CN101766329B - Pretreatment method of tobacco stalk raw material - Google Patents
Pretreatment method of tobacco stalk raw material Download PDFInfo
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- CN101766329B CN101766329B CN2010100391558A CN201010039155A CN101766329B CN 101766329 B CN101766329 B CN 101766329B CN 2010100391558 A CN2010100391558 A CN 2010100391558A CN 201010039155 A CN201010039155 A CN 201010039155A CN 101766329 B CN101766329 B CN 101766329B
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Abstract
The invention discloses a pretreatment method of tobacco stalk raw material, comprising the following steps: firstly, dissolving 0.1-30 parts of ammonium salt into 10-100 parts of water according to weight parts, mixing and dissolving the ammonium salt to prepare ammonium salt solution for stand-by application; the ammonium salt is one or more than two compound(s) selected from the group of ammonium bicarbonate, ammonium citrate, ammonium tartrate, quadrol, carbamide, diammonium hydrogen phosphate or ammonium dihydrogen phosphate; then, smashing quicklime and screening the smashed quicklime through a 40 mesh screen, and then, preparing the quicklime powder whose diameter is smaller than 40 mesh for stand-by application; spraying the ammonium salt solution to the tobacco stalk of 100-1000 parts and mixing them tolead the tobacco stalk to be fully absorbed; lastly, evenly mixing the 0.1-10 parts of quicklime powder and the tobacco stalk which is processed through ammonium salt solution, and stacking and storing the tobacco stalk for 20-40 days. The invention can complete the pretreatment of the tobacco stalk during the storing course of the tobacco stalk, can not affect the re-using of the production process time for the tobacco stalk; meanwhile, the pretreatment of large quantities of raw materials can be simultaneously conducted, therefore, the invention not only can improve the physical and chemical structure of the tobacco stalk, but also can effectively increase the internal quality of the tobacco stalk.
Description
Technical field
The invention belongs to the tobacco material manufacture field, particularly offal is at the process for chemically pretreating of storage period.
Background technology
Offal belongs to the product of former cigarette in the beating and double roasting process, and the content in former cigarette is about 25-30%, and the formulation cost that the height of its utilization rate in the cigarette industry raw material directly has influence on cigarette reduces the amplitude size.In view of offal self characteristics---main chemical compositions has than big difference with tobacco leaf on content, and it is very low mainly to show as total nitrogen and nicotine content, and reduced sugar is lower slightly, thereby candy alkali ratio height; Cellulose, hemicellulose, pectin and content of lignin are apparently higher than tobacco leaf content, and more weak these architectural features that wait of fragrance influence its use value in the cigarette industry raw material.To this situation; The process for chemically pretreating of offal is to manufacture in the production process that satisfies the tobacco industry material condition at offal to accomplish mostly at present; As when the production of papermaking-method reconstituted tobaccos; In the offal leaching process, adopt ammonium salt and alkaline matter to improve offal material quality, but that one of limitation of this method is a treating capacity is limited, treatment temperature is higher, energy consumption is big; Two of limitation is that this processing procedure occurs in the production process, can add the production technology time of long products on the one hand, the responsible influence factor of the big grade of different batches material quality fluctuation range that also can cause different time to handle on the other hand; And be mostly artificial fermentation or enzyme facture at present at the preprocess method of storage period of offal; The limitation of this processing method is: for ensureing the biologically active of enzyme; The humiture that must control environment is in certain scope; Treatment conditions are comparatively harsh, cause negative effect factors such as the higher or difficult control of result of processing cost.
Summary of the invention
The objective of the invention is deficiency to prior art; Providing a kind of can accomplish in the storage of offal; Do not influence offal and utilize the production technology time again; Can make raw material in enormous quantities carry out preliminary treatment simultaneously, can improve offal physics and chemistry structure, can effectively improve the preprocess method of offal interior quality again.
The objective of the invention is to realize through following technical scheme.
A kind of preprocess method of tobacco stalk raw material, method step is following:
parts by weight are dissolved in 0.1~30 part of ammonium salt in 10~100 parts of water, and it is for use that stirring and dissolving is processed ammonium salt solution; Said ammonium salt is that carbonic hydroammonium, ammonium citrate, ammonium tartrate, ethylenediamine, urea are plain, one or more the mixture in diammonium hydrogen phosphate or the ammonium dihydrogen phosphate (ADP);
2. quick lime was pulverized 40 mesh sieves, the cut-off footpath is subsequent use less than 40 purpose quick lime powder;
3. spraying ammonium salt solution in parts by weight is mixing in 100~1000 parts the offal, offal is fully absorbed;
4. after 0.1~10 part of quick lime powder and the offal of handling through ammonium salt solution being mixed, pile was preserved 20~40 days at normal temperatures.
The present invention introduces ammonium salt and quick lime as inorganic agent in the storage of offal, in the processing procedure, after quick lime ran into the offal that has a little moisture, reacting with part moisture in the offal generated alkaline matter Ca (OH)
2And emit the part thermal discharge; This reaction can increase the alkaline environment in the stockpile and improve environment temperature; Ammonium salt in the slightly high alkaline environment of temperature with the cell wall substance effect that constitutes offal; Macromolecular substances such as polymer substances such as lignin in the offal cell membrane, hemicellulose and pectin are effectively transformed, thereby improve the cell wall structure of offal.On the other hand; Ammonium salt and lime can provide nitrogenous source and alkaline environment to the preliminary treatment of offal on certain degree, add the high characteristics of offal self total reducing sugar; Inorganic agent can facilitate the offal material that certain chemical reaction takes place, and increases the aroma component or the latent perfumery matter of tobacco stalk raw material.In addition, in the entire process process, part quick lime has desiccation, to the tobacco stalk raw material in the preprocessing process go mouldy, carbonization has control action.In a word, the inventive method can improve the use value of offal through the physics and chemistry structure of improving the offal material, handles the tobacco stalk raw material that obtains through the inventive method, can be used for producing expanded cut stem or papermaking-method reconstituted tobaccos.
Compared with prior art, the present invention has the following advantages:
A. to compare browning degree less for the inventive method and artificial fermentation's process, can reduce the rotten risk of tobacco stalk raw material in the processing procedure greatly.
B. the inventive method does not need extra increase treatment conditions, and is workable, can make tobacco stalk raw material realize mass disposal, the fluctuation range of result between can reducing batch.
Further set forth content of the present invention below in conjunction with embodiment.But protection scope of the present invention is not limited in embodiment.
The specific embodiment
The accessible tobacco stalk raw material of the present invention do not limit the production ground, source, kind also can be the offal stalk groups of prescription arbitrarily.
Embodiment 1
By following step tobacco stalk raw material is carried out preliminary treatment:
1. by weight 2 parts of diammonium hydrogen phosphates are dissolved in 10 parts of water, it is for use that stirring and dissolving is processed ammonium dibasic phosphate solution;
2. quick lime was pulverized 40 mesh sieves, the cut-off footpath is subsequent use less than 40 purpose quick lime powder;
3. spraying ammonium dibasic phosphate solution in parts by weight is mixing in 100 parts the offal, offal is fully absorbed;
4. after mixing with 0.5 part quick lime powder and through the offal that ammonium dibasic phosphate solution is handled, pile is preserved and was got final product in 30 days at normal temperatures.
The offal that after above-mentioned preliminary treatment, obtains manufactures the reconstituted tobacco finished product by the manufacturing condition of existing papermaking-method reconstituted tobaccos; Through chopping, roll into after cigarette props up, propping up with reconstituted tobacco cigarette that stalk group untreated, identical quality is processed is contrast, the difference between the sense organ suction quality that each cigarette of comparison of smokeing panel test props up; Through smokeing panel test; The sensory evaluation result who handles is: fragrance more enough, bitter taste slightly, residual still have, and stimulates, assorted gas and strength diminishes.
Embodiment 2
By following step tobacco stalk raw material is carried out preliminary treatment:
1. by weight 10 parts of carbonic hydroammonium are dissolved in 100 parts of water, it is for use that stirring and dissolving is processed ammonium bicarbonate soln;
2. quick lime was pulverized 40 mesh sieves, the cut-off footpath is subsequent use less than 40 purpose quick lime powder;
3. spraying in parts by weight with reinforced mode ammonium bicarbonate soln is mixing in 500 parts the offal, offal is fully absorbed;
4. after 5 parts of quick lime powder and the offal of handling through ammonium bicarbonate soln being mixed, pile is preserved and was got final product in 40 days at normal temperatures.
Offal after above-mentioned preliminary treatment finishes directly gets into the production line of expanded cut stem, produces expanded cut stem, carries out sensory evaluation, and smoking result is: handle fragrance concentration and improve, sweet sense is arranged back, and rich enhancing, stimulating, mix, gas diminishes and strength diminishes.
Embodiment 3
By following step tobacco stalk raw material is carried out preliminary treatment:
1. by weight with urea plain 5 parts with 5 parts of ammonium tartrates mixing after, be dissolved in that to be mixed with ammonium salt solution in 100 parts of water for use;
2. quick lime was pulverized 40 mesh sieves, the cut-off footpath is subsequent use less than 40 purpose quick lime powder;
3. spraying ammonium salt solution in parts by weight is mixing in 1000 parts the offal, offal is fully absorbed;
4. after 10 parts of quick lime powder and the offal of handling through ammonium salt solution being mixed, pile is preserved and was got final product in 20 days at normal temperatures.
Offal after processing finishes is used to produce reconstituted tobacco, and reconstituted tobacco is carried out sensory evaluation, and smoking result is: smoke treatment is fine and smooth, stimulates and reduces, slightly assorted gas, and pleasant impression is still clean, and strength is slightly little.
Embodiment 4
By following step tobacco stalk raw material is carried out preliminary treatment:
1. by weight 0.1 part of second two ammonium is dissolved in 15 parts of water, it is for use that stirring and dissolving is processed second two ammonium salt solutions;
2. quick lime was pulverized 40 mesh sieves, the cut-off footpath is subsequent use less than 40 purpose quick lime powder;
3. spraying second two ammonium salt solutions in parts by weight is mixing in 100 parts the offal, offal is fully absorbed;
4. after 0.1 part of quick lime powder and the offal of handling through ammonium salt solution being mixed, pile was preserved 25 days at normal temperatures.
Embodiment 5
By following step tobacco stalk raw material is carried out preliminary treatment:
1. after by weight 10 parts of lemon acid amides and 20 parts of ammonium dihydrogen phosphate (ADP)s being mixed, be dissolved in 100 parts of water, it is for use that stirring and dissolving is processed ammonium salt solution;
2. quick lime was pulverized 40 mesh sieves, the cut-off footpath is subsequent use less than 40 purpose quick lime powder;
3. spraying ammonium salt solution in parts by weight is mixing in 1000 parts the offal, offal is fully absorbed;
4. after 10 parts of quick lime powder and the offal of handling through ammonium salt solution being mixed, pile was preserved 30 days at normal temperatures.
Embodiment 6
By following step tobacco stalk raw material is carried out preliminary treatment:
1. by weight 20 parts of ammonium tartrates are dissolved in 90 parts of water, stirring and dissolving is processed the ammonium tartrate solution for later use;
2. quick lime was pulverized 40 mesh sieves, the cut-off footpath is subsequent use less than 40 purpose quick lime powder;
3. spraying ammonium tartrate solution in parts by weight is mixing in 800 parts the offal, offal is fully absorbed;
4. after 7 parts of quick lime powder and the offal that passes through the ammonium tartrate solution-treated being mixed, pile was preserved 35 days at normal temperatures.
Claims (1)
1. the preprocess method of a tobacco stalk raw material is characterized in that, method step is following:
1. by weight 0.1~30 part of ammonium salt is dissolved in 10~100 parts of water, it is for use that stirring and dissolving is processed ammonium salt solution; Said ammonium salt is that carbonic hydroammonium, ammonium citrate, ammonium tartrate, ethylenediamine, urea are plain, one or more the mixture in diammonium hydrogen phosphate or the ammonium dihydrogen phosphate (ADP);
2. quick lime was pulverized 40 mesh sieves, the cut-off footpath is subsequent use less than 40 purpose quick lime powder;
3. spraying ammonium salt solution in parts by weight is mixing in 100~1000 parts the offal, offal is fully absorbed;
4. after 0.1~10 part of quick lime powder and the offal of handling through ammonium salt solution being mixed, pile was preserved 20~40 days at normal temperatures.
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CN2010100391558A CN101766329B (en) | 2010-01-13 | 2010-01-13 | Pretreatment method of tobacco stalk raw material |
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CN2010100391558A CN101766329B (en) | 2010-01-13 | 2010-01-13 | Pretreatment method of tobacco stalk raw material |
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CN101766329B true CN101766329B (en) | 2012-06-06 |
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Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN102488322A (en) * | 2011-11-18 | 2012-06-13 | 安徽中烟工业有限责任公司 | Method for reducing release of harmful components in papermaking tobacco sheet |
CN102715649B (en) * | 2012-03-06 | 2014-06-18 | 湖北中烟工业有限责任公司 | Tobacco slice additive and preparation method of tobacco slices |
CN103211290A (en) * | 2013-05-13 | 2013-07-24 | 湖北中烟工业有限责任公司 | Method for improving quality of all-stem reconstituted tobaccos |
CN104452437A (en) * | 2014-10-30 | 2015-03-25 | 云南中烟工业有限责任公司 | Cigarette paper capable of improving suction satisfaction |
CN114287658B (en) * | 2021-12-31 | 2023-05-23 | 湖北省烟草科学研究院 | Method for improving carotenoid degradation efficiency in cigar tobacco fermentation process |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB863287A (en) * | 1957-12-13 | 1961-03-22 | Lorillard Co P | Smoking tobacco product |
CN1095248A (en) * | 1992-12-17 | 1994-11-23 | 菲利普莫里斯生产公司 | Dipping of tobacco and expanding method |
CN1246307A (en) * | 1998-08-31 | 2000-03-08 | 朱大恒 | Method for making tobacco sheet |
EP2130444A1 (en) * | 2008-06-06 | 2009-12-09 | Xavier Wertz | Smokable material and smokable articles |
-
2010
- 2010-01-13 CN CN2010100391558A patent/CN101766329B/en active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB863287A (en) * | 1957-12-13 | 1961-03-22 | Lorillard Co P | Smoking tobacco product |
CN1095248A (en) * | 1992-12-17 | 1994-11-23 | 菲利普莫里斯生产公司 | Dipping of tobacco and expanding method |
CN1246307A (en) * | 1998-08-31 | 2000-03-08 | 朱大恒 | Method for making tobacco sheet |
EP2130444A1 (en) * | 2008-06-06 | 2009-12-09 | Xavier Wertz | Smokable material and smokable articles |
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Owner name: YUNNAN ZHONGYAN RECONSTITUTED TOBACCO CO., LTD. Free format text: FORMER NAME: YUNNAN ZHONGYAN KUNCHUAN RUISHENG TECHNOLOGY CO., LTD. |
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Address after: 650106 Kunming science and Technology Industrial Development Zone, Yunnan Province Road No. 41 Patentee after: Yunnan Zhongyan Reconstituted Tobacco Co., Ltd. Address before: 650106 Yunnan province Haiyuan Kunming high tech Industrial Development Zone, Road No. 1699 Patentee before: Yunnan Zhongyan Kunchuan Ruisheng Technology Co., Ltd. |