CN101811719A - Aluminium trichloride synthesizing catcher set - Google Patents
Aluminium trichloride synthesizing catcher set Download PDFInfo
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- CN101811719A CN101811719A CN200910154986A CN200910154986A CN101811719A CN 101811719 A CN101811719 A CN 101811719A CN 200910154986 A CN200910154986 A CN 200910154986A CN 200910154986 A CN200910154986 A CN 200910154986A CN 101811719 A CN101811719 A CN 101811719A
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- catcher
- trap
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- little
- small
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- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Abstract
The invention discloses an aluminium trichloride synthesizing catcher set, and belongs to the technical field of aluminium trichloride synthesizing equipment. The aluminium trichloride synthesizing catcher set consists of an air inlet, a big catcher, a connecting pipe, an air outlet, a small catcher, a small catcher butterfly valve operating rod, a small catcher discharge hole, a lower connecting pipe, a big catcher butterfly valve operating rod and a big catcher discharge hole, and is characterized in that: the right side of the big catcher is connected with the small catcher through the connecting pipe; the small catcher is connected with three small catchers with the same type row by row through the lower connecting pipe and the connecting pipe; the big catcher is reserved with the air inlet and the big catcher butterfly valve operating rod; and the small catcher is reserved with the small catcher butterfly valve operating rod. The aluminium trichloride synthesizing catcher set has the advantages of simple design, low cost, convenience and practicability, and high practicability so as to improve product purity and meet the requirements of pharmaceutical factories.
Description
Affiliated technical field
The present invention relates to a kind of aluminium trichloride synthesizing catcher group, relate in particular to a kind of one big four little aluminium trichloride synthesizing catcher group, belong to Aluminum chloride anhydrous synthesis device technical field.
Background technology
At present, the aluminium trichloride synthesizing catcher of known technology is made 1.2 meters of diameters, the big trap that staving is 2.6 meters is used to collect the gaseous state Aluminum chloride anhydrous by on the chlorination furnace sublimation pipe, if in building-up process, infiltrate the irony of denier, will make Aluminum chloride anhydrous yellowing or brown, gray product appears even, domestic many pharmaceutical factories press for the pure Aluminum chloride anhydrous of white, thereby begin to attract much attention, before the present invention does not make, none big four little aluminium trichloride synthesizing catcher group is used, the patent searching document, and no technical scheme is open.
Summary of the invention
In order to overcome in the prior art deficiency of none big four little aluminium trichloride synthesizing catcher group, the objective of the invention is for a kind of one big four little aluminium trichloride synthesizing catcher group is provided, this aluminium trichloride synthesizing catcher group can supportingly be used in the chlorination synthetic furnace of prior art, the gaseous state Aluminum chloride anhydrous that pours on the sublimation pipe can be captured crystallization by a big trap to the Aluminum chloride anhydrous gaseous state that contains irony, simultaneously the Aluminum chloride anhydrous gas that does not have irony is entered the interior capture of four the little traps crystallization of back, unnecessary residual chlorine can be assembled in big trap bottom, absorb by entering the environmental protection pond after the discharging, and can in four little traps, collect the Aluminum chloride anhydrous of white, reach disposable purification purpose.
The present invention solves the technical scheme that its technical problem takes: by inlet mouth, big trap, pipe connecting, the air outlet, little trap, little trap butterfly valve operating stick, little capture discharge port, following pipe connecting, big trap butterfly valve operating stick, big trap discharge port is formed, it is characterized in that big trap the right connects little trap through pipe connecting, little trap warp pipe connecting down is connected three little traps of the same type by row with pipe connecting, leave inlet mouth on the big trap, big trap butterfly valve operating stick, leave little trap butterfly valve operating stick on the little trap, during installation inlet mouth is connected with sublimation pipe, packing of product bag is inserted on big trap discharge port and the little trap discharge port and gets final product, after the gaseous state Aluminum chloride anhydrous in the sublimation pipe pours in big trap, be subjected to temperature to reduce reason, the crystallization on big trap inwall of gaseous state Aluminum chloride anhydrous, the gaseous state Aluminum chloride anhydrous that purity is high enters in the little trap, in like manner be subjected to temperature to reduce reason, the crystallization on little trap inwall of gaseous state Aluminum chloride anhydrous, through after a few hours, beat the yellow Aluminum chloride anhydrous xln that can obtain contain iron on the iron wall of the Tie Bi of big trap and little trap at big trap discharge port with iron hammer, little trap discharge port obtains white iron-free Aluminum chloride anhydrous xln.
Beneficial effect of the present invention is a simplicity of design, and is with low cost, convenient and practical, to improve product purity, satisfies the needs in pharmaceutical factory, and practicality is big.
Description of drawings
The invention will be further described below in conjunction with drawings and Examples.
Fig. 1 is a synoptic diagram of the present invention.
1. inlet mouths among Fig. 1,2. big trap, 3. pipe connecting, 4. air outlet, 5. little trap, 6. little trap butterfly valve operating stick, 7. little capture discharge port 8. descends pipe connecting, and 9, big trap butterfly valve operating stick, 10. big trap discharge port.
Embodiment
Embodiment:
The present invention is by inlet mouth 1, big trap 2, pipe connecting 3, air outlet 4, little trap 5, little trap butterfly valve operating stick 6, little capture discharge port 7, following pipe connecting 8, big trap butterfly valve operating stick 9, big trap discharge port 10 is formed, it is characterized in that big trap 2 the right connect little trap 5 through pipe connecting 3, little trap 5 warps pipe connecting 8 down are connected three little traps 5 of the same type by row with pipe connecting 3, leave 1 mouthful of air inlet on the big trap 2, big trap butterfly valve operating stick 9, leave little trap butterfly valve operating stick 6 on the little trap 5, during installation inlet mouth 1 is connected with sublimation pipe, packing of product bag is inserted on big trap discharge port 10 and the little trap discharge port 7 and gets final product, after the gaseous state Aluminum chloride anhydrous in the sublimation pipe pours in big trap 2, be subjected to temperature to reduce reason, the crystallization on big trap 2 inwalls of gaseous state Aluminum chloride anhydrous, the gaseous state Aluminum chloride anhydrous that purity is high enters in the little trap 5, in like manner be subjected to temperature to reduce reason, the crystallization on little trap 5 inwalls of gaseous state Aluminum chloride anhydrous, through after a few hours, beat the yellow Aluminum chloride anhydrous xln that can obtain contain iron on the iron wall of the Tie Bi of big trap 2 and little trap 5 at big trap discharge port 10 with iron hammer, little trap discharge port 7 obtains white iron-free Aluminum chloride anhydrous xln.
Claims (4)
1. aluminium trichloride synthesizing catcher group, form by inlet mouth (1), big trap (2), pipe connecting (3), air outlet (4), little trap (5), little trap butterfly valve operating stick (6), little capture discharge port (7), following pipe connecting (8), big trap butterfly valve operating stick (9), big trap discharge port (10), it is characterized in that big trap (2) the right connects little trap (5) through pipe connecting (3).
2. a kind of aluminium trichloride synthesizing catcher group according to claim 1 is characterized in that pipe connecting (8) is connected three little traps (5) of the same type by row with pipe connecting (3) under little trap (5) warp.
3. a kind of aluminium trichloride synthesizing catcher group according to claim 1 is characterized in that leaving on the big trap (2) air inlet (1) mouth, big trap butterfly valve operating stick (9).
4. a kind of aluminium trichloride synthesizing catcher group according to claim 1 is characterized in that leaving on the little trap (5) little trap butterfly valve operating stick (6).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910154986A CN101811719A (en) | 2009-12-04 | 2009-12-04 | Aluminium trichloride synthesizing catcher set |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910154986A CN101811719A (en) | 2009-12-04 | 2009-12-04 | Aluminium trichloride synthesizing catcher set |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN101811719A true CN101811719A (en) | 2010-08-25 |
Family
ID=42619112
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN200910154986A Pending CN101811719A (en) | 2009-12-04 | 2009-12-04 | Aluminium trichloride synthesizing catcher set |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101811719A (en) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4479927A (en) * | 1982-08-09 | 1984-10-30 | The Perkin-Elmer Corporation | Regenerable cold trap for aluminum chloride effluent |
| CN201634452U (en) * | 2009-12-04 | 2010-11-17 | 吴伟明 | Anhydrous aluminum chloride synthesis trap group |
-
2009
- 2009-12-04 CN CN200910154986A patent/CN101811719A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4479927A (en) * | 1982-08-09 | 1984-10-30 | The Perkin-Elmer Corporation | Regenerable cold trap for aluminum chloride effluent |
| CN201634452U (en) * | 2009-12-04 | 2010-11-17 | 吴伟明 | Anhydrous aluminum chloride synthesis trap group |
Non-Patent Citations (1)
| Title |
|---|
| 锦西化工厂: "沸腾法制取无水三氯化铝", 《无机盐工业》 * |
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|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20100825 |