CN101811931A - Energy-saving vinyl chloride conversion dehydrating device - Google Patents

Energy-saving vinyl chloride conversion dehydrating device Download PDF

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Publication number
CN101811931A
CN101811931A CN201010159063A CN201010159063A CN101811931A CN 101811931 A CN101811931 A CN 101811931A CN 201010159063 A CN201010159063 A CN 201010159063A CN 201010159063 A CN201010159063 A CN 201010159063A CN 101811931 A CN101811931 A CN 101811931A
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China
Prior art keywords
gas mixture
mixed gas
energy
acid mist
preheater
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Granted
Application number
CN201010159063A
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Chinese (zh)
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CN101811931B (en
Inventor
陈炳谦
王志杰
曹占国
张明友
张学辉
杨善厚
赵清
杜建军
王林喜
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Tangshan Alkali Chloride Co., Ltd.
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Tangshan Alkali Chloride Co Ltd
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Priority to CN2010101590633A priority Critical patent/CN101811931B/en
Publication of CN101811931A publication Critical patent/CN101811931A/en
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Publication of CN101811931B publication Critical patent/CN101811931B/en
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency

Abstract

The invention belongs to a vinyl chloride monomer preparation device, more particularly to an energy-saving vinyl chloride conversion dehydrating device, which comprises a mixer, graphite coolers, acid mist filters and a preheater and further comprises a mixed gas heat exchanger, wherein a shell side inlet of the mixed gas heat exchanger is connected with a gas outlet of the mixer through a connecting pipeline and a shell side outlet of the mixed gas heat exchanger is connected with the gas inlet of a primary graphite cooler through the connecting pipeline, the primary graphite cooler, a secondary graphite cooler, a primary acid mist filter and a secondary acid mist filter are connected with each other in sequence through the connecting pipeline, a gas outlet of the secondary acid mist filter is connected with a tube side inlet of the mixed gas heat exchanger through the connecting pipeline, and a tube side outlet of the mixed gas heat exchanger is connected with the preheater through the connecting pipeline. The device cools the deep cooling-prior mixed gas by demisting-subsequent cooling energy to save the cooling energy, and simultaneously, a part of heat is obtained by the deep-cooled mixed gas after demisting to economize on the circulation amount of hot water of the preheater, thus the energy consumption is obviously lowered.

Description

Energy-saving vinyl chloride conversion dehydrating device
Technical field
The invention belongs to the vinyl chloride monomer preparation facilities, specifically a kind of energy-saving vinyl chloride conversion dehydrating device.
Background technology
At present, the vinyl chloride monomer preparation facilities by mixing tank, one-level graphite cooler, secondary graphite cooler, two-stage acid mist strainer,, preheater constitutes, the principle of work of this device is: the refining acetylene gas of being sent here by the acetylene operation mixes in mixing tank with the hydrogen chloride gas that the hydrogenchloride device is sent here, enter and carry out degree of depth cooled dehydrated in the I and II graphite cooler, enter two-stage acid mist strainer afterwards and further remove acid mist, enter preheater again and heat.The method of the first deep cooling that this existing device embodied, back heat has caused the lot of energy waste.
Summary of the invention
The present invention is intended to solve the problem of a large amount of energy wastages that have the existence of vinyl chloride monomer preparation facilities now, and provide a kind of gas mixture before utilizing cold after the demist to deep cooling to cool off, deep cooling gas mixture after the demist simultaneously obtains the part heat, to save the energy-saving vinyl chloride conversion dehydrating device of preheater hot water circulation amount.
The technical scheme that the present invention solves its technical problem employing is: a kind of energy-saving vinyl chloride conversion dehydrating device, comprise mixing tank, the one-level graphite cooler, the secondary graphite cooler, the primary acids mist resistant filter, secondary acid mist strainer, preheater, it also comprises a gas mixture interchanger, its shell side import of this gas mixture interchanger is connected with the pneumatic outlet of mixing tank by connecting tube, its shell side outlet is connected by the gas feed of connecting tube with the one-level graphite cooler, this one-level graphite cooler, the secondary graphite cooler, the primary acids mist resistant filter, secondary acid mist strainer connects by connecting tube successively, the pneumatic outlet of this secondary acid mist strainer is connected with the tube side import of this gas mixture interchanger by connecting tube, and the tube side outlet of this gas mixture interchanger is connected with this preheater by connecting tube.
Compared with prior art, the invention has the beneficial effects as follows: between lyophilization and preheater, increased the gas mixture interchanger, gas mixture before using cold after the demist to deep cooling cools off has saved cold, deep cooling gas mixture after the demist simultaneously obtains the part heat, has saved the hot water circulation amount of preheater.Adopt vinyl chloride monomer preparation facilities of the present invention, energy consumption obviously reduces, and quality product improves, stable operation.
Description of drawings
Fig. 1 is a structural representation of the present invention.
Fig. 2 is a gas mixture heat exchanger structure synoptic diagram of the present invention.
Among the figure: connecting tube 1, gas mixture interchanger 2, one-level graphite cooler 3, secondary graphite changes water cooler 4, primary acids mist resistant filter 5, secondary acid mist strainer 6, mixing tank 7, preheater 8, shell side import 9, shell side outlet 10, tube side import 11, tube side outlet 12, shell 13, tubulation 14, sieve plate 15.
Embodiment
Below in conjunction with drawings and Examples in detail the present invention is described in detail:
As Fig. 1, shown in Figure 2, energy-saving vinyl chloride conversion dehydrating device is by connecting tube 1, gas mixture interchanger 2, one-level graphite cooler 3, secondary graphite changes water cooler 4, primary acids mist resistant filter 5, secondary acid mist strainer 6, mixing tank 7, preheater 8 constitutes, these gas mixture interchanger 2 its shell side imports 9 are connected with the pneumatic outlet of mixing tank 7 by connecting tube 1, its shell side outlet 10 is connected with the gas feed of one-level graphite cooler 3 by connecting tube 1, this one-level graphite cooler 3, secondary graphite cooler 4, primary acids mist resistant filter 5, secondary acid mist strainer 6 connects by connecting tube 1 successively, the pneumatic outlet of this secondary acid mist strainer 6 is connected with the tube side import 11 of this gas mixture interchanger 2 by connecting tube 1, and the tube side outlet 12 of this gas mixture interchanger 2 is connected with this preheater 8 by connecting tube 1.
The interchanger 2 of gas mixture described in the present embodiment is made of shell 13, tubulation 14, sieve plate 15, and this shell 13 is tubular construction, is welded with the tubulation 14 of vertical setting in it by upper and lower sieve plate 15.
The graphite cooler of one-level described in the present embodiment 3, secondary graphite change water cooler 4, primary acids mist resistant filter 5, secondary acid mist strainer 6, mixing tank 7, preheater 8 and are conventional equipment in the existing vinyl chloride monomer preparation facilities.
The working process of energy-saving vinyl chloride conversion dehydrating device is summarized as follows: after the hydrogen chloride gas that refining acetylene gas of being sent here by the acetylene operation and hydrogenchloride device are sent here mixes in mixing tank 7, through the outlet of mixing tank 7 by connecting tube 1 and in shell side import 9 enters the housing 13 of gas mixture interchanger 2, again by the shell side outlet 10 of gas mixture interchanger 2 and the import that enters one-level graphite heat exchanger 3 through connecting tube 1, thus successively by one-level graphite heat exchanger 3, secondary graphite heat exchanger pipe connecting 4, primary acids mist resistant filter 5, secondary acid mist strainer 6, again in the tubulation in tube side import 11 enters gas mixture interchanger 2 14, enter preheater 8 through tube side outlet 12 again by connecting tube 1 then.
In this device, gas mixture has carried out the exchange of cold and hot amount in by the process of gas mixture interchanger 2 at twice, realized that the gas mixture before cold after the demist is to deep cooling cools off to save cold, deep cooling gas mixture after the demist has simultaneously obtained the part heat, has saved the hot water circulation amount of preheater 8 again.

Claims (2)

1. energy-saving vinyl chloride conversion dehydrating device, comprise mixing tank, the one-level graphite cooler, the secondary graphite cooler, the primary acids mist resistant filter, secondary acid mist strainer, preheater, it is characterized in that, it also comprises a gas mixture interchanger, its shell side import of this gas mixture interchanger is connected with the pneumatic outlet of mixing tank by connecting tube, its shell side outlet is connected by the gas feed of connecting tube with the one-level graphite cooler, this one-level graphite cooler, the secondary graphite cooler, the primary acids mist resistant filter, secondary acid mist strainer connects by connecting tube successively, the pneumatic outlet of this secondary acid mist strainer is connected with the tube side import of this gas mixture interchanger by connecting tube, and the tube side outlet of this gas mixture interchanger is connected with this preheater by connecting tube.
2. energy-saving vinyl chloride conversion dehydrating device according to claim 1 is characterized in that, described gas mixture interchanger is made of shell, tubulation, sieve plate, and this shell is tubular construction, is welded with the tubulation of vertical setting in it by upper and lower sieve plate.
CN2010101590633A 2010-04-29 2010-04-29 Energy-saving vinyl chloride conversion dehydrating device Active CN101811931B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2010101590633A CN101811931B (en) 2010-04-29 2010-04-29 Energy-saving vinyl chloride conversion dehydrating device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2010101590633A CN101811931B (en) 2010-04-29 2010-04-29 Energy-saving vinyl chloride conversion dehydrating device

Publications (2)

Publication Number Publication Date
CN101811931A true CN101811931A (en) 2010-08-25
CN101811931B CN101811931B (en) 2013-05-22

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CN2010101590633A Active CN101811931B (en) 2010-04-29 2010-04-29 Energy-saving vinyl chloride conversion dehydrating device

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3285980A (en) * 1960-05-02 1966-11-15 Dynamit Nobel Ag Process for the production of vinyl chloride
CN101544530A (en) * 2009-03-21 2009-09-30 青岛科技大学 Method for deep removal of water in ethyne and chlorine hydride mixed gas
CN201694975U (en) * 2010-04-29 2011-01-05 唐山氯碱有限责任公司 Energy-saving vinyl chloride conversion dewatering device

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3285980A (en) * 1960-05-02 1966-11-15 Dynamit Nobel Ag Process for the production of vinyl chloride
CN101544530A (en) * 2009-03-21 2009-09-30 青岛科技大学 Method for deep removal of water in ethyne and chlorine hydride mixed gas
CN201694975U (en) * 2010-04-29 2011-01-05 唐山氯碱有限责任公司 Energy-saving vinyl chloride conversion dewatering device

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
吴丽君,郝章来: "氯乙烯合成混合冷冻脱水工艺的技术改进", 《中国氯碱》 *

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Address after: 063305 Nanpu Development Zone, Hebei, Tangshan City

Patentee after: Tangshan Alkali Chloride Co., Ltd.

Address before: 063305 Nanpu Development Zone, Hebei, Tangshan City

Patentee before: Tangshan Alkali Chloride Co., Ltd.