CN101738459A - Expansion/shrinkage stress testing device for cement-based material - Google Patents

Expansion/shrinkage stress testing device for cement-based material Download PDF

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CN101738459A
CN101738459A CN201010100448A CN201010100448A CN101738459A CN 101738459 A CN101738459 A CN 101738459A CN 201010100448 A CN201010100448 A CN 201010100448A CN 201010100448 A CN201010100448 A CN 201010100448A CN 101738459 A CN101738459 A CN 101738459A
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cement
testing device
based material
expansion
annulus
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CN101738459B (en
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缪昌文
田倩
刘加平
张建业
姚婷
郭飞
王育江
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Sobute New Materials Co Ltd
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NANJING DAOLU CONSTRUCTION MATERIAL FACTORY
Jiangsu Bote New Materials Co Ltd
Jiangsu Research Institute of Building Science Co Ltd
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Abstract

The invention relates to an expansion/shrinkage stress testing device for a cement-based material, which comprises an inner circular ring and an outer circular ring which are coaxial and have the same height, and a stress testing device and a data acquisition device which are electrically interconnected, wherein the inner circular ring and the outer circular ring are made of the same material; and the stress testing device comprises a plurality of test stress plates which are distributed evenly along the circumferential direction on the outer surface of the outer circular ring and the inner surface of the inner circular ring and are electrically connected with the data acquisition device. When the testing device is used, the cement-based material (such as pure slurry, mortar or concrete) is cast between the two rings. The expansion and shrinkage stress can be calculated according to the analysis of material mechanics by measuring the stress. Compared with the prior method, the testing device has the main advantages that: a, the testing device is simple, and simple and convenient to operate; b, the restraint stress is even; and c, the testing of starting self water addition molding can be implemented, the testing process needs no manpower to move the test piece, and continuous and automatic test can be realized.

Description

Expansion/shrinkage stress testing device for cement-based material
Technical field
The present invention relates to a kind of expansion/shrinkage stress testing device for cement-based material, can estimate the swelling agent expansion effect that is used to prepare expansive concrete, belong to the cement-based material technical field of measurement and test.
Background technology
Expansive concrete is meant to be mixed swelling agent or uses expansive cement in concrete, under certain constraint condition, produce the appropriateness expansion and produce certain concrete from stress.Be mainly used in reinforced concrete works and the mass concrete engineering of structure from the continuous placing of waterproof, fillibility expansion the second stage of the project, prolongation buildings expansion joint or post-cast strip spacing.The chemical reaction of expanded constituents dependence itself or with the reaction of other compositions of cement, in course of hardening, produce certain confined expansion compensation or the contraction in the part compensating concrete hardening process.
The gordian technique of expansive concrete preparation is to mix swelling agent, and generation is expanded, and produces turgor pressure stress under certain constraint condition, to compensate under drying condition because the tension that contraction produces improves concrete splitting resistance.Estimating on the effect of swelling agent compensate for shrinkage at present, main still the employing tested cement paste, mortar, the concrete expansion deflection that mixes swelling agent under certain match ratio and curing condition, compare and the effect of passing judgment on different swelling agents, as JC 476 " cement expansive material " standard code mix the restriction glue sand test specimen of a certain amount of swelling agent by test, limited expansion rate by testing maintenance 7d in 20 ℃ of water and relative humidity 65% airborne dry-shrinkage deformed passed judgment on the quality with more different swelling agents; Patent 00261525.8 " sand-cement slurry expansion contraction measuring instrument " and patent 0324493.1 " concrete confined expansion constriction device " has proposed to be specifically designed to the test sand-cement slurry and concrete limits the method for shrinking.These proving installations and evaluation method can reflect the size of different swelling agent expansion performances to a certain extent.But, because a kind of elastic-plastic material of cement concrete with time varying characteristic.Its Young modulus and the parameter of creeping all can develop along with the time, and in length of time morning of hydration and hardening, modulus is less relatively, and the lax feature of creeping is obvious, and expansion performance consumes owing to stress relaxation, and therefore big swell value not necessarily produces big turgor pressure stress; Otherwise after the hydration and hardening of cement reached certain degree, modulus increased significantly, and the lax behavior of creeping weakens, and swell value less under the constraint condition also may produce big turgor pressure stress.Therefore, from the angle of assessment cracking risk, it is not enough testing the expansion performance that the expansion value estimates swelling agent merely, and the evaluation method of science is to test out expansion/contraction stress more, with the expansion performance of correct reflection swelling agent.
As a kind of elastic-plastic material, because the stress itself that distortion produces can not directly be measured, the method that adopts is the restrained deformation of measuring under the constraint condition mostly usually, and further comes calculated stress by mechanical analysis under the constraint condition.The constraint condition difference, the model difference of mechanical analysis all might be brought remarkable influence to precision of calculation results.It is to detect the cracking behavior of test specimen under different condition by the axial deformation of confined concrete bar shaped test specimen and the stress of measurement test specimen that axle retrains test method.As the split test frame of Munich, Germany polytechnical university development and the temperature stress testing machine that developed afterwards, by concrete sample is monitored in real time from the strain that moulding begins, and reset by stepper motor, thereby approximate 100% constraint is provided, and corresponding expansion/contraction stress also can come out by the force transducer synchronism detection that is installed in above the stepper motor.This method can reflect the stress-strain characteristics of concrete material comprehensively, all sidedly, also can be used for the expansion performance of scientific evaluation swelling agent.But this method equipment one-time investment is very big, and complicated operation fails to apply in engineering practice.Patent 200310117098.0 has been announced a kind of easy sand-cement slurry, concrete shrinkage stress method of testing and device, wherein device as shown in Figure 1, wherein 1 for the constraint reinforcing bar, 2 for the slippage sleeve pipe, 3 for constraint end plate, 4 be that anchoring piece, 5 is observation district, crack for confining region, 7 for spheric probe, 6.Concreting is out of shape with framework of steel reinforcement in framework of steel reinforcement, calculates expansion/contraction stress by the distortion of test two ends ailhead, and the computation process of stress σ is as follows:
σ = ϵ × E × πD 2 4 × ( A - πD 2 4 )
Wherein: E limits in " concrete confined expansion constriction device " to make the elastic modulus of reinforcing bar; Springform measures 2.0 * 10 5MPa;
D is the diameter of above-mentioned restriction reinforcing bar;
A is the cross-sectional area of " concrete confined expansion constriction device ";
ε is at the deflection of specifying measurement time test " concrete confined expansion constriction device ".
The deflection ε of above-mentioned concrete confined expansion constriction device is calculated by following formula:
ϵ = L 2 - L 1 L 0 × 100 %
Wherein: L 2The length reading that-test block recorded in experimental period;
L 1The initial reading of-test block length;
L 0-test block datum length is perfused with sand-cement slurry or concrete length partly in " concrete confined expansion constriction device ".
Adopt this method can calculate the pucker ﹠ bloat stress of cement concrete under restrictive condition easily, but because constraint is mainly provided by the reinforcing bar of centre, its degree of restraint is mainly determined by the size of middle part reinforcing bar, degree of restraint is big inadequately, and middle part and two ends all exist stress to concentrate.In addition, this method needs to move test specimen in test process, be difficult to resetting, therefore cause measuring error easily, influence result of calculation, and owing to need move test specimen, can't measure early stage expansion and differential contraction stress, and,, therefore can't accurately judge owing to need artificial observation for the judgement of incipient crack time.
Summary of the invention
The invention provides a kind of expansion/shrinkage stress testing device for cement-based material, simple in structure, can realize that operation is simple and reliable from building the strain measurement that moulding begins, mechanical model is clear.
Described expansion/shrinkage stress testing device for cement-based material, comprise coaxial setting and highly identical inside and outside annulus, strain detection testing device and the data collector that is electrically connected mutually, described inside and outside annulus material is identical, described strain detection testing device comprises a plurality of test foil gauges, described test foil gauge circumferentially evenly distributes at outer toroid outside surface and interior circle ring inner surface upper edge, and each test foil gauge all is electrically connected with data collector.
Use when of the present invention, cement-based material (as clean slurry, mortar or concrete) is cast between two rings.In expansion process, interior ring and outer shroud all provide constraint, and the strain by ring and outer shroud in testing out can accurately calculate differential expansion stress according to mechanical analysis.After the end of expanding, if cement-based material begins to shrink, then early stage differential expansion stress discharges gradually, and in contraction process, interior ring can further provide pinch confinement again, by the strain of ring in measuring, can calculate differential contraction stress according to the analysis meter of the mechanics of materials equally, further combined with subtest means such as tensile strength, elastic modulus, can assess the cracking risk.Make and use the present invention to test specifically and may further comprise the steps:
1. determine the height h of annulus and thickness (thickness of the institute's moulding cement-based material) t between two rings.The xsect of generally building moulding is square, h=t at this moment.For cement paste or mortar, h is 25~40mm, for corresponding with the free shrink test specimen, and the sectional dimension that should get 25 * 25mm or 40 * 40mm, i.e. h=t=25mm or 40mm; For concrete sample, h and t all should get the value more than 3 times of the maximum particle diameter of gathering materials in the concrete.
2. determine the size of inside and outside annulus, definite foundation is followed following principle:
A) the external radius R of annulus in 2Be 50mm-200mm;
B) the inside radius R of outer toroid 3Be R 2+ t, wherein t is the thickness of institute's moulding cement-based material;
C) interior annulus inside radius R 1According to required constraint degree, obtain by the computing formula of constraint degree
ψ = 1 - E C ′ E S · 1 E C ′ E S - 1 - ( R 1 R 2 ) 2 1 - ( R 3 R 2 ) 2 · [ ( 1 + v C ) ( R 3 R 2 ) 2 + ( 1 - v C ) ] [ ( 1 + v S ) ( R 1 R 2 ) 2 + ( 1 - v S ) ] - - - ( I )
E wherein SThe elastic modulus of annulus;
E C' elastic modulus of tested cement-based material, calculate for simplifying, get empirical value and get final product;
v SThe Poisson ratio of annulus;
v CThe Poisson ratio of tested cement-based material;
To determine that parameter brings formula I into and can obtain R 1,
D) outer toroid wall thickness (R 4-R 3) equal (R 2-R 1)~1.2 * (R 2-R 1).
3. make annulus with the line cutting mode, also can buy the steel pipe processing of commercially available suitable dimension.As preferred version of the present invention, the material of described inside and outside annulus is a steel, more preferably mild carbon steel or Invar steel.Because the linear expansion coefficient of Invar steel only is about 1/10 of a common iron, adopt the Invar steel can avoid Temperature Influence more effectively.
4. install dog screw on the flat board that does not absorb water, planar surface is put the PVC plastic sheeting of one deck flexibility, and interior annulus and outer toroid are placed on the flat board, and the center of circle of annulus and outer toroid overlapped in dog screw can be guaranteed.
5. the inside surface of ring outer surface and interior ring is along circumferentially evenly sticking a plurality of test foil gauges outside, and described test foil gauge can be by having bought on the market, and common have a resistance strain gage.As preferred version, outer toroid outside surface and interior circle ring inner surface are along upwards respectively pasting 3-4 test foil gauge the week of centre-height.As improvement, described strain detection testing device also comprises temperature compensation foil gauge and reference member, and described temperature compensation foil gauge is attached to the reference member surface, and described reference member is identical with the outer toroid material with interior annulus.To test foil gauge and the temperature compensation foil gauge all is electrically connected with data collector.
6. testing starting material and test unit should deposit 1 day in that the test temperature condition is following at least.
Clean slurry, mortar or the concrete mix that 7. will stir divides two-layer pouring between two steel loops, inserts puddling in fact.According to the test needs, determine that needed curing condition carries out maintenance, every composing type test specimen is no less than 3.
8. build moulding intact after, can adopt data collector to test immediately, described data collector can be by having bought on the market, as strainometer.Data collecting instrument should have 0.000001m/m resolution at least, and data acquisition should be set within 30 minutes at interval.By the strain that strainometer is measured inside and outside steel loop, can calculate differential expansion stress or differential contraction stress in cement paste, mortar or the concrete, concrete grammar is as follows:
Cement paste, mortar or concrete inside radius are the differential expansion stress or the differential contraction stress σ at r place CCalculate by following formula,
σ C = R 3 2 r 2 + 1 R 2 2 R 3 2 - 1 P 1 - R 2 2 r 2 + 1 1 - R 2 2 R 3 2 P 2 - - - ( II )
P in the formula (II) 1And P 2Be respectively the stress that acts on outer shroud and the interior ring,
P 1 = - ϵI * Es R 2 2 - R 1 2 2 R 2 2
P 2 = - ϵo * Es R 4 2 - R 3 2 2 R 3 2
ε IBe annulus strain in surveying;
ε OBe the strain of actual measurement outer toroid;
The implication of other symbols of formula (II) is the same, works as r=R 2Shi Yingli is σ to the maximum MAX
9. the synchronous forming test specimen carries out the split tensile strength measurement, and evaluation or prediction cracking risk, specifically comprises following content:
A) incipient crack time T CDetermine: by the incipient crack time of definite each test specimen of interior ring strain sudden change, precision is not less than 0.25 day.If cracking not in the test duration then is recorded as ' not cracking ', and test length of time when writing down off-test simultaneously.
B) stress development speed: when when cracking or off-test (test specimen that not have cracking), the speed that stress develops average every day.
C) stress coefficient: the maximal value σ of test specimen differential contraction stress when test specimen shrinks MAXRatio with split tensile strength.
D) prediction of cracking risk can be carried out according to following table, and the cracking risk reaches specialized range according to any one index in the table 1 and judges.
Table 1 cracking risk profile
Adopt the present invention not only can retrain the strain on the inside and outside surface of steel loop by test, quantitative Analysis is mixed the differential expansion stress and the differential contraction stress of different swelling agent concrete/mortars, clean slurry, and by judging that incipient crack time, stress development speed and safety coefficient come cement paste, mortar or crack on concrete risk under synthetic determination, the prediction-constraint condition, compare with existent method, major advantage of the present invention is as follows:
A. test unit is simple, has multifunctionality, and is easy and simple to handle, and within the specific limits, sample dimensions, border condition to the experimental result influence not quite are easy to promote and standardization, are convenient to analysis and comparison to test findings;
B. because the axial symmetry of annulus, test specimen is in the even drawing stress state of hoop, and can not produce stress and concentrate, how much and clear boundary condition, restraint stress is even, can overcome axial test specimen effectively and apply the difficulty of end restraint and easily produce shortcoming such as off-centre;
C. retrain steel loop and can provide enough constrained to concrete shrinkage, constraint degree can be greater than 90%;
D. calculate the actual unrelieved stress (being contraction or expansion stress) of concrete ring with the steel loop strain that records, with free shrink, annulus distortion and concrete bullet mould theory of computation elastic stress, compare unrelieved stress and theoretical elastic stress, the information of stress relaxation in the material is provided, can reflect material expansion, drying shrinkage, self-constriction, creep, the combined action aspect splitting resistance such as ultimate elongation and elastic property, fully characterized the expansion and the contraction behavior of this elastic-plastic material of cement paste/mortar/concrete;
E. can realize the test that the self-watering moulding begins, test process need not the people for moving test specimen, can realize testing continuously, robotization, both can Validity Test early the length of time effectively avoided the personal error in the test process, can accurately judge the incipient crack time again.
Description of drawings
Fig. 1 is the stress test device of patent 200310117098.0;
Fig. 2 is a structural representation of the present invention;
Fig. 3 be among Fig. 2 in the vertical view cutaway drawing of inside and outside annulus;
Fig. 4 is the annulus strain of benchmark test specimen test among the embodiment 1;
Fig. 5 is the annulus strain of mixing the test of swelling agent test specimen among the embodiment 1;
Fig. 6 is a benchmark test specimen and the stress development curve of mixing the swelling agent test specimen among the embodiment 1;
Fig. 7 is the annulus strain of benchmark test specimen test among the embodiment 2;
Fig. 8 is the annulus strain of mixing the test of swelling agent test specimen among the embodiment 2;
Fig. 9 is a benchmark test specimen and the stress development curve of mixing the swelling agent test specimen among the embodiment 2.
Embodiment
Shown in Fig. 2,3, expansion/shrinkage stress testing device for cement-based material comprises coaxial setting and highly identical inside and outside annulus 1,2, the strain detection testing device and the data collector 4 that are electrically connected mutually, described strain detection testing device comprises a plurality of test foil gauges 3, temperature compensation foil gauge 5 and reference member 6, each is along circumferentially even 4 the described test foil gauges 3 that distribute of centre-height on outer toroid 2 outside surfaces and interior annulus 1 inside surface, described temperature compensation foil gauge 5 is attached to reference member 6 surfaces, and described reference member 6 is identical with outer toroid 2 materials with interior annulus 1.Each test foil gauge 3 and temperature compensation foil gauge 5 all are electrically connected with data collector 4.Described test foil gauge 3 is a resistance strain gage, and described data collector 4 is a strainmeter.Test foil gauge 3 and temperature compensation foil gauge 5, data collector 4 all are purchased.During test, earlier the cement-based material 7 that mixes is cast between the inside and outside annulus 1,2, tests then.
Embodiment 1
1: the test basic parameter
Annulus material selection mild carbon steel, elastic modulus are 206GPa, Poisson ratio 0.3.
Annulus is of a size of R 1=52mm, R 2=60mm, R 3=85mm, R 4=95mm, b=t=25mm.
Test proportioning (clean slurry) is as following table:
Table 2 test match ratio (kg/m 3)
KB is benchmark test specimen (elastic modulus 20GPa, a Poisson ratio 0.2) in the table 2, and PZJ is a test specimen (elastic modulus 18GPa, Poisson ratio 0.2) of mixing swelling agent, and the experimental enviroment condition is 20 ℃, 60% relative humidity.
2: test findings and analysis
Fig. 4 is the strain of C50-KB group steel loop.Not being subjected to external force for clean slurry KB outer shroud, is 0 substantially, and therefore interior ring pressurized is negative strain.The ring strain suddenlys change in the time of 4.2 days, has characterized the incipient crack time of test specimen.
Fig. 5 was the steel loop strain of mixing the test specimen of swelling agent, and test specimen was in swelling state at preceding 1.5 days, and outer shroud outwards expands and presents normal strain, and interior ring pressurized inwardly contracts and presents negative strain.Begin afterwards to shrink, returned to just longly up to 5.5 days, the strain of interior ring outer shroud becomes 0, and test specimen begins clean contraction afterwards, the outer shroud no strain that do not stress substantially, and interior ring pressurized is a negative strain.
Fig. 6 adopts formula (II) to calculate the maximal value σ of back test specimen stress according to test result MAXDevelopment figure.Normal stress is tension, and negative stress is a compressive stress.The test specimen contraction tension of not mixing swelling agent is linear growth substantially, develops into about 4MPa at 4.6 days and ftractures, and possess certain unrelieved stress, and this does not cause owing to cracking discharges internal contraction stress fully.Mix the swelling agent PZJ compressive pre-stress that expands at the beginning and increase fast, promptly rise to 3MPa in less than the time, differential expansion stress slowly discharges afterwards, in the time of about 5.5 days, become 0. after since contraction slowly produce and shrink tension.When end of test (EOT), be about 1.2MPa, not cracking.
Table 3 cracking risk assessment
Figure GSA00000005782700072
According to above-mentioned test results and analysis as can be seen mixing of swelling agent produced differential expansion stress, compensated contraction, postponed the incipient crack time, greatly reduce the cracking risk of cement paste, improved the splitting resistance of cement paste.
Embodiment 2
1: the test basic parameter
Annulus material selection Invar steel, elastic modulus is 160GPa, Poisson ratio 0.3.
Annulus is of a size of R 1=100mm, R 2=115mm, R 3=145mm, R 4=160mm, h=t=75mm.
Concrete test proportioning such as following table (aggregate size 5mm-10mm):
Table 4 embodiment 2 concrete mix (kg/m 3)
KB is normal concrete test specimen (elastic modulus 30GPa, a Poisson ratio 0.2) in the table 4, PZJ is a concrete sample (elastic modulus 28GPa, Poisson ratio 0.2) of mixing swelling agent, the experimental enviroment condition is 20 ℃, 35% relative humidity, the maintenance of surface coverage vinyl plastics film waterproof are placed under 35% relative humidity dry after 2.5 days.
Fig. 7 is the strain of concrete KB group steel loop.The strain of ring outer shroud is 0 substantially in 2.5 days, i.e. concrete not obviously distortion under the waterproof curing condition.2.5 begin drying after it, interior ring pressurized does not ftracture during to end of test (EOT).
Fig. 8 is for mixing the concrete steel loop strain of swelling agent.Be in swelling state at preceding 2.5 days under the waterproof condition for concrete PZJ.Drying began to shrink afterwards, returned to just longly up to 7.5 days, and test specimen began clean contraction after the strain of interior ring outer shroud became 0. substantially, the outer shroud no strain that do not stress substantially, and interior ring pressurized is a negative strain.
Fig. 9 adopts formula (II) to calculate the maximal value σ of back test specimen stress according to test result MAXDevelopment figure.The KB group is unstressed substantially before 2.5 days, begins the near linear development at the dry post shrinkage stress of beginning.Develop into about 2MPa the 14 days length of time in off-test, but do not ftracture.Concrete PZJ differential expansion stress period of expansion not in 2.5 days.Began dry after expansion stress at 2.5 days and begin to reduce, swollen differential expansion stress is reduced to 0 during by about 7.5 days, begins to transfer to differential contraction stress afterwards.Last 14 days development of age to about the 1MPa, cracking, although all not have to ftracture, test findings proves that equally the part of mixing of swelling agent has compensated concrete contraction, has reduced the speed of development of differential contraction stress, has improved concrete anti-crack ability.

Claims (9)

1. expansion/shrinkage stress testing device for cement-based material, it is characterized in that, comprise coaxial setting and highly identical inside and outside annulus, strain detection testing device and the data collector that is electrically connected mutually, described inside and outside annulus material is identical, described strain detection testing device comprises a plurality of test foil gauges, described test foil gauge circumferentially evenly distributes at outer toroid outside surface and interior circle ring inner surface upper edge, and each test foil gauge all is electrically connected with data collector.
2. expansion/shrinkage stress testing device for cement-based material as claimed in claim 1 is characterized in that, the method for determining size of inside and outside annulus is as follows:
A) the external radius R of annulus in 2Be 50mm-200mm;
B) the inside radius R of outer toroid 3Be R 2+ t, wherein t is the thickness of institute's moulding cement-based material;
C) interior annulus inside radius R 1According to required constraint degree, obtain by the computing formula of constraint degree
ψ = 1 - E C , E S · 1 E C , E S - 1 - ( R 1 R 2 ) 2 1 - ( R 3 R 2 ) 2 · [ ( 1 + v C ) ( R 3 R 2 ) 2 + ( 1 - v C ) ] [ ( 1 + v S ) ( R 1 R 2 ) 2 + ( 1 - v S ) ] - - - ( I )
E wherein SThe elastic modulus of annulus;
E C' elastic modulus of tested cement-based material;
v SThe Poisson ratio of annulus;
v CThe Poisson ratio of tested cement-based material;
To determine that parameter brings formula I into and can obtain R 1,
D) outer toroid wall thickness (R 4-R 3) equal (R 2-R 1)~1.2 * (R 2-R 1).
3. expansion/shrinkage stress testing device for cement-based material as claimed in claim 1, it is characterized in that, when described cement-based material is cement paste or mortar, the height h of annulus is 25~40mm in described, when described cement-based material was concrete, the height h of described interior annulus was more than 3 times of maximum particle diameter that gather materials in the concrete.
4. as claim 2 or 3 described expansion/shrinkage stress testing device for cement-based material, it is characterized in that h=t.
5. as each described expansion/shrinkage stress testing device for cement-based material among the claim 1-3, it is characterized in that, described strain detection testing device also comprises temperature compensation foil gauge and reference member, described temperature compensation foil gauge is attached to the reference member surface, and be electrically connected with data collector, described reference member is identical with the outer toroid material with interior annulus.
6. as each described expansion/shrinkage stress testing device for cement-based material among the claim 1-3, it is characterized in that the material of described inside and outside annulus is a steel.
7. expansion/shrinkage stress testing device for cement-based material as claimed in claim 6 is characterized in that, the material of described inside and outside annulus is mild carbon steel or Invar steel.
8. as each described expansion/shrinkage stress testing device for cement-based material among the claim 1-3, it is characterized in that outer toroid outside surface and interior circle ring inner surface are along upwards respectively pasting 3-4 test foil gauge the week of centre-height.
9. as each described expansion/shrinkage stress testing device for cement-based material among the claim 1-3, it is characterized in that described data collector has 0.000001m/m resolution at least, data acquisition is not more than 30min at interval.
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