CN101884896A - Automatic extraction experimental device of high-pressure reactor - Google Patents
Automatic extraction experimental device of high-pressure reactor Download PDFInfo
- Publication number
- CN101884896A CN101884896A CN 201010206696 CN201010206696A CN101884896A CN 101884896 A CN101884896 A CN 101884896A CN 201010206696 CN201010206696 CN 201010206696 CN 201010206696 A CN201010206696 A CN 201010206696A CN 101884896 A CN101884896 A CN 101884896A
- Authority
- CN
- China
- Prior art keywords
- pressure reactor
- autoclave
- cooling device
- motor
- pressure
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Images
Abstract
The invention discloses an automatic extraction experimental device of a high-pressure reactor, comprising an electric furnace (1) on which a vertical heating hole (2) is arranged. A high-pressure reactor (3) is arranged in the heating hole, a gold tube capable of containing a sample is arranged in the high-pressure reactor, a high-pressure water pipeline (4) communicated into the high-pressure reactor is connected to the high-pressure reactor connected with a steel wire rope (5), the upper end of the steel wire rope is connected with a motor (6) capable of driving the steel wire rope to move up and down, the side above the heating hole is provided with a temperature sensor (7) and a cooling device (8), the motor, the temperature sensor and the cooling device are connected with an automatic controller (9), the temperature sensor outputs signals to the automatic controller, and the automatic controller outputs the signals to the motor and the cooling device for controlling the work of the motor and the cooling device. The invention can realize automatic control, thereby improving the working efficiency, reducing the labor intensity and improving the time accuracy of a sampling point. Due to unmanned operation, the automatic extraction experimental device can prevent the accident leakage of high-pressure steam or the ejection of high-pressure parts so that human bodies can not be hurt.
Description
Technical field
The present invention relates to a kind of automatic extraction experimental device of high-pressure reactor that is used for petroleum gas geochemical investigation field.
Background technology
At present, in petroleum gas geochemical investigation field, need organic quantity and the composition that is subjected to thermogenetic oil gas in the research stratum.At present advanced method is that sample is encapsulated in the gold pipe, the golden pipe that sample is housed is put into the autoclave that stainless steel is done, and injects water under high pressure by pipeline in still, and water under high pressure flattens the gold pipe, thereby sample is wherein exerted pressure.A series of autoclaves that golden pipe is housed are put into electric furnace, make the electric furnace temperature programming, in certain temperature the specific autoclave that golden pipe is housed is taken out from electric furnace, and analyze the oil gas that sample in the golden pipe produces, just can know under conditions such as uniform temperature, pressure, heated time the quantity and the composition of the organic oil gas that produces.Because once testing the autoclave of putting into same electric furnace has more than 14, need take out autoclave one by one by certain hour, abroad all be the method for manually on time autoclave being taken out from stove that adopts at present, this method labour intensity big (once testing sustainable 20 days), and certain risk is arranged.For addressing this problem, this patent has manufactured and designed automatic extraction experimental device of high-pressure reactor.
Summary of the invention
The object of the present invention is to provide a kind of automatic extraction experimental device of high-pressure reactor that can automatically autoclave be taken out and cool off automatically from electric furnace.
For solving the problems of the technologies described above, the technical solution used in the present invention is: automatic extraction experimental device of high-pressure reactor, comprise electric furnace, be provided with vertical bottoming hole above the electric furnace, be provided with autoclave in the bottoming hole, be provided with the gold pipe that to install sample in the autoclave, be connected to the high-pressure water pipeline that is communicated in the autoclave on the autoclave, described autoclave is connected to steel wire rope, the upper end of steel wire rope is connected to and can drives the motor that steel wire rope moves up and down, sidepiece above bottoming hole is provided with temperature detector and cooling device, described motor, temperature detector and cooling device are connected with automatic controller, temperature detector outputs signal to automatic controller, and automatic controller outputs signal to motor and cooling device with control motor and cooling device work.
The oral area of described bottoming hole is provided with ceramic cap, the ceramic cap dimidiation, and the outside of two halves is arranged on the electric furnace rotationally.
Described ceramic cap middle part is provided with the through hole that can supply high-pressure water pipeline to pass, and through hole is surrounded by the ceramic cap of two halves.
Described cooling device is made of water spout and the valve that is arranged on the water spout, and valve is connected with automatic controller.
The lower end of described steel wire rope is connected on the high-pressure water pipeline by securing member.
Described high-pressure water pipeline is provided with the pneumatic high-voltage water valve.
Described pneumatic high-voltage water valve is connected with automatic controller.
Described bottoming hole is 14.
When the present invention worked, electric furnace heated autoclave, arrive sample time after, motor by steel wire rope autoclave upwards traction the electric furnace bottoming hole is proposed.After autoclave proposed electric furnace, temperature detector detected autoclave, and temperature detector outputs signal to automatic controller, and automatic controller outputs signal to cooling device with the work of control cooling device, thereby autoclave is lowered the temperature rapidly.The action of motor, temperature detector and cooling device is subjected to the control of automatic controller, can carry out automatically according to predefined program.
Owing to adopted above-mentioned structure, action of the present invention can be carried out automatically according to predefined program, realizes control automatically, thereby can increase work efficiency, and reduces the time accuracy of labour intensity and raising sample point.Because of unattended, can avoid ejecting injury to human body because of high steam accidental release or high voltage component.
Description of drawings
Below in conjunction with accompanying drawing the specific embodiment of the present invention is described in further detail.
Fig. 1 is the structural representation of automatic extraction experimental device of high-pressure reactor;
Fig. 2 is that motor, temperature detector, cooling device and automatic controller are connected block diagram;
Fig. 3 is that autoclave is put into bottoming hole structural representation before;
Fig. 4 is that autoclave is put into bottoming hole structural representation afterwards;
The structural representation that Fig. 5 is an autoclave when bottoming hole takes out;
Fig. 6 is the structural representation after autoclave takes out from bottoming hole.
The specific embodiment
As shown in Figure 1 and Figure 2, automatic extraction experimental device of high-pressure reactor of the present invention comprises electric furnace 1, is provided with vertical bottoming hole 2 above the electric furnace 1, and described bottoming hole 2 is 14, and annular spread is on electric furnace 1.Be provided with autoclave 3 in the described bottoming hole 2, be provided with the gold pipe that can install sample in the autoclave 3, be connected to the high-pressure water pipeline 4 that is communicated in the autoclave 3 on the autoclave 3, described high-pressure water pipeline 4 is provided with pneumatic high-voltage water valve 15.Described autoclave 3 is connected to steel wire rope 5, and the lower end of described steel wire rope 5 can be connected on the high-pressure water pipeline 4 by securing member 14.The upper end of described steel wire rope 5 is connected to and can drives the motor 6 that steel wire rope 5 moves up and down, and motor 6 is a reducing motor, the stable action of motor 6, and speed can be set arbitrarily, the functional reliability height.Sidepiece above bottoming hole 2 is provided with temperature detector 7 and cooling device 8.Temperature detector 7 is infrared temperature detectors, and after autoclave 3 proposed electric furnace, autoclave 3 temperature were higher, and infrared temperature detector 7 may detect autoclave 3.Described motor 6, temperature detector 7 and cooling device 8 are connected with automatic controller 9, and temperature detector 7 outputs signal to automatic controller 9, and automatic controller 9 outputs signal to motor 6 and cooling device 8 is worked with control motor 6 and cooling device 8.Described pneumatic high-voltage water valve 15 also links to each other with automatic controller 9, and automatic controller 9 can be controlled the open and close of pneumatic high-voltage water valve 15.
Described cooling device 8 can be made of water spout 12 and the valve 13 that is arranged on the water spout 12, valve 13 is connected with automatic controller 9, automatic controller 9 exportable signals open or close for valve 13 with by-pass valve control 12, realize the automatic control to cooling device 8 work.
To shown in Figure 6, the oral area of described bottoming hole 2 is provided with ceramic cap 10 as Fig. 3, ceramic cap 10 dimidiations, and the outside of two halves is arranged on the electric furnace 1 rotationally.When autoclave 3 proposed, ceramic cap 10 can be backed down by autoclave 3, and after autoclave 3 proposed, ceramic cap 10 also can automatically reset in the gravity effect and cover on bottoming hole 2.Described ceramic cap 10 middle parts are provided with the through hole 11 that can supply high-pressure water pipeline 4 to pass, and through hole 11 is surrounded by the ceramic cap 10 of two halves.
When the present invention specifically works, as shown in Figure 3, earlier open ceramic cap 10 laterally, starter motor 6 is transferred steel wire rope 5, and autoclave 3 is put into the bottoming hole 2 of electric furnace along the direction of arrow, then ceramic cap 10 is resetted, and this moment as shown in Figure 4.Open pneumatic high-voltage water valve 15 then, electric furnace begins autoclave 3 heating.After arriving sample time, automatic controller 9 outputs signal to pneumatic high-voltage water valve 15, closes pneumatic high-voltage water valve 15, and automatic controller 9 outputs signal to motor 6 simultaneously, motor 6 upwards draws high-pressure water pipeline 4 by steel wire rope 5, thereby autoclave 3 is proposed electric furnace bottoming holes 2.When autoclave 3 proposed, ceramic cap 10 was opened automatically, and this moment as shown in Figure 5.After autoclave 3 proposed, ceramic cap 10 can automatically reset in the gravity effect and cover on bottoming hole 2, prevents energy dissipation.After autoclave 3 proposes electric furnace, infrared temperature detector 7 detects autoclave 3, output signal to automatic controller 9, automatic controller 9 outputs signal to cooling device 8 and opens with the valve 12 of control cooling device 8, cooling water is vaporific and sprays to autoclave 3 by water spout 12, thereby autoclave 3 is lowered the temperature rapidly.The action of motor 6, temperature detector 7 and cooling device 8 is subjected to the control of automatic controller 9, can carry out automatically according to predefined program.
In a word; though the present invention has exemplified above-mentioned preferred implementation, should illustrate, though those skilled in the art can carry out various variations and remodeling; unless such variation and remodeling have departed from scope of the present invention, otherwise all should be included in protection scope of the present invention.
Claims (8)
1. automatic extraction experimental device of high-pressure reactor, comprise electric furnace (1), be provided with vertical bottoming hole (2) above the electric furnace (1), be provided with autoclave (3) in the bottoming hole (2), be provided with the gold pipe that to install sample in the autoclave (3), be connected to the high-pressure water pipeline (4) that is communicated in the autoclave (3) on the autoclave (3), it is characterized in that: described autoclave (3) is connected to steel wire rope (5), the upper end of steel wire rope (5) is connected to and can drives the motor (6) that steel wire rope (5) moves up and down, sidepiece in bottoming hole (2) top is provided with temperature detector (7) and cooling device (8), described motor (6), temperature detector (7) and cooling device (8) are connected with automatic controller (9), temperature detector (7) outputs signal to automatic controller (9), and automatic controller (9) outputs signal to motor (6) and cooling device (8) is worked with control motor (6) and cooling device (8).
2. according to the described automatic extraction experimental device of high-pressure reactor of claim 1, it is characterized in that: the oral area of described bottoming hole (2) is provided with ceramic cap (10), ceramic cap (10) dimidiation, and the outside of two halves is arranged on the electric furnace (1) rotationally.
3. according to the described automatic extraction experimental device of high-pressure reactor of claim 2, it is characterized in that: described ceramic cap (10) middle part is provided with the through hole (11) that can supply high-pressure water pipeline (4) to pass, and through hole (11) is surrounded by the ceramic cap (10) of two halves.
4. according to claim 1 or 2 or 3 described automatic extraction experimental device of high-pressure reactor, it is characterized in that: described cooling device (8) is made of water spout (12) and the valve (13) that is arranged on the water spout (12), and valve (13) is connected with automatic controller (9).
5. according to claim 1 or 2 or 3 described automatic extraction experimental device of high-pressure reactor, it is characterized in that: the lower end of described steel wire rope (5) is connected on the high-pressure water pipeline (4) by securing member (14).
6. according to claim 1 or 2 or 3 described automatic extraction experimental device of high-pressure reactor, it is characterized in that: described high-pressure water pipeline (4) is provided with pneumatic high-voltage water valve (15).
7. according to the described automatic extraction experimental device of high-pressure reactor of claim 6, it is characterized in that: described pneumatic high-voltage water valve (15) is connected with automatic controller (9).
8. according to claim 1 or 2 or 3 described automatic extraction experimental device of high-pressure reactor, it is characterized in that: described bottoming hole (2) is 14.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201010206696 CN101884896B (en) | 2010-06-22 | 2010-06-22 | Automatic extraction experimental device of high-pressure reactor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201010206696 CN101884896B (en) | 2010-06-22 | 2010-06-22 | Automatic extraction experimental device of high-pressure reactor |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101884896A true CN101884896A (en) | 2010-11-17 |
| CN101884896B CN101884896B (en) | 2013-06-05 |
Family
ID=43071084
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201010206696 Expired - Fee Related CN101884896B (en) | 2010-06-22 | 2010-06-22 | Automatic extraction experimental device of high-pressure reactor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101884896B (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6074610A (en) * | 1997-05-22 | 2000-06-13 | Exxonmobil Upstream Research Company | Multi-sample reactor |
| CN101149363A (en) * | 2007-10-29 | 2008-03-26 | 中国科学院广州地球化学研究所 | Rock sample hydrocarbon generation kinetics high pressure thermal simulation experimental method and device |
| CN201313045Y (en) * | 2008-11-26 | 2009-09-23 | 中国科学院广州地球化学研究所 | Hydrocarbon generation kinetics high-pressure thermal simulation device of rock sample |
| CN201752645U (en) * | 2010-06-22 | 2011-03-02 | 中国科学院广州地球化学研究所 | Automatic extraction experimental device of high-pressure reactor |
-
2010
- 2010-06-22 CN CN 201010206696 patent/CN101884896B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6074610A (en) * | 1997-05-22 | 2000-06-13 | Exxonmobil Upstream Research Company | Multi-sample reactor |
| CN101149363A (en) * | 2007-10-29 | 2008-03-26 | 中国科学院广州地球化学研究所 | Rock sample hydrocarbon generation kinetics high pressure thermal simulation experimental method and device |
| CN201313045Y (en) * | 2008-11-26 | 2009-09-23 | 中国科学院广州地球化学研究所 | Hydrocarbon generation kinetics high-pressure thermal simulation device of rock sample |
| CN201752645U (en) * | 2010-06-22 | 2011-03-02 | 中国科学院广州地球化学研究所 | Automatic extraction experimental device of high-pressure reactor |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101884896B (en) | 2013-06-05 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104567418B (en) | A kind of energy-saving control method of recuperative heater discharging door | |
| CN109236250A (en) | A kind of supercritical CO2Pressure break coal petrography enhances coal bed gas harvesting simulation experiment method and system | |
| CN204807353U (en) | Quality of water sampling test device based on thing networking | |
| CN105033987B (en) | Intelligent manipulator and automatic incubator assembly control method thereof | |
| CN201752645U (en) | Automatic extraction experimental device of high-pressure reactor | |
| CN104280188B (en) | A kind of pressure sensor chip automated testing method and device thereof | |
| CN201314635Y (en) | Novel human body induction infrared stove controller | |
| CN101884896B (en) | Automatic extraction experimental device of high-pressure reactor | |
| CN205898798U (en) | Concrete freeze -thaw cycle and axial pressurized composite set | |
| CN104695878A (en) | Remote control type hydraulic clamp device and control method | |
| CN204203021U (en) | A kind of high-temperature high-pressure in-situ Compound Fretting Wear test unit | |
| CN104338390A (en) | PLC based automatic bag dedusting control system and method | |
| CN107643151A (en) | A kind of fire-fighting spraying head device for detecting sealability | |
| CN204534530U (en) | Heating tube dry burning device is prevented on electric heating steam generator | |
| CN201921533U (en) | Automatic liquid drainage and collection device | |
| CN203385622U (en) | Water pressure testing device for mechanical product | |
| CN206792253U (en) | A kind of automatic steam heating machine | |
| CN105363239A (en) | Traditional Chinese medicine extraction device for detecting extraction rate in real time | |
| CN107481779A (en) | A kind of target piece transfer tool | |
| CN202968656U (en) | Experimental device for pre-heating and drying pellets | |
| CN104680895A (en) | Teaching experimental device about influence of air pressure on boiling point | |
| CN203212536U (en) | Automatic coal detection device used for gas producer | |
| CN203719647U (en) | Automatic detection device for outer diameter of high temperature furnace tube | |
| CN110090088B (en) | Poultry production mobile vehicle | |
| CN207077663U (en) | A kind of automotive upholstery base material hot oil heater |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20130605 Termination date: 20140622 |
|
| EXPY | Termination of patent right or utility model |