CN101874929A - Desuperheating device in alkali vaporization station - Google Patents

Desuperheating device in alkali vaporization station Download PDF

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Publication number
CN101874929A
CN101874929A CN2010101899007A CN201010189900A CN101874929A CN 101874929 A CN101874929 A CN 101874929A CN 2010101899007 A CN2010101899007 A CN 2010101899007A CN 201010189900 A CN201010189900 A CN 201010189900A CN 101874929 A CN101874929 A CN 101874929A
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China
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tube connector
evaporator
evaporimeter
alkali
tube
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CN2010101899007A
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CN101874929B (en
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彭小红
杜修权
朱仁华
郑美娟
弧素琴
李军华
马荣辉
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Chang Hua machine (Suzhou) heavy equipment Co., Ltd.
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Zhangjiagang Chemical Machinery Co Ltd
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Abstract

The invention discloses a desuperheating device in an alkali vaporization station, which comprises a first desuperheater, a second desuperheater and a third desuperheater, wherein the first desuperheater, the second desuperheater and the third desuperheater are connected through connection water branch pipes and cooling water pipes respectively, and all the connection water branch pipes are respectively provided with a regulating valve and a flow meter. The invention has the advantages that desuperheating device in the alkali vaporization station can cool produced overheated secondary vapor into saturated vapor with corresponding pressure parameter, so that the heat transfer efficiency of an evaporator is greatly increased, and the evaporation efficiency of the whole evaporator is also increased. Meanwhile, desuperheating water injected into the evaporator becomes vapor, the quantity of heating vapor is increased, and the consumption of new vapor is saved.

Description

Desuperheating device in the alkali vaporization station
Technical field
The present invention relates to a kind of alkali evaporation technique, relate in particular to the Desuperheating device in a kind of alkali vaporization station.
Background technology
The existing alkali vaporization station structure that is used for the alkali evaporation mainly comprises: first evaporimeter, second evaporimeter and the 3rd evaporimeter, an identical tube type falling-film heater and the evaporator of all comprising of the structure of first evaporimeter, second evaporimeter and the 3rd evaporimeter; The stoste import of first tube type falling-film heater upper end is connected with former liquid bath by feed tube, the indirect steam outlet of first evaporator upper end is connected with stram condenser by first escape pipe, the alkali lye outlet of the first evaporator lower end is connected by the stoste import of first tube connector with second tube type falling-film heater upper end, and first tube connector is provided with first alkali pump; The indirect steam outlet of second evaporator upper end is connected with the first tube type falling-film heater by second escape pipe, the alkali lye outlet of the second evaporator lower end is connected by the stoste import of second tube connector with three-tube type falling film heating device upper end, and second tube connector is provided with second alkali pump; Three-tube type falling film heating device is connected with the initial steam air inlet pipe, the 3rd preheater is connected with the condensation water pot, the indirect steam outlet of the 3rd evaporator upper end is connected with the second tube type falling-film heater by the 3rd escape pipe, the alkali lye outlet of the 3rd evaporator lower end is connected with the alkali groove by the 3rd tube connector, the 3rd tube connector is provided with the 3rd alkali pump and cooling device, the 3rd tube connector and second tube connector are together by first preheater, the 3rd tube connector and first tube connector be second preheater together, and the 3rd tube connector passes through the 3rd preheater with cooling water pipe.During use, the initial steam that boiler comes enters the 3rd evaporimeter and heats the alkali lye that second evaporimeter comes, the indirect steam that the 3rd evaporimeter produces enters second evaporimeter and heats the alkali lye that first evaporimeter comes, the indirect steam that second evaporimeter produces enters first evaporimeter and heats the alkali lye that former liquid caustic soda groove comes, and the indirect steam that first evaporimeter produces advances stram condenser by heat exchange becomes condensed water with cooling water.Many weeks, alkali lye has ebullioscopic characteristics: promptly the boiling point of alkali lye is than the boiling point height with water under the pressure parameter, and along with the rising of concentration of lye, the boiling point liter of alkali lye is also just big more.The indirect steam of three evaporator generations all is a superheated steam.If directly the indirect steam that produces is delivered in corresponding next evaporimeter, do not undergo phase transition from overtemperature to the saturation temperature stage so, promptly be equivalent to incoagulable gas, the existence of incoagulable gas has a strong impact on the heat-transfer effect of evaporimeter, as in the heating steam if there is 1% incoagulable gas, the overall heat-transfer coefficient of evaporimeter will descend about 60% so.
Summary of the invention
Technical problem to be solved by this invention is: the Desuperheating device in a kind of alkali vaporization station that the indirect steam that produces can be become saturated vapor is provided.
In order to solve the problems of the technologies described above, the technical solution used in the present invention is: the Desuperheating device in the alkali vaporization station, comprise: first evaporimeter, second evaporimeter and the 3rd evaporimeter, an identical tube type falling-film heater and the evaporator of all comprising of the structure of first evaporimeter, second evaporimeter and the 3rd evaporimeter; The stoste import of first tube type falling-film heater upper end is connected with former liquid bath by feed tube, the indirect steam outlet of first evaporator upper end is connected with stram condenser by first escape pipe, the alkali lye outlet of the first evaporator lower end is connected by the stoste import of first tube connector with second tube type falling-film heater upper end, and first tube connector is provided with first alkali pump; The indirect steam outlet of second evaporator upper end is connected with the first tube type falling-film heater by second escape pipe, the alkali lye outlet of the second evaporator lower end is connected by the stoste import of second tube connector with three-tube type falling film heating device upper end, and second tube connector is provided with second alkali pump; Three-tube type falling film heating device is connected with the initial steam air inlet pipe, the indirect steam outlet of the 3rd evaporator upper end is connected with the second tube type falling-film heater by the 3rd escape pipe, the alkali lye outlet of the 3rd evaporator lower end is connected with the alkali groove by the 3rd tube connector, the 3rd tube connector is provided with the 3rd alkali pump, the 3rd tube connector and second tube connector are together by first preheater, the 3rd tube connector and first tube connector be second preheater together, the 3rd tube connector passes through the 3rd preheater with cooling water pipe, on described first escape pipe, first attemperator is set, described second escape pipe is provided with second attemperator, described the 3rd escape pipe is provided with the 3rd attemperator, first attemperator, second attemperator is connected with cooling water pipe by being connected the water arm respectively with the 3rd attemperator, all is respectively arranged with control valve and flowmeter on connection water arm.
In order to solve the problems of the technologies described above better, the further technical scheme that the present invention adopts is: described first tube connector is provided with first connecting branch, and first connecting branch is by the 4th preheater; Described second tube connector is provided with second connecting branch, and second connecting branch is by the 5th preheater; Described three-tube type falling film heating device is connected with the condensation water pot by the 4th tube connector, and the lower end of condensation water pot is connected with condensate pipe, and condensate pipe is successively by the 5th preheater and the 4th preheater.
In order to solve the problems of the technologies described above better, the further technical scheme that the present invention adopts is: described first evaporimeter, second evaporimeter and the 3rd evaporimeter are split-type evaporator, and the tube type falling-film heater is connected with evaporator by tube connector.
Advantage of the present invention is: the Desuperheating device in the above-mentioned alkali vaporization station, and the overheated indirect steam cooling that produces can be become the saturated vapor under the relevant pressure parameter, thereby improve the heat transfer efficiency of evaporimeter greatly, also improved the evaporation efficiency of whole evaporate station.Simultaneously, the desuperheating water that sprays in the attemperator can become steam, has increased the heating steam amount, has saved the consumption of initial steam.
Description of drawings
Fig. 1 is the structural principle schematic diagram of the Desuperheating device in the alkali vaporization station of the present invention.
Among the figure: 1, the first tube type falling-film heater, 2, feed tube, 3, former liquid bath, 4, first evaporator, 5, first escape pipe, 6, first tube connector, 7, the second tube type falling-film heater, 8, first alkali pump, 9, second evaporator, 10, second escape pipe, 11, second tube connector, 12, three-tube type falling film heating device, 13, second alkali pump, 14, the initial steam air inlet pipe, 15, the 3rd evaporator, 16, the 3rd escape pipe, 17, the 3rd tube connector, 18, the alkali groove, 19, the 3rd alkali pump, 20, first preheater, 21, second preheater, 22, cooling water pipe, 23, the 3rd preheater, 24, first connecting branch, 25, the 4th preheater, 26, second connecting branch, 27, the 5th preheater, 28, the 4th tube connector, 29, the condensation water pot, 30, condensate pipe, 31, the 5th tube connector, 32, the 6th tube connector, 33, the 7th tube connector, 34, stram condenser, 35, first attemperator, 36, second attemperator, 37, the 3rd attemperator, 38, connect the water arm, 39, cooling water pipe, 40, control valve, 41, flowmeter.
The specific embodiment
Describe particular content of the present invention in detail below in conjunction with the drawings and specific embodiments.
As shown in Figure 1, the Desuperheating device in the alkali vaporization station comprises: first evaporimeter, second evaporimeter and the 3rd evaporimeter, an identical tube type falling-film heater and the evaporator of all comprising of the structure of first evaporimeter, second evaporimeter and the 3rd evaporimeter; The stoste import of the first tube type falling-film heater, 1 upper end is connected with former liquid bath 3 by feed tube 2, the indirect steam outlet of first evaporator, 4 upper ends is connected with stram condenser 34 by first escape pipe 5, the alkali lye outlet of first evaporator, 4 lower ends is connected by the stoste import of first tube connector 6 with the second tube type falling-film heater, 7 upper ends, and first tube connector 6 is provided with first alkali pump 8; The indirect steam outlet of second evaporator, 9 upper ends is connected with the first tube type falling-film heater 1 by second escape pipe 10, the alkali lye outlet of second evaporator, 9 lower ends is connected by the stoste import of second tube connector 11 with three-tube type falling film heating device 12 upper ends, and second tube connector 12 is provided with second alkali pump 13; Three-tube type falling film heating device 12 is connected with initial steam air inlet pipe 14, the indirect steam outlet of the 3rd evaporator 15 upper ends is connected with the second tube type falling-film heater 7 by the 3rd escape pipe 16, the alkali lye outlet of the 3rd evaporator 15 lower ends is connected with alkali groove 18 by the 3rd tube connector 17, the 3rd tube connector 17 is provided with the 3rd alkali pump 19, described the 3rd tube connector 17 and second tube connector 11 are together by first preheater 20, described the 3rd tube connector 17 and first tube connector 6 be second preheater 21 together, and described the 3rd tube connector 17 passes through the 3rd preheater 23 with cooling water pipe 22.On described first escape pipe 5, first attemperator 35 is set, described second escape pipe 10 is provided with second attemperator 36, described the 3rd escape pipe 16 is provided with the 3rd attemperator 37, first attemperator 35, second attemperator 36 and the 3rd attemperator 37 are connected with cooling water pipe 39 by being connected water arm 38 respectively, all are respectively arranged with control valve 40 and flowmeter 41 on connection water arm 38.
In the present embodiment, described first tube connector 6 is provided with first connecting branch, 24, the first connecting branches 24 by the 4th preheater 25; Described second tube connector 11 is provided with second connecting branch, 26, the second connecting branches 26 by the 5th preheater 27; Described three-tube type falling film heating device 12 is connected with condensation water pot 29 by the 4th tube connector 28, and the lower end of condensation water pot 29 is connected with condensate pipe 30, and condensate pipe 30 is successively by the 5th preheater 27 and the 4th preheater 25.
In the present embodiment, described first evaporimeter, second evaporimeter and the 3rd evaporimeter are split-type evaporator, the tube type falling-film heater is connected with evaporator by tube connector, as shown in Figure 1, the first tube type falling-film heater 1 is connected with first evaporator 4 by the 5th tube connector 31, the second tube type falling-film heater 7 is connected with second evaporator 9 by the 6th tube connector 32, and three-tube type falling film heating device 12 is connected with the 3rd evaporator 15 by the 7th tube connector 33.
During the alkali evaporation, vaporizing raw liquor in the former liquid bath 3 (alkali of low concentration) enters into the first tube type falling-film heater 1 by feed tube 2, enter into first evaporator 4 through the 5th tube connector 31 then, concentration increases after first evaporator evaporation concentrates, and the indirect steam that produces in the evaporation process is discharged to enter into through first escape pipe 5 and carried out condensation in the indirect steam condenser 34.By first alkali pump 8 alkali lye is transported in the second tube type falling-film heater 7 by first tube connector 6 and first connecting branch 24, at this moment, first tube connector 6 can carry out heat exchange by second preheater 21 and the 3rd tube connector 17, makes low temperature alkali lye in first tube connector 6 and the high temperature alkaline solution in the 3rd tube connector 17 carry out heat exchange and obtains intensification.First connecting branch 24 carries out heat exchange by the 4th preheater 25 and condensate pipe 30, makes low temperature alkali lye in first connecting branch 24 carry out heat exchange with the high-temperature condensation water in the condensate pipe 30 and obtains intensification.Alkali lye in the second tube type falling-film heater 7 enters into second evaporator 9 through the 6th tube connector 32, concentration continues to increase after second evaporator evaporation concentrates, and the indirect steam that produces in the evaporation process enters into the first tube type falling-film heater 1 through second escape pipe 10.By second alkali pump 13 alkali lye is transported in the three-tube type falling film heating device 12 by second tube connector 11 and second connecting branch 26, at this moment, second tube connector 11 can carry out heat exchange by first preheater 20 and the 3rd tube connector 17, makes low temperature alkali lye in second tube connector 11 and the high temperature alkaline solution in the 3rd tube connector 17 carry out heat exchange and obtains intensification.Second connecting branch 26 carries out heat exchange by the 5th preheater 27 and condensate pipe 30, makes low temperature alkali lye in second connecting branch 26 carry out heat exchange with the high-temperature condensation water in the condensate pipe 30 and obtains intensification.Alkali lye in the three-tube type falling film heating device 12 enters into the 3rd evaporator 15 through the 7th tube connector 33, concentration reaches requirement after the 3rd evaporator evaporation concentrates, by the 3rd alkali pump 19 high temperature alkaline solution is carried by the 3rd tube connector 17, in course of conveying, high temperature alkaline solution in the 3rd tube connector 17 can carry out heat exchange with low temperature alkali lye in second tube connector 11 and the low temperature alkali lye in first tube connector 6, carry out heat exchange by the 3rd preheater 23 with cooling water pipe 22 at last, make the temperature of alkali reach requirement, enter into alkali groove 18 at last and carry out the finished product storage tank.The initial steam that boiler comes enters into three-tube type falling film heating device 12 by initial steam air inlet pipe 14, the high-temperature condensation water that produces enters in the condensation water pot 29 by the 4th tube connector 28, high-temperature condensation water in the condensation water pot 29 enters into condensate pipe 30, high-temperature condensation water in the condensate pipe 3 can carry out heat exchange with low temperature alkali lye in second connecting branch 26 and the low temperature alkali lye in first connecting branch 24, the temperature of condensed water is reduced, meet user's temperature parameter requirement, its heat energy is utilized effectively, reduce the consumption of initial steam and cooling water, reduced energy consumption.
When the Desuperheating device in the alkali vaporization station of said structure is used for the alkali evaporation, introduce cooling water by cooling water pipe 39, by control system each control valve 40 and flowmeter 41 are controlled, in corresponding attemperator 36, spray into an amount of cooling water by each connecting branch 38 cooling of overheated indirect steam is become saturated vapor under the relevant pressure parameter, thereby improved the heat transfer efficiency of evaporimeter greatly, also improved the evaporation efficiency of whole evaporate station.Simultaneously, the desuperheating water that sprays in the attemperator can become steam, has increased the heating steam amount, has saved the consumption of initial steam.
The foregoing description is only for the usefulness that the present invention is described; and be not to be limitation of the present invention; the those of ordinary skill in relevant technologies field; without departing from the spirit and scope of the present invention; can also make various variations and modification, so all technical schemes that are equal to also should belong to protection category of the present invention.

Claims (3)

1. the Desuperheating device in the alkali vaporization station comprises: first evaporimeter, second evaporimeter and the 3rd evaporimeter, an identical tube type falling-film heater and the evaporator of all comprising of the structure of first evaporimeter, second evaporimeter and the 3rd evaporimeter; The stoste import of first tube type falling-film heater upper end is connected with former liquid bath by feed tube, the indirect steam outlet of first evaporator upper end is connected with stram condenser by first escape pipe, the alkali lye outlet of the first evaporator lower end is connected by the stoste import of first tube connector with second tube type falling-film heater upper end, and first tube connector is provided with first alkali pump; The indirect steam outlet of second evaporator upper end is connected with the first tube type falling-film heater by second escape pipe, the alkali lye outlet of the second evaporator lower end is connected by the stoste import of second tube connector with three-tube type falling film heating device upper end, and second tube connector is provided with second alkali pump; Three-tube type falling film heating device is connected with the initial steam air inlet pipe, the indirect steam outlet of the 3rd evaporator upper end is connected with the second tube type falling-film heater by the 3rd escape pipe, the alkali lye outlet of the 3rd evaporator lower end is connected with the alkali groove by the 3rd tube connector, the 3rd tube connector is provided with the 3rd alkali pump, the 3rd tube connector and second tube connector are together by first preheater, the 3rd tube connector and first tube connector be second preheater together, the 3rd tube connector passes through the 3rd preheater with cooling water pipe, it is characterized in that: on described first escape pipe, first attemperator is set, described second escape pipe is provided with second attemperator, described the 3rd escape pipe is provided with the 3rd attemperator, first attemperator, second attemperator is connected with cooling water pipe by being connected the water arm respectively with the 3rd attemperator, all is respectively arranged with control valve and flowmeter on connection water arm.
2. according to the Desuperheating device in the described alkali vaporization station of claim 1, it is characterized in that: described first tube connector is provided with first connecting branch, and first connecting branch is by the 4th preheater; Described second tube connector is provided with second connecting branch, and second connecting branch is by the 5th preheater; Described three-tube type falling film heating device is connected with the condensation water pot by the 4th tube connector, and the lower end of condensation water pot is connected with condensate pipe, and condensate pipe is successively by the 5th preheater and the 4th preheater.
3. according to the Desuperheating device in claim 1 or the 2 described alkali vaporization stations, it is characterized in that: described first evaporimeter, second evaporimeter and the 3rd evaporimeter are split-type evaporator, and the tube type falling-film heater is connected with evaporator by tube connector.
CN2010101899007A 2010-05-31 2010-05-31 Desuperheating device in alkali vaporization station Active CN101874929B (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108686399A (en) * 2018-06-24 2018-10-23 茌平信发华兴化工有限公司 Piece alkali is secondary to coagulate into resin tower regenerative system

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5843202A (en) * 1981-09-07 1983-03-12 Toray Ind Inc Removing method for scale stuck to multiple effect evaporator
CN2094375U (en) * 1991-05-22 1992-01-29 刘继希 Three effect combined concentrator
CN2542308Y (en) * 2002-04-10 2003-04-02 李志贤 Combined double-effect concentration evaporator
JP2007136374A (en) * 2005-11-21 2007-06-07 Sasakura Engineering Co Ltd Evaporating/concentrating device
CN201157698Y (en) * 2008-02-01 2008-12-03 赵玉斌 Multi-effect evaporation compression apparatus
CN201727975U (en) * 2010-05-31 2011-02-02 张家港化工机械股份有限公司 Temperature reducing device in alkali evaporation station

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5843202A (en) * 1981-09-07 1983-03-12 Toray Ind Inc Removing method for scale stuck to multiple effect evaporator
CN2094375U (en) * 1991-05-22 1992-01-29 刘继希 Three effect combined concentrator
CN2542308Y (en) * 2002-04-10 2003-04-02 李志贤 Combined double-effect concentration evaporator
JP2007136374A (en) * 2005-11-21 2007-06-07 Sasakura Engineering Co Ltd Evaporating/concentrating device
CN201157698Y (en) * 2008-02-01 2008-12-03 赵玉斌 Multi-effect evaporation compression apparatus
CN201727975U (en) * 2010-05-31 2011-02-02 张家港化工机械股份有限公司 Temperature reducing device in alkali evaporation station

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108686399A (en) * 2018-06-24 2018-10-23 茌平信发华兴化工有限公司 Piece alkali is secondary to coagulate into resin tower regenerative system
CN108686399B (en) * 2018-06-24 2024-03-29 茌平信发华兴化工有限公司 Regeneration system of caustic soda flake secondary condensation resin tower

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