CN101954196B - Distillation recovery system - Google Patents

Distillation recovery system Download PDF

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Publication number
CN101954196B
CN101954196B CN2010102682882A CN201010268288A CN101954196B CN 101954196 B CN101954196 B CN 101954196B CN 2010102682882 A CN2010102682882 A CN 2010102682882A CN 201010268288 A CN201010268288 A CN 201010268288A CN 101954196 B CN101954196 B CN 101954196B
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distillation
tank
carbon dioxide
recovery system
trap
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CN101954196A (en
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石井郁男
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Actfive (shanghai) Washing Machines Manufacturing Co Ltd
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Actfive (shanghai) Washing Machines Manufacturing Co Ltd
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  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Cleaning By Liquid Or Steam (AREA)

Abstract

The invention discloses a distillation recovery system and is applied to the technical field of industrial cleaners. The distillation recovery system comprises a distillation tank, a carbon dioxide compressor and a carbon dioxide pressure reducer, wherein a heating loop is formed by a heater and the distillation tank; a cooling loop is formed by a cooler, a condensate tank and a circulating tank respectively; a carbon dioxide refrigerating and heating system is formed by the carbon dioxide compressor, the heater, the carbon dioxide pressure reducer and the cooler; and the distillation tank, the condensate tank and the circulating tank are sequentially connected through pipelines. The distillation recovery system has the advantages of simple structure, high energy utilization rate and convenient cleaning and maintenance.

Description

The distillation recovery system
Technical field
The present invention relates to industrial cleaning machine technical field, relate in particular to a kind of distillation recovery system.
Background technology
Used cleaning agent in the industry cleaning machine contaminatedly gradually in cleaning process is lost cleaning capacity for the cleaning agent waste liquid.If these cleaning agent waste liquids are directly outwelled, not only increase and clean cost, and can pollute environment.Therefore, need recycle processing to the cleaning agent waste liquid.
Usually adopt the distillation recovery system that the cleaning agent waste liquid is recycled processing, earlier the distillation of cleaning agent waste liquid is obtained cleaning agent volatilization composition, and then the cleaning agent composition condensation of volatilizing is obtained pure cleaning agent.In the distillation recovery system of prior art, needing external heat source usually provides the cleaning agent waste liquid of heat in the heating distillation tank that the low-volatile cleaning agent composition in the cleaning agent waste liquid is taken away in vacuum state evaporation and quilt; Simultaneously, need establish external source in addition is condensed into the cleaning agent composition of extracting out and becomes pure cleaning agent and flow out at condensate tank(trap).This not only needs a special heating so that distillation tank is heated with regard to making, and needs a special refrigeration system be used for the condensation of cleaning agent volatilization composition so that cold to be provided in addition.Therefore, there is baroque defective in existing distillation recovery system.
And; Because present heat, refrigeration system all is to adopt electric energy to carry out work; And we know that evaporation 1 premium on currency needs about 540 caloric heats; And 1 kilowatt of eletctric energy (KWE) can be converted into about 860 caloric heats, even under the situation that energy is very changed, 1 kilowatt energy approximately can only make 1.59 liters water evaporation.That is to say that present distillation recovery system directly utilizes electric energy to heat, freezing exists the defective that energy consumption is high, capacity usage ratio is low, it is unfavorable that enterprise's need energy-saving and emission-reduction that this and current social are advocated require.
In addition, the distillation tank that uses in the present distillation recovery system, its structure is that coil pipe is set in groove.During heating, be connected with the heating agent conduction oil in the coil pipe cleaning agent waste liquid is heated.Because coil pipe produces very high temperature after heating, make the impurity in the cleaning agent waste liquid be prone to be adsorbed near it, just make the coil pipe fouling for a long time.Coil pipe after the fouling the heating distillate the time, be prone to the heating uneven situation.Therefore, this regularly cleans distillation tank and coil pipe with regard to needs, because coil pipe is complicated helical structure, directly cleaning can't be carried out, and must coil pipe be dismantled during cleaning.Therefore, there is the defective of cleaning difficulty in existing distillation tank.
Summary of the invention
First technical problem to be solved by this invention provide a kind of simple in structure, capacity usage ratio is high, the distillation recovery system of saving the energy, to overcome the deficiency that prior art exists.
In order to solve the problems of the technologies described above, the present invention adopts following technical scheme:
A kind of distillation recovery system; Comprise distillation tank, carbon dioxide compression device and carbon dioxide pressure reducer; Heater and distillation tank form heating circuit; Cooler forms cooling circuit with condensate tank(trap) and circulating slot respectively, and carbon dioxide compression device, heater, carbon dioxide pressure reducer and cooler form the carbon dioxide refrigeration heating, and said distillation tank, condensate tank(trap), circulating slot are linked in sequence through pipeline.In the present invention, owing to only relate to distillation tank, condensate tank(trap), circulating slot, carbon dioxide refrigeration heating and carbon dioxide refrigeration heating in the whole distillation recovery system thermal source and low-temperature receiver can be provided simultaneously, therefore, the present invention has advantage of simple structure.
In addition, in the carbon dioxide refrigeration heating, on the one hand send heater to, realize heating distillation tank with producing heat in the carbon dioxide compression device carbon dioxide being compressed; On the other hand, pass to cooler and think that condensate tank(trap), circulating slot provide cold with in the carbon dioxide pressure reducer carbon dioxide of high pressure being discharged to obtain cold, same system can heat and can freeze.And this system 1 kilowatt of eletctric energy (KWE) approximately can produce 4300 caloric heats, and its efficient is about 5 times of the prior art, and therefore, the present invention also has the capacity usage ratio height, the advantage that can economize on resources.
Second technical problem to be solved by this invention is that distillation tank can convenient for cleaningly be safeguarded; For this reason; Distillation tank of the present invention comprises cell body and is arranged at the groove lid on the cell body that heating interlayer and said cell body bottom interior wall that said cell body bottom has hollow are pasted with one deck high-temperature resistant membrane.
In distillation tank distillation cleaning agent waste liquid process, bubble can be produced, and impurity can be mingled with in the bubble, in order to access pure cleaning agent volatilization composition, the present invention is in further improving, and said groove lid below is provided with an electromagnetic shaker.This electromagnetic shaker can be shatter with bubble, sneaks into down-stream in the bubble thereby avoided impurity to be mixed in, thereby avoiding influencing reclaims the pure of the cleaning agent that obtains.The heating-up temperature of heater of the present invention is 90-100 ℃; The chilling temperature of cooler is 15-20 ℃.
In order the cleaning agent condensation fluid power in the condensate tank(trap) successfully to be transferred to circulating slot; Also include circulating pump and threeway, said circulating slot and circulating pump, threeway form closed circuit, said threeway one end communication loop pump; One end communication loop groove, the other end is communicated with condensate tank(trap).Abundant for the condensation that further guarantees cleaning agent volatilization composition, between said condensate tank(trap) and distillation tank, also be provided with heat exchanger, said cooler and condensate tank(trap), heat exchanger also form a cooling circuit.
Therefore, in sum, that distillation recovery system of the present invention has is simple in structure, energy utilizes high, cleaning advantage easily.
Description of drawings
Fig. 1 is a system schematic of the present invention;
Fig. 2 is a distillation tank system schematic of the present invention.
Among the figure: 100-cleaning agent waste liquid inlet 200-filter 300-distillation tank 301-cell body 302-groove lid 303-carrier pipe 304-hollow heating interlayer 305-high-temperature resistant membrane 306-electromagnetic shaker 400-heat exchanger 500-condensate tank(trap) 600-circulating slot 601-circulating pump 602-threeway 700-outlet 800-carbon dioxide refrigeration heating 801-cooler 802-heater 803-compressor reducer 804-pressure reducer 900-heat is used heat exchanger.
The specific embodiment
Below in conjunction with specific embodiment the present invention is further described:
See also Fig. 1, it is a system schematic of the present invention, comprises filter 200, distillation tank 300, heat exchanger 400, condensate tank(trap) 500, circulating slot 600 and carbon dioxide refrigeration heating 800.
Axial-flow pump sucks the cleaning agent waste liquid from the cleaning agent waste liquid inlet 100 that distills the recovery system bottom, be mixed with impurity such as impurity, dirt, iron powder usually owing in the cleaning agent waste liquid, the cleaning agent waste liquid is filtered to be delivered to through filter 200 reach distillation tank 300.
See also Fig. 2, distillation tank 300 comprises cell body 301, groove lid 302, and groove lid 302 covers on cell body 301, and makes whole distillation tank 300 inside be in sealing through sealing means.Hollow heating interlayer 304 is arranged in cell body 301 bottoms, and the inside is connected with the heating agent conduction oil.Be connected in carrier pipe 303 1 ends on the groove lid 302, carrier pipe 303 other ends are connected with condensate tank(trap) 500.
Cleaning agent waste liquid in cell body 301 the insides through the heating agent heat-conducting oil heating of 304 li of empty heating interlayers, makes the volatilization of cleaning agent composition and passes through carrier pipe 303 to condensate tank(trap) 500 conveyings.
Groove covers 302 belows and is provided with an electromagnetic shaker 306.Electromagnetic shaker 306 can be shatter with bubble, sneaks into down-stream in the bubble thereby avoided impurity to be mixed in, thereby avoiding influencing reclaims the pure of the cleaning agent that obtains.
Distillation tank 300 also is included in cell body 301 bottom interior wall and is pasted with one deck high-temperature resistant membrane 305, and high-temperature resistant membrane 305 is high temperature resistant about the 150 ℃ resin films of ability.When distillation tank 300 is carried out the cleaning of inner dirt, only need high-temperature resistant membrane 305 taken off from cell body 301 bottoms get final product, need not to adopt in addition again cleaning agent or water to clean cell body inside, economize on resources, reduce pollution, clear up very convenient.
See also Fig. 1, carbon dioxide refrigeration heating 800 is formed by carbon dioxide compression device 803, heater 802, carbon dioxide pressure reducer 804 and cooler 801.
Distillation tank 300 forms heating circuit through heat release with heat exchanger 900 and heater 802.802 pairs of heating agent heat-conducting oil heating of heater, this gives distillation tank 300 the insides cleaning agent waste liquid heating to be processed indirectly.
In distillation tank 300, the low volatilization composition in the cleaning agent waste liquid is heated volatilization and is detached distillation tank 300, and the cleaning agent volatilization composition of being taken away arrives condensate tank(trap) 500 through heat exchanger 400.
Condensate tank(trap) 500 and circulating slot 600 rely on cooler 801 coolings, and condensate tank(trap) 500 and circulating slot 600 form cooling circuit with cooler 801 respectively.
In condensate tank(trap) 500, cleaning agent volatilization composition is condensed into the cleaning agent condensate liquid, and condensate liquid is through circulating slot 600 and export 700 outflow systems.
In order the cleaning agent condensation fluid power in the condensate tank(trap) 500 successfully to be transferred to circulating slot 600; Also include circulating pump 601 and threeway 602; Said circulating slot 600 forms closed circuit with circulating pump 601, threeway 602; Said threeway 602 1 end communication loop pumps 601, one end communication loop grooves 600, the other end is communicated with condensate tank(trap) 500.
Abundant for the condensation that further guarantees cleaning agent volatilization composition, between condensate tank(trap) 500 and distillation tank 300, also be provided with heat exchanger 400, cooler 801 also forms a cooling circuit with condensate tank(trap) 500, heat exchanger 400.
In the carbon dioxide refrigeration heating 800, on the one hand send heater 802 to, realize heating distillation tank 300 with producing heat in the carbon dioxide compression device 803 carbon dioxide being compressed; On the other hand, pass to cooler 801 and think that condensate tank(trap) 500, circulating slot 600 provide cold with in the carbon dioxide pressure reducer 804 carbon dioxide of high pressure being discharged to obtain cold, same system can heat and can freeze.And this system 1 kilowatt of eletctric energy (KWE) approximately can produce 4300 caloric heats, and its efficient is about 5 times of the prior art, and therefore, the present invention also has the capacity usage ratio height, the advantage that can economize on resources.
Owing to only relate to distillation tank 300, condensate tank(trap) 500, circulating slot 600, carbon dioxide refrigeration heating 800 and carbon dioxide refrigeration heating 800 in the whole distillation recovery system thermal source and low-temperature receiver, advantage of simple structure can be provided simultaneously.
This makes and need not be provided with under the situation of independent external heat source and external source that the recycling through carbon dioxide refrigeration heating 800 realization cleaning agent waste liquids not only simplifies the structure, and reaches the environmental protection purpose of energy-saving and emission-reduction.

Claims (7)

1. one kind is distilled recovery system; It is characterized in that: comprise distillation tank, carbon dioxide compression device and carbon dioxide pressure reducer; Heater and distillation tank form heating circuit; Cooler forms cooling circuit with condensate tank(trap) and circulating slot respectively, and carbon dioxide compression device, heater, carbon dioxide pressure reducer and cooler form the carbon dioxide refrigeration heating, and said distillation tank, condensate tank(trap), circulating slot are linked in sequence through pipeline.
2. distillation recovery system according to claim 1 is characterized in that: said distillation tank comprises cell body and is arranged at the groove lid on the cell body that heating interlayer and said cell body bottom interior wall that said cell body bottom has hollow are pasted with one deck high-temperature resistant membrane.
3. distillation recovery system according to claim 2 is characterized in that: said groove lid below is provided with an electromagnetic shaker.
4. distillation recovery system according to claim 1 is characterized in that: the heating-up temperature of said heater is 90-100 ℃.
5. distillation recovery system according to claim 1 is characterized in that: the chilling temperature of said cooler is 15-20 ℃.
6. distillation recovery system according to claim 1; It is characterized in that: also include circulating pump and threeway, said circulating slot and circulating pump, threeway form closed circuit, said threeway one end communication loop pump; One end communication loop groove, the other end is communicated with condensate tank(trap).
7. distillation recovery system according to claim 1 is characterized in that: also be provided with heat exchanger between said condensate tank(trap) and the distillation tank, said cooler and condensate tank(trap), heat exchanger also form a cooling circuit.
CN2010102682882A 2010-08-27 2010-08-27 Distillation recovery system Active CN101954196B (en)

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Publication number Priority date Publication date Assignee Title
CN103288154B (en) * 2013-05-15 2015-04-08 中色科技股份有限公司 Device and method for recovering metal material surface cleaning agent
CN103520942B (en) * 2013-10-12 2015-08-12 象山医疗精密仪器有限公司 Medicine concentration and evaporation device
CN108096866A (en) * 2018-01-31 2018-06-01 深圳市鑫承诺环保产业股份有限公司 Hydrocarbon solution recovery device
CN109621472A (en) * 2018-12-27 2019-04-16 昆山城东化工有限公司 A kind of multistage cooling recovery system for organic solvent

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Publication number Priority date Publication date Assignee Title
CN1846827A (en) * 2005-04-15 2006-10-18 上海科伟达超声波科技有限公司 Vacuum distillation process for recovering and regenerating washing liquid
CN101002991A (en) * 2006-01-20 2007-07-25 梁诗文 Closing circulation type system for recovering solvent
CN201216885Y (en) * 2008-07-08 2009-04-08 江苏卡特石油新能源有限公司 Methanol recycling apparatus
CN201551863U (en) * 2009-12-03 2010-08-18 立邦涂料(中国)有限公司 Solvent recovery system and reactor thereof

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH09290101A (en) * 1996-04-24 1997-11-11 Asahi Seimitsu Kk Cleaning liquid recycling device

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1846827A (en) * 2005-04-15 2006-10-18 上海科伟达超声波科技有限公司 Vacuum distillation process for recovering and regenerating washing liquid
CN101002991A (en) * 2006-01-20 2007-07-25 梁诗文 Closing circulation type system for recovering solvent
CN201216885Y (en) * 2008-07-08 2009-04-08 江苏卡特石油新能源有限公司 Methanol recycling apparatus
CN201551863U (en) * 2009-12-03 2010-08-18 立邦涂料(中国)有限公司 Solvent recovery system and reactor thereof

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