.
Step 108, to add relative pulp quality mark at the paper of manufacturing paper with pulp out be that 1.5% latex coating carries out dip coated.
Embodiment two
Use following method to produce high filler cultural paper:
Send into after step 201, the bleached sulphate needlebush pulpboard water power pulper size degradation dispersion with 40 weight portions and kowtow preceding pulp storage tank, the calcium silicate filling material that adds 60 weight portions before this is kowtowed in the pulp storage tank obtains paper pulp; Add the water adjusting and obtain mixed slurry A in paper pulp, the mass percent that makes paper pulp account for mixed slurry A is 6.0%;
Calcium silicate filling material whiteness in this step is 93%, and bulk density is 0.25g/cm
3, average grain diameter is 23 μ m;
Step 202, with disc mill the mixed slurry A that obtains in the step 201 is pulled an oar after the beating degree of 42 ° of SR, thin up obtains mixed slurry B, and the mass percent that makes paper pulp account for mixed slurry B is 5.0%; And with mixed slurry B send into kowtow the back pulp storage tank;
Step 203, the mixed slurry B that step 202 is obtained send into the pond of sizing mixing after pulp screen and desander purification;
Step 204, add that to account for pulp quality percentage be 2.5% reinforcing agent in the pond of sizing mixing, stir and mix;
Step 205, add that to account for pulp quality percentage be 1.0% dispersant and to account for pulp quality percentage be 0.4% retention and drainage aid agent in the pond of sizing mixing again, obtain mixed slurry C;
Step 206, add water regulate and to obtain mixed slurry D in mixed slurry C, the mass percent that makes paper pulp account for mixed slurry D is 0.8%; And mixed slurry D sent into copy preceding stock tank;
Step 207, with the paper machine required quantitative paper of manufacturing paper with pulp out;
According to different demands, the speed of a motor vehicle of control head box flow velocity and the paper machine required dissimilar cultural paper of manufacturing paper with pulp out is the performance of the dissimilar cultural papers that make below:
Offset printing paper, quantitatively 70.2g/m
2, thickness 173 μ m, whiteness 80.7%, opacity 98.2%, satisfy the requirement of QB/T1012-1991;
Light-duty printing paper, quantitatively 63.1g/m
2, brightness 71.4%, opacity 95.3%, tensile index 30.01N.m/g, satisfy the requirement of QB/T2809-2006;
Copy paper, quantitatively 71.5g/m
2, thickness 165 μ m, whiteness 90.9%, opacity 98.7%, satisfy the requirement of QB/T2342-2006;
Writing paper, quantitatively 60.2g/m
2, tightness 0.83g/m
2, whiteness 82.9%, opacity 95.5%, satisfy the requirement of GB/T12654-2008;
Step 208, to add relative pulp quality mark at the paper of manufacturing paper with pulp out be that 3.0% latex coating carries out dip coated.
Embodiment three
Use following method to produce high filler cultural paper:
Send into after step 301, the bleached sulphate needlebush pulpboard water power pulper size degradation dispersion with 30 weight portions and kowtow preceding pulp storage tank, the calcium silicate filling material that adds 70 weight portions before this is kowtowed in the pulp storage tank obtains paper pulp; Add the water adjusting and obtain mixed slurry A in paper pulp, the mass percent that makes paper pulp account for mixed slurry A is 8.0%;
Calcium silicate filling material whiteness in this step is 91%, and bulk density is 0.20g/cm
3, average grain diameter is 28 μ m;
Step 302, with disc mill the mixed slurry A that obtains in the step 301 is pulled an oar after the beating degree of 45 ° of SR, thin up obtains mixed slurry B, and the mass percent that makes paper pulp account for mixed slurry B is 5.0%; And with mixed slurry B send into kowtow the back pulp storage tank;
Step 303, the mixed slurry B that step 302 is obtained send into the pond of sizing mixing after pulp screen and desander purification;
Step 304, add that to account for pulp quality percentage be 3.0% reinforcing agent in the pond of sizing mixing, stir and mix;
Step 305, to add that to account for pulp quality percentage be 1.0% dispersant in the pond of sizing mixing again, account for pulp quality percentage be 0.5% retention and drainage aid agent etc., obtains mixed slurry C;
Step 306, add water regulate and to obtain mixed slurry D in mixed slurry C, the mass percent that makes paper pulp account for mixed slurry D is 0.5%; And mixed slurry D sent into copy preceding stock tank;
Step 307, with the paper machine required quantitative paper of manufacturing paper with pulp out;
According to different demands, the speed of a motor vehicle of control head box flow velocity and the paper machine required dissimilar cultural paper of manufacturing paper with pulp out is the performance of the dissimilar cultural papers that make below:
Light-duty printing paper, quantitatively 59.1g/m
2, brightness 76.6%, opacity 99.3%, tensile index 28.05N.m/g, satisfy the requirement of QB/T2809-2006;
Writing paper, quantitatively 59.1g/m
2, tightness 0.78g/m
2, whiteness 76.6%, opacity 99.3%, satisfy the requirement of GB/T12654-2008;
Step 308, to add relative pulp quality mark at the paper of manufacturing paper with pulp out be that 3.5% latex coating carries out dip coated.
By the various embodiments described above as can be known; use the high filler cultural paper of method preparation provided by the invention; the index request that meets multiple cultural paper; but the present invention is not limited to limited several paper kinds of mentioning in the various embodiments described above, so long as the paper that adopts operating process described in the invention and method or similar operating process and method to produce all belongs to protection scope of the present invention.
The invention solves the lower problem of the addition of filler in the prior art; High filler cultural paper provided by the invention, when keeping existing cultural paper character, can save the plant wood pulp fibre significantly, reduce the consumption of plant material, and the calcium silicate filling material among the present invention can utilize trade waste to obtain, thereby makes raw material economics and environmental protection.Compare with cultural paper at present commonly used, high filler cultural paper has advantages such as anti-flammability is strong, proportion is low, percentage elongation is low, production cost is low, particularly in the powerful advantages of saving significantly aspect the string, makes it have very wide application prospect.
It should be noted that at last: above embodiment only in order to technical scheme of the present invention to be described, is not intended to limit; Although with reference to previous embodiment the present invention is had been described in detail, those of ordinary skill in the art is to be understood that: it still can be made amendment to the technical scheme that aforementioned each embodiment puts down in writing, and perhaps part technical characterictic wherein is equal to replacement; And these modifications or replacement do not make the essence of appropriate technical solution break away from the spirit and scope of various embodiments of the present invention technical scheme.
Claims (7)
1. the production method of a high filler cultural paper is characterized in that, may further comprise the steps:
Disperse back the mixing with the active silicic acid calcium filler of 40 ~ 75 weight portions to obtain paper pulp the wood pulp size degradation of 25-60 weight portion; Described paper pulp thin up is obtained mixed slurry A, and the mass percent that makes described paper pulp account for described mixed slurry A is 5 ~ 12%; Described active silicic acid calcium filler is loose porous white powder, whiteness 〉=80%, and bulk density is 0.10-0.50g/cm
3, particle diameter is 3-40 μ m;
After mixed slurry A making beating, thin up obtains mixed slurry B, and the mass percent that makes described paper pulp account for described mixed slurry B is 3-7%;
After described mixed slurry B slagging-off, add reinforcing agent, dispersant and retention and drainage aid agent, obtain mixed slurry C;
Thin up obtains mixed slurry D in the described mixed slurry C, and the mass percent that makes described paper pulp account for described mixed slurry D is 0.3-4%;
With paper machine with the described mixed slurry D cultural paper of manufacturing paper with pulp out.
2. the production method of high filler cultural paper according to claim 1 is characterized in that:
Whiteness 〉=85% of described active silicic acid calcium filler, bulk density are 0.17-0.30g/cm
3, particle diameter is 5-30 μ m.
3. the production method of high filler cultural paper according to claim 1, it is characterized in that: described wood pulp is the 30-50 weight portion, described active silicic acid calcium filler is the 50-70 weight portion.
4. the production method of high filler cultural paper according to claim 1, it is characterized in that: it is 1-5% that the addition of described reinforcing agent accounts for described pulp quality percentage, described reinforcing agent is water miscible PVA fiber.
5. the production method of high filler cultural paper according to claim 1, it is characterized in that: it is 0.5-1.5% that the addition of described dispersant accounts for described pulp quality percentage, described dispersant is polyethylene glycol oxide.
6. the production method of high filler cultural paper according to claim 1, it is characterized in that: it is 0.3-3% that the addition of described retention and drainage aid agent accounts for described pulp quality percentage, described retention and drainage aid agent is high molecular polymer.
7. a right to use requires the high filler cultural paper that the arbitrary described method of 1-6 makes.
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Families Citing this family (7)
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CN102493283A (en) * | 2011-11-22 | 2012-06-13 | 陕西科技大学 | Technology for producing white clay-filled paper |
CN103669089A (en) * | 2012-09-10 | 2014-03-26 | 国能纸业有限公司 | Rear drying system used for multi-cylinder long mesh paper machine |
CN103422397B (en) * | 2013-06-13 | 2015-11-25 | 大唐国际发电股份有限公司高铝煤炭资源开发利用研发中心 | Height adds filler millboard and pulping method thereof |
CN103526630B (en) * | 2013-11-05 | 2015-11-25 | 大唐国际发电股份有限公司高铝煤炭资源开发利用研发中心 | Pulping method of high surface strength offset printing paper and products thereof |
CN105113323B (en) * | 2015-07-31 | 2017-09-19 | 杜德光 | A kind of stone paper and preparation method thereof |
CN106868925A (en) * | 2016-12-30 | 2017-06-20 | 芜湖市哈贝纸业有限公司 | A kind of high-strength filler paper high and preparation method thereof |
CN110331624A (en) * | 2019-08-01 | 2019-10-15 | 江南大学 | A kind of material and preparation method of granular filler moulded paper pulp product |
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CN101476259A (en) * | 2009-01-19 | 2009-07-08 | 南昌大学 | Inorganic filler reinforced paper pallet and preparation thereof |
CN102011347A (en) * | 2010-09-29 | 2011-04-13 | 宋旭 | Calcium silicate high-filling polymer modified paper |
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CN1238820A (en) * | 1996-09-27 | 1999-12-15 | 普罗格特-甘布尔公司 | Process for making smooth uncreped tissue paper containing fine particulate fillers |
CN1861901A (en) * | 2006-06-16 | 2006-11-15 | 中国建筑材料科学研究总院 | High temp. resisting low thermoconducting flexible ceramics fibre composite paper and its making method |
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