CN102131400A - Method for producing plastic fat composition - Google Patents
Method for producing plastic fat composition Download PDFInfo
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- CN102131400A CN102131400A CN2009801328398A CN200980132839A CN102131400A CN 102131400 A CN102131400 A CN 102131400A CN 2009801328398 A CN2009801328398 A CN 2009801328398A CN 200980132839 A CN200980132839 A CN 200980132839A CN 102131400 A CN102131400 A CN 102131400A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
- A23D9/04—Working-up
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- Oil, Petroleum & Natural Gas (AREA)
- Life Sciences & Earth Sciences (AREA)
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- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Edible Oils And Fats (AREA)
- Fats And Perfumes (AREA)
Abstract
Provided is a novel method for producing a plastic lipid composition wherein a ''tempering '' step, which takes a long time and much labor in the existing methods for producing a plastic fat composition, can be carried out more efficiently. It is found out that, in the preparation of a plastic lipid composition, an equivalent effect to the conventional tempering operation can be obtained by lowering the material temperature to a definite level by cold kneading and, after a definite retention time, heating to a definite temperature in an inline system.
Description
Technical field
The present invention relates to a kind of autofrettage of plastic fat composition.
Background technology
The manufacturing of margarine, low fat margarine, shortening wet goods plastic fat composition is following carrying out usually: the solution that will be also referred to as the grease of concoction or contain the emulsion of grease is passed into scraper-type heat exchanger (Kombinator
), Perfector
Scraped surface heat exchanger (Votator
) wait the scraping type heat exchanger for representative to carry out chilling, mixing, be filled to then in the case, via at curing chamber or be also referred to as the curing step (being also referred to as temperature adjustment) that keeps certain hour in the heat room in temperature adjustment storehouse, obtain the goods of stabilizing quality.By via temperature adjustment, the ductility of improving margarine, low fat margarine, shortening wet goods plastic fat composition and the tendency of beating frothing capacity are arranged.The mixing goods that obtain of chilling are not carried out temperature adjustment and directly refrigeration, store, during circulation, ductility arranged and beat the tendency of frothing capacity difference, and, can show more significantly through the time hardness rise, not preferred.Therefore, for needing ductility especially and beating the goods that use in the purposes of frothing capacity, in most cases need to implement temperature adjustment.Especially nearest, because the price of glyceride stock is surging, thereby can see the tendency of a large amount of uses as grease relatively cheap grease, that be derived from palm, and but be derived from the plastic fat composition of the grease of palm for a large amount of uses, then the tendency of rerum natura variation is bigger if do not carry out temperature adjustment.Therefore, a large amount of plastic fat compositions of the grease that is derived from palm that use just have requirement to implement the tendency of temperature adjustment more.In the non-patent literature 1 about palm oil put down in writing " the palm oil crystallization is slow, though after handling through the such chilling plasticizing device of margarine maker also ... in packing after the time hardening, cause the reduction of extensibility.", those skilled in the art know the poor properties of this fat or oil composition usually.Also put down in writing in addition, " ... owing to easily cause thickization of the crystal (growning of grease; Coarse), therefore in the past got the cooperation proportion control in margarine or the shortening very low.", in order not use palm oil, controlling its use level very low is a kind of method with ging wrong.
Temperature adjustment is carried out usually in the following way: keep certain hour (24 hours to 72 hours) in the storage vault temperature adjustment storehouse, that keeping a certain fixed temperature being called as, products temperature is warming up to curing temperature than the low some degree of softening point of grease contained in the goods.Therefore, the goods that need temperature adjustment are elongated from being fabricated onto goods needed time of dispatching from the factory, and can see the tendency that production efficiency reduces.In addition, every kind of goods need be set at the temperature adjustment storehouse of different temperatures, have cost burden to become big tendency from the equipment aspect.And then, goods once need put into the temperature adjustment storehouse and after temperature adjustment is finished, it transferred to freezer, operate pretty troublesome.
Bothering with time, the improvement of shortening above-mentioned temperature adjustment is purpose, and several applications are arranged.For example patent documentation 1 (Japanese kokai publication sho 52-151759 communique), patent documentation 2 (Japanese kokai publication sho 57-138343 communique), patent documentation 3 (Japanese kokai publication sho 59-41396 communique), patent documentation 4 (TOHKEMY 2007-37467 communique) expectation utilize microwave to be warming up to the temperature adjustment temperature by after being filled to plastic fat composition in the case, thereby obtain the effect equal with temperature adjustment.Yet, when utilizing microwave to heat up, because the degree of depth that partly declines of microwave is superficial, therefore need must be thinner with the THICKNESS CONTROL of case, versatility is low.In addition, be difficult to utilize microwave that object is heated up equably,, need utilize a plurality of microwave generators irradiating microwaves discontinuously as patent documentation 4.Therefore, need large-scale device, cost burden is bigger.
In addition, also has following application: as patent documentation 5 (Japanese kokai publication sho 59-6841 communique), be used in combination the intensification and the online intensification that utilizes microwave that utilize microwave after the vanning, as patent documentation 6 (Japanese kokai publication sho 59-6842 communique), patent documentation 7 (Japanese kokai publication sho 59-80499 communique), only utilize microwave that goods are warming up to target temperature in addition with online mode.About the method for patent documentation 5, make equalizing temperature aspect, think and compare more effectively with the method that only irradiating microwaves heats up after vanning that however, the degree of depth that partly declines of having to consider microwave adopts the size of case, versatility is low.The present application people also tries to reproduce the method for patent documentation 6,7, but can't achieve the goal with the condition of specification record.Especially for the cooperation of grease that a large amount of uses are derived from palm, its effect is low, is judged as and is difficult to replace thus temperature adjustment.
Originally, the online microwave that utilizes heats up in the method for patent documentation 5,6,7, but because the microwave generator part can not be used metal material, thereby resistance to pressure is low, is difficult in the physical device and uses.
Trial as improving temperature of articles with the means beyond the microwave has patent documentation 8 (Japanese kokai publication hei 2-182790).Use high frequency waves as the means that heat up herein.High frequency waves are compared the degree of depth that partly declines with microwave deep, therefore under the situation that goods is filled to irradiation high frequency waves in back in the case, compares and can set case darker with microwave.But however, it is bigger that the temperature in the temperature-rise ratio deep of near surface rises, and when irradiation was proceeded to the deep and reaches target temperature, the surface has been warming up to the degree that begins to melt, and was impracticable.
Patent documentation 1: Japanese kokai publication sho 52-151759 communique
Patent documentation 2: Japanese kokai publication sho 57-138343 communique
Patent documentation 3: Japanese kokai publication sho 59-41396 communique
Patent documentation 4: TOHKEMY 2007-37467 communique
Patent documentation 5: Japanese kokai publication sho 59-6841 communique
Patent documentation 6: Japanese kokai publication sho 59-6842 communique
Patent documentation 7: Japanese kokai publication sho 59-80499 communique
Patent documentation 8: Japanese kokai publication hei 2-182790 communique
Non-patent literature 1: " utilization of palm oil palm-kernel oil " adds rattan autumn man and writes P154 good fortune study nineteen ninety
Summary of the invention
The problem that invention will solve
The object of the present invention is to provide a kind of new autofrettage of plastic fat composition, will in the manufacturing of plastic fat composition, need " temperature adjustment " process efficiencyization of long period and troublesome poeration in the past.
The scheme that is used to deal with problems
The inventor etc. further investigate repeatedly to above-mentioned problem, found that, in the preparation of plastic fat composition, utilize on-line equipment to be warming up to the temperature adjustment temperature immediately even cool off after mixing, also can't obtain and the identical effect of temperature adjustment of using the temperature adjustment storehouse usually, but find by accident, mixing temperature is reduced to a certain fixing level by cooling off, be warming up to certain temperature through after certain holdup time then, thereby can access and the equal effect of common temperature adjustment, thereby finish the present invention.
That is, the present invention relates to
(1) a kind of autofrettage of plastic fat composition, it is characterized in that, the state chilling that concoction is melted fully from grease is mixing to than the temperature of low 12 ℃～27 ℃ of the softening point of grease and make it to separate out crystal, be warming up to softening fusing point with respect to grease then and be-5.0 ℃～+ 1.0 ℃ scope and the temperature below the rising fusing point, then, be filled in the packing container.
(2) according to (1) described manufacture method, wherein, contain the SUS type triglyceride of 5 weight %～37 weight % in the grease, wherein S is that saturated fatty acid, U are unrighted acid.
(3) according to (1) described autofrettage, wherein, the grease in the concoction contains the palmitic composition that is derived from more than the 20 weight %.
(4) according to each described autofrettage in (1)～(3), wherein, be to have in the pipeline of agitating function to carry out near the intensification the fusing point.
(5), wherein, refrigerate after being filled in the packing container according to each described autofrettage in (1)～(4).
(6) according to each described autofrettage in (1)～(5), wherein, plastic fat composition is any of margarine, low fat margarine, shortening.
The effect of invention
According to the present invention, temperature adjustment does not need for a long time, and becomes and do not need the temperature adjustment storehouse, and the goods that will once put into the temperature adjustment storehouse as previous methods are transferred to the such trouble of freezer once more and disappeared.Its result can more effectively produce plastic fat composition.
The specific embodiment
Below, the present invention is carried out specific description.
The raw material that use among the present invention can use with common plastic fat composition in the material identical materials used.About main raw material(s), be grease and water when margarine or low fat margarine, during shortening grease, as other auxiliary material, use skimmed milk power or whole milk powder etc. when margarine or low fat margarine sometimes.As additive, can suitably use emulsifying agent or spices in addition.Among the present invention, the liquid object that whole raw material are mixed is called concoction in addition.
As the grease that uses among the present invention, same with common plastic fat composition, can list animal raw fats such as rapeseed oil, soybean oil, sunflower oil, cottonseed oil, arachis oil, rice bran oil, corn oil, safflower oil, olive oil, kopok oil, sesame oil, evening primrose oil, palm oil, Butyrospermum grease, Bimbisara tree grease, cocoa butter, coconut oil, palm kernel wet goods vegetative grease and butterfat, butter, lard etc., these grease classes separately or miscella or these have been implemented to divide carry, the processing grease of curing, ester exchange etc.
Recently, the relatively cheap tendency that is derived from palmitic grease of a large amount of uses is arranged.Said palm oil only is meant and makes with extra care, do not divide and carry or the palm oil of processing such as curing, ester exchange among the present invention.In addition, be derived from that palmitic grease is meant palm oil itself and palm oil divided carry, processing and the general name of the grease that obtains more than a kind such as curing, ester exchange.In the ester exchange, do not influence other oil and plant also using of raw material.When being called " being derived from palmitic composition " in addition, for the grease of ester exchange, be meant the wherein contained palmitic composition that is derived from.
Cooperated when being derived from palmitic grease in a large number, had and contain the triglyceride of representing with SUS in a large number (S is that saturated fatty acid, U are unrighted acid.Below abbreviate SUS sometimes as.) tendency.The grease that contains SUS is not limited to and is derived from palmitic grease, also comprise deriving from and be derived from palmitic grease grease in addition, under the situation that finally becomes the prescription that in grease, contains a large amount of SUS, in order to give fat or oil composition, need to carry out temperature adjustment under the situation mostly as desired good hardness of goods and ductility.Among the present invention, when containing the SUS more than the 5 weight % in the grease of concoction, its effect is significantly embodied.In addition, SUS carries out temperature adjustment and also is difficult to obtain the good hardness and the tendency of ductility even have when surpassing the amount of 37 weight % in the grease of concoction.About the SUS amount in the contained grease of concoction of the present invention, the preferred scope of application is 7 weight %～33 weight %.
Cooperated when being derived from palmitic grease in a large number,, also had to carry out temperature adjustment under most situation owing to may be the influence of the essential factor except that SUS.For example, for having cooperated a large amount of fat or oil compositions that from palm oil, divide the low melting point fraction of putting forward,, have to carry out temperature adjustment under the situation mostly in order to give its rerum natura as goods.Usually, comprise ester exchange grease etc., contain in the contained total grease of concoction when being derived from palmitic composition more than the 20 weight %, have to carry out temperature adjustment under the situation mostly, under the situation of such a prescription, use that its effect is significantly embodied when of the present invention.In addition, contain in the contained total grease of concoction when being derived from palmitic composition more than the 25 weight %, effect of the present invention obtains more significant embodiment, when 30 weight % are above, are beneficial to and further embody effect of the present invention significantly.
The grease that uses among the present invention melted fully and suitably add emulsifying agent etc.Then, add water when margarine and low fat margarine.Water is based on water, be dissolved in auxiliary materials such as water-soluble skimmed milk power etc. in the water and obtain as required.Add water in the grease of fusing after, add spices etc. as required, agitation as appropriate and homogenising are made concoction.Therefore in addition, do not make water during shortening, the material that suitably adds emulsifying agent etc. and obtain in grease is called concoction.The concoction pumped liquid, carry out sterilization after, feed Kombinator
Perfector
Votator
Deng scraping type chilling mixer.Lower 12 ℃～27 ℃ and be more than 0 ℃ by the temperature behind scraping type chilling mixer expectation than the softening point of grease in the concoction, more expect lowlyer 14 ℃～27 ℃ and be more than 0 ℃ than the softening point of grease in the concoction, further expectation is lower 16 ℃～27 ℃ and be more than 0 ℃ than the softening point of grease in the concoction.When being higher than temperature than low 12 ℃ of the softening point of grease in the concoction by the temperature of charge behind the scraping type chilling mixing roll, the amount of the grease crystal that obtains is insufficient, and the rerum natura of goods is caused adverse influence, and is not preferred.In addition, when further being lower than temperature than low 27 ℃ of the softening point of grease in the concoction by the temperature of charge behind the scraping type chilling mixing roll, the concoction too cooling that becomes produces crystal quickly in the delay after this, be difficult to obtain preferred rerum natura.In addition, no matter under which kind of situation, when being lower than 0 ℃ by the temperature of charge behind the scraping type chilling mixing roll, the too cooling that not only becomes, and also may produce ice shape crystal when margarine and low fat margarine, not preferred.In addition, the assay method of the softening point of grease (ring and ball method) is according to " (1996) 1996 years versions of the Japanese oiling formulation reference oil fat analytical test method 2.2.4.3 of association ".
Behind scraping type chilling mixer, in device, be detained 140 seconds～600 seconds, more expectation is 150 seconds～500 seconds, further expectation is 160 seconds～450 seconds.Said herein " in the device " is meant in the production line of a series of plastic fat composition manufacturing installation.The holdup time that needs is according to the composition of grease and difference, but uses SUS or palm oil in a large number, elongated tendency of required holdup time is arranged when being derived from palmitic grease.In addition, though the adverse effect to the rerum natura of fat or oil composition is limited when spending the long holdup time, the holdup time, it is big that the volume of the arresting device that needs becomes, and therefore expects that the holdup time is short as far as possible when long.
Therefore the crystal growth of estimation grease between above-mentioned demurrage, but holdup time when being less than 140 seconds may be difficult to reach purpose of the present invention because the amount of grease crystal is also insufficient.On the other hand, the holdup time, the capacity that needs for delay was big when surpassing 600 seconds, and the cost burden of equipment aspect becomes excessive, and is not preferred.
Delay in device can be by continuously extra heavy pipe of connection and so on or the pin rotation machine etc. that is called as the B tube carry out from the chilling mixing machine.At this moment, be detained around the pipe, the chuck etc. and the warm water that circulates therein preferably suitably are set in order to prevent that fat or oil composition is attached to.When being detained with the B tube, preferred rotating shaft rotates as far as possible lentamente.In addition, the holdup time in the device also can be totally based on holdup time of the pipe arrangement capacity between jockey.
In addition, the method for patent documentation 6,7 needless to say makes device miniaturization as much as possible thereby pipe arrangement is lacked as far as possible, the direction design apparatus that loses with goods in the minimizing pipe arrangement under most in addition situation.Yet among the present invention, owing to heat up after being necessary in device, fully to produce crystal, therefore device need be designed in installing, can be detained 140 seconds～600 seconds time.
After being detained official hour, be heated near the processing of heating of fusing point.Heating continuously in manufacturing installation when handling, can make effectively, is preferred.Heat riser as this moment can use オ Application レ one タ one
Scraping type heat exchanger or multitube cylindrical heat exchangers (Japan system Co., Ltd.) such as (Co., Ltd. cherry make institute), (NORITAKECO. LIMITED) etc., but is not limited to these to the built-in heat exchanger of static mixer.Wherein, have in the pipeline agitating function the built-in heat exchanger of static mixer that area is set is few, be preferred.Also can utilize the intensification of microwave, but because the microwave generator part can not be used metal material, so resistance to pressure is not enough, is difficult to the manufacturing installation of industrial level.
An example during as the built-in heat exchanger of use static mixer, for oil content in the concoction is the margarine of 83 weight %, with respect to 16 ℃ of the products temperatures of the flow 53kg/hr of goods, heat exchanger entrance, when the heat-conducting area of heat exchanger is that 0.2 square metre, target temperature of charge are under 27 ℃ the situation, by warm water, thereby can will be increased to target temperature by the temperature of charge behind the heat exchanger with 32 ℃ of the flow heat exchanger of 325L/h circulations.This is a reference value, and its condition is different and different according to flow or prescription, target temperature of charge, the kind of heat exchanger or the size of heat-conducting area etc. of goods, so long as those skilled in the art just can easily impose a condition.But heat-conducting area too hour in order to obtain the target temperature of charge, is had to heat exchanger is set at higher temperature, but in this case, probably can be caused the fusing of goods, and is not preferred.As a reference value, the temperature of heat exchanger is higher more than 5 ℃ the time than the rising fusing point of grease contained in the concoction, causes that in heat exchanger inside the possibility of emulsification composition fusing is bigger, not preferred.In addition, rising Measurement of melting point method is according to " (1996) 1996 years versions of the Japanese oiling formulation reference oil fat analytical test method 2.2.4.2 of association ".
The softening point that the target temperature of charge is preferably with respect to grease in each concoction is-5.0 ℃～+ 1.0 ℃ scope and the temperature that is no more than the rising fusing point.More preferably the softening point with respect to grease is-4.0 ℃～+ 1.0 ℃ scope and the temperature that is no more than the rising fusing point, and more preferably the softening point with respect to grease is-4.0 ℃～+ 0.5 ℃ scope and the temperature that is no more than the rising fusing point.When temperature of charge also hanged down than the temperature that with respect to the softening point of grease in the concoction be-5 ℃, becoming was difficult to obtain the effect of temperature adjustment, not preferred.On the other hand, when temperature of charge is also higher than the temperature that with respect to the softening point of grease in the concoction is+1.0 ℃, or when also higher, might can melt by composition than rising fusing point, not preferred.
Preferably heat up afterwards, further pass through the B tube the goods homogenising with heat exchanger.Then, be filled in the case, but expectation capacity at this moment is more than the 5kg that more expectation is for more than the 10kg.Volume is during less than 5kg, and products temperature can descend at short notice when putting into freezer after this, and might become is difficult to obtain the effect of temperature adjustment.That is, among the present invention, supposition is after the goods that will be warming up to set point of temperature are filled in the case, in the process that the refrigeration storehouse temperature slowly reduces, caused the variation same with temperature adjustment, but should the time more in short-term, think finish with the same variation of temperature adjustment before, may reach low temperature.
Can transfer to freezer rapidly after being filled in the case, even but place at normal temperatures about 1 hour, influence also is limited.In addition, can use the freezer that in the past used.Then, as long as goods become 3 ℃～7 ℃ and can use.
About the evaluation of the goods that obtain, undertaken by the ductility evaluation of hardness and sense organ.By implementing temperature adjustment, hardness has the tendency of bigger improvement, and therefore, whether effectively hardness be to judge temperature adjustment operation key factor.
Below put down in writing embodiment.
Embodiment
＜embodiment 1 〉
Use Kombinator
To partly be by the grease of 83 weight % palm oil, palm solidified oil, super palm oil (Super Palm Olein) mixture (29.5 ℃ of softening points, 36.0 ℃ of rising fusing points, SUS containing ratio: 30 weight % in the grease of concoction, be derived from palmitic composition: 100 weight % in the grease of concoction), the water of 16 weight %, to amount to state (65 ℃) chilling that the emulsifying agent of 1 weight % and prescription A that spices is formed melt fully from grease mixing to 5 ℃, then with being detained pipe delay 180 seconds in device.Then, temperature of charge is risen to 28 ℃, by the B tube, in case, respectively fill 10kg then by the built-in heat exchanger of static mixer.The goods that obtain are transferred in the freezer immediately, after 48 hours, carried out quality evaluation.
" mensuration of hardness "
It is the cube of 5 ± 1cm on one side that the goods that obtain are cut into, and puts into 20 ℃ incubator, measures through the hardness after 24 hours.Hardness is to measure by using motionless industrial group system " flow graph " to be pressed into Φ 1cm plunger with the speed of 5cm/min.Prescription is during A, and it is qualified that the hardness of 100～280g/cm Φ is judged as.In addition, carry out sensory evaluation, carry out quality judging.
The result
" mensuration of hardness "
Hardness among the embodiment 1 is 160g/cm Φ, and is qualified.Ductility is also good on the sense organ.
＜comparative example 1 〉
Use Kombinator similarly to Example 1
The prescription A chilling of embodiment 1 is mixing after 5 ℃, be detained 180 seconds with being detained pipe.Utilize the built-in heat exchanger of static mixer that temperature of charge is warming up to 22.6 ℃ then, by the B tube, in case, respectively fill 10kg then.The goods that obtain are transferred in the freezer immediately, after 48 hours, carried out quality evaluation.
The result
" mensuration of hardness "
Measure hardness with method similarly to Example 1.Hardness in the comparative example 1 is 290g/cm Φ, and is defective.Ductility is also bad.
When prescription A is suitable for the number range of claim, use Kombinator
Intensification after chilling is mixing need be warming up to 24.5 ℃～30.5 ℃ scope, and only is warming up to 22.6 ℃ herein.As a result, the specification of hardness does not just fall into acceptable ranges.
＜embodiment 2 〉
Use Kombinator similarly to Example 1
The prescription A chilling of embodiment 1 is mixing after 5 ℃, be detained 180 seconds with being detained pipe.Utilize the built-in heat exchanger of static mixer that temperature of charge is warming up to 29.3 ℃ then, by the B tube, in case, respectively fill 10kg then.The goods that obtain are transferred in the freezer immediately, after 48 hours, carried out quality evaluation.
The result
" mensuration of hardness "
Measure hardness with method similarly to Example 1.Hardness among the embodiment 2 is 220g/cm Φ, and is qualified.Ductility is also good on the sense organ.
When prescription A is suitable for the number range of claim, use Kombinator
Intensification after chilling is mixing need be warming up to 24.5 ℃～30.5 ℃ scope, and is warming up to 29.3 ℃ herein.As a result, the specification of hardness is an acceptability limit.
＜embodiment 3 〉
Use Kombinator similarly to Example 1
The prescription A chilling of embodiment 1 is mixing after 5 ℃, be detained 180 seconds with being detained pipe.Utilize the built-in heat exchanger of static mixer that temperature of charge is warming up to 26.4 ℃ then, by the B tube, in case, respectively fill 10kg then.The goods that obtain are transferred in the freezer immediately, after 48 hours, carried out quality evaluation.
The result
" mensuration of hardness "
Measure hardness with method similarly to Example 1.Hardness among the embodiment 3 is 280g/cm Φ, and is qualified.Ductility is also good on the sense organ.
When prescription A is suitable for the number range of claim, use Kombinator
Intensification after chilling is mixing need be warming up to 24.5 ℃～30.5 ℃ scope, and is warming up to 26.4 ℃ herein.As a result, the specification of hardness is an acceptability limit.
＜embodiment 4 〉
Use Kombinator similarly to Example 1
The prescription A chilling of embodiment 1 is mixing after 16 ℃, be detained 150 seconds with being detained pipe.Utilize the built-in heat exchanger of static mixer that temperature of charge is warming up to 28.0 ℃ then, by the B tube, in case, respectively fill 10kg then.The goods that obtain are transferred in the freezer immediately, after 48 hours, carried out quality evaluation.
The result
" mensuration of hardness "
Measure hardness with method similarly to Example 1.Hardness among the embodiment 4 is 280g/cm Φ, and is qualified.Ductility is also good on the sense organ.
When being suitable for the number range of claim, use Kombinator
Temperature after chilling is mixing is 2.5 ℃～17.5 ℃ a scope, and is 16.0 ℃ herein.In addition, the holdup time expectation after chilling is mixing is 140 seconds～600 seconds, and implements 150 seconds herein.As a result, the specification of hardness is an acceptability limit.
＜comparative example 2 〉
Use Kombinator similarly to Example 1
The prescription A chilling of embodiment 1 is mixing after 10 ℃, be detained 120 seconds with being detained pipe.Utilize the built-in heat exchanger of static mixer that temperature of charge is warming up to 28.1 ℃ then, by the B tube, in case, respectively fill 10kg then.The goods that obtain are transferred in the freezer immediately, after 48 hours, carried out quality evaluation.
The result
" mensuration of hardness "
Measure hardness with method similarly to Example 1.Hardness in the comparative example 2 is 330g/cm Φ, and is defective.Ductility is also bad on the sense organ.
Holdup time expectation after chilling is mixing is 140 seconds～600 seconds, and implements 120 seconds herein.As a result, the specification of hardness is defective.
Utilizability on the industry
As previously discussed, the method for the application of the invention, thereby in the plastic fat composition that needs the temperature adjustment operation, can be with its production efficiency.
Claims (6)
1. the autofrettage of a plastic fat composition, it is characterized in that, the state chilling that concoction is melted fully from grease is mixing to than the temperature of low 12 ℃～27 ℃ of the softening point of grease and make it to separate out crystal, be warming up to softening fusing point with respect to grease then and be-5.0 ℃～+ 1.0 ℃ scope and the temperature below the rising fusing point, then, be filled in the packing container.
2. manufacture method according to claim 1 wherein, contains the SUS type triglyceride of 5 weight %～37 weight % in the grease, wherein S is that saturated fatty acid, U are unrighted acid.
3. autofrettage according to claim 1, wherein, the grease in the concoction contains the palmitic composition that is derived from more than the 20 weight %.
4. according to each described autofrettage in the claim 1～3, wherein, be to have in the pipeline of agitating function to carry out near the intensification the fusing point.
5. according to each described autofrettage in the claim 1～4, wherein, refrigerate after being filled in the packing container.
6. according to each described autofrettage in the claim 1～5, wherein, plastic fat composition is any of margarine, low fat margarine, shortening.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2008-255250 | 2008-09-30 | ||
| JP2008255250 | 2008-09-30 | ||
| PCT/JP2009/003791 WO2010038346A1 (en) | 2008-09-30 | 2009-08-07 | Method for producing plastic fat composition |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102131400A true CN102131400A (en) | 2011-07-20 |
| CN102131400B CN102131400B (en) | 2013-04-24 |
Family
ID=42073135
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN200980132839.8A Expired - Fee Related CN102131400B (en) | 2008-09-30 | 2009-08-07 | Method for producing plastic fat composition |
Country Status (3)
| Country | Link |
|---|---|
| JP (1) | JP5077438B2 (en) |
| CN (1) | CN102131400B (en) |
| WO (1) | WO2010038346A1 (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105208871A (en) * | 2013-03-07 | 2015-12-30 | 日清奥利友集团株式会社 | Emulsified oil composition |
| CN112040779A (en) * | 2018-04-27 | 2020-12-04 | 株式会社钟化 | Novel rolling margarine |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS63146750U (en) * | 1987-03-17 | 1988-09-28 | ||
| US5275835A (en) * | 1992-09-29 | 1994-01-04 | The Procter & Gamble Company | Process for preparing reduced calorie flavored confectionery compositions using dynamic tempering conditions |
| JP2001072992A (en) * | 1999-09-06 | 2001-03-21 | Snow Brand Milk Prod Co Ltd | Preparation of fat or fat composition free from generation of granular crystal |
| JP2001321080A (en) * | 2000-05-11 | 2001-11-20 | Kanegafuchi Chem Ind Co Ltd | Method for producing oil and fat-containing confectionery food and oil and fat-containing confectionery food |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS63146750A (en) * | 1986-12-10 | 1988-06-18 | Kanegafuchi Chem Ind Co Ltd | Preparation of fat and oil composition |
| JP4877775B2 (en) * | 2006-10-19 | 2012-02-15 | 株式会社Ａｄｅｋａ | Method for producing plastic fat composition |
-
2009
- 2009-08-07 JP JP2010531710A patent/JP5077438B2/en not_active Expired - Fee Related
- 2009-08-07 CN CN200980132839.8A patent/CN102131400B/en not_active Expired - Fee Related
- 2009-08-07 WO PCT/JP2009/003791 patent/WO2010038346A1/en active Application Filing
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS63146750U (en) * | 1987-03-17 | 1988-09-28 | ||
| US5275835A (en) * | 1992-09-29 | 1994-01-04 | The Procter & Gamble Company | Process for preparing reduced calorie flavored confectionery compositions using dynamic tempering conditions |
| JP2001072992A (en) * | 1999-09-06 | 2001-03-21 | Snow Brand Milk Prod Co Ltd | Preparation of fat or fat composition free from generation of granular crystal |
| JP2001321080A (en) * | 2000-05-11 | 2001-11-20 | Kanegafuchi Chem Ind Co Ltd | Method for producing oil and fat-containing confectionery food and oil and fat-containing confectionery food |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105208871A (en) * | 2013-03-07 | 2015-12-30 | 日清奥利友集团株式会社 | Emulsified oil composition |
| CN112040779A (en) * | 2018-04-27 | 2020-12-04 | 株式会社钟化 | Novel rolling margarine |
| CN112040779B (en) * | 2018-04-27 | 2024-01-09 | 株式会社钟化 | Novel roll-in margarine |
Also Published As
| Publication number | Publication date |
|---|---|
| WO2010038346A1 (en) | 2010-04-08 |
| JPWO2010038346A1 (en) | 2012-02-23 |
| JP5077438B2 (en) | 2012-11-21 |
| CN102131400B (en) | 2013-04-24 |
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