CN101712485A - Preparation method of basic zinc chloride - Google Patents
Preparation method of basic zinc chloride Download PDFInfo
- Publication number
- CN101712485A CN101712485A CN200910310420A CN200910310420A CN101712485A CN 101712485 A CN101712485 A CN 101712485A CN 200910310420 A CN200910310420 A CN 200910310420A CN 200910310420 A CN200910310420 A CN 200910310420A CN 101712485 A CN101712485 A CN 101712485A
- Authority
- CN
- China
- Prior art keywords
- zinc chloride
- basic zinc
- preparation
- reaction
- basic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 title claims abstract description 77
- 235000005074 zinc chloride Nutrition 0.000 title claims abstract description 39
- 239000011592 zinc chloride Substances 0.000 title claims abstract description 38
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 30
- 238000006243 chemical reaction Methods 0.000 claims abstract description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- 235000011114 ammonium hydroxide Nutrition 0.000 claims abstract description 12
- 239000007795 chemical reaction product Substances 0.000 claims abstract description 8
- 238000001035 drying Methods 0.000 claims abstract description 7
- 238000005406 washing Methods 0.000 claims abstract description 3
- 238000000034 method Methods 0.000 claims description 10
- 230000035484 reaction time Effects 0.000 claims description 3
- 235000011121 sodium hydroxide Nutrition 0.000 claims description 3
- 239000000047 product Substances 0.000 abstract description 21
- 238000004519 manufacturing process Methods 0.000 abstract description 7
- 239000002699 waste material Substances 0.000 abstract description 2
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 abstract 2
- 239000011701 zinc Substances 0.000 description 16
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 14
- 229910052725 zinc Inorganic materials 0.000 description 14
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 10
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 6
- 238000001816 cooling Methods 0.000 description 6
- 239000002994 raw material Substances 0.000 description 6
- 239000000654 additive Substances 0.000 description 5
- 229910052785 arsenic Inorganic materials 0.000 description 5
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 5
- 229910052793 cadmium Inorganic materials 0.000 description 5
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium atom Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 description 5
- 239000011787 zinc oxide Substances 0.000 description 5
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 4
- 241001465754 Metazoa Species 0.000 description 3
- 239000002826 coolant Substances 0.000 description 3
- 238000001514 detection method Methods 0.000 description 3
- 238000010792 warming Methods 0.000 description 3
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 2
- XTEGARKTQYYJKE-UHFFFAOYSA-M Chlorate Chemical compound [O-]Cl(=O)=O XTEGARKTQYYJKE-UHFFFAOYSA-M 0.000 description 2
- 229910021529 ammonia Inorganic materials 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 201000010099 disease Diseases 0.000 description 2
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000003053 immunization Effects 0.000 description 2
- UOURRHZRLGCVDA-UHFFFAOYSA-D pentazinc;dicarbonate;hexahydroxide Chemical compound [OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[Zn+2].[Zn+2].[Zn+2].[Zn+2].[Zn+2].[O-]C([O-])=O.[O-]C([O-])=O UOURRHZRLGCVDA-UHFFFAOYSA-D 0.000 description 2
- 238000001228 spectrum Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 description 2
- 229960001763 zinc sulfate Drugs 0.000 description 2
- 229910000368 zinc sulfate Inorganic materials 0.000 description 2
- 206010012735 Diarrhoea Diseases 0.000 description 1
- 241000282887 Suidae Species 0.000 description 1
- FMRLDPWIRHBCCC-UHFFFAOYSA-L Zinc carbonate Chemical compound [Zn+2].[O-]C([O-])=O FMRLDPWIRHBCCC-UHFFFAOYSA-L 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 235000019270 ammonium chloride Nutrition 0.000 description 1
- 239000003674 animal food additive Substances 0.000 description 1
- 230000002180 anti-stress Effects 0.000 description 1
- 238000003556 assay Methods 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 238000009395 breeding Methods 0.000 description 1
- 230000001488 breeding effect Effects 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000005660 chlorination reaction Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 210000003746 feather Anatomy 0.000 description 1
- 230000003031 feeding effect Effects 0.000 description 1
- 230000004720 fertilization Effects 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 230000037308 hair color Effects 0.000 description 1
- 125000005843 halogen group Chemical group 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000012452 mother liquor Substances 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 235000019629 palatability Nutrition 0.000 description 1
- 244000144977 poultry Species 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 230000003245 working effect Effects 0.000 description 1
- 239000011667 zinc carbonate Substances 0.000 description 1
- 235000004416 zinc carbonate Nutrition 0.000 description 1
- 229910000010 zinc carbonate Inorganic materials 0.000 description 1
- -1 zinc oxide Chemical class 0.000 description 1
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- Fodder In General (AREA)
Abstract
Description
Claims (4)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2009103104209A CN101712485B (en) | 2009-11-25 | 2009-11-25 | Preparation method of basic zinc chloride |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2009103104209A CN101712485B (en) | 2009-11-25 | 2009-11-25 | Preparation method of basic zinc chloride |
Publications (2)
Publication Number | Publication Date |
---|---|
CN101712485A true CN101712485A (en) | 2010-05-26 |
CN101712485B CN101712485B (en) | 2012-06-27 |
Family
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN2009103104209A Active CN101712485B (en) | 2009-11-25 | 2009-11-25 | Preparation method of basic zinc chloride |
Country Status (1)
Country | Link |
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CN (1) | CN101712485B (en) |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102502783A (en) * | 2011-10-14 | 2012-06-20 | 中国科学院上海硅酸盐研究所 | Method for preparing alkali zinc chloride nano-powder in hexagonal flake structures |
CN102745737A (en) * | 2012-07-27 | 2012-10-24 | 大连交通大学 | Synthesis method of basic zinc chloride monocrystal nanorods |
CN102976390A (en) * | 2012-12-10 | 2013-03-20 | 常州大学 | Blue-violet fluorescent nano-material and preparation method thereof |
WO2014139193A1 (en) * | 2013-03-11 | 2014-09-18 | 深圳市危险废物处理站有限公司 | Method for preparing basic zinc chloride |
CN104276595A (en) * | 2014-10-28 | 2015-01-14 | 东江环保股份有限公司 | Preparation method of basic zinc chloride |
CN107324375A (en) * | 2017-06-16 | 2017-11-07 | 河北奥新金属材料科技有限公司 | A kind of preparation method of basic zinc chloride |
CN110484730A (en) * | 2019-08-14 | 2019-11-22 | 广州科城环保科技有限公司 | A method of recycling feed grade basic zinc chloride from zinc-containing sludge |
CN110980799A (en) * | 2019-12-26 | 2020-04-10 | 江西省愚人纳米科技有限公司 | Preparation method of basic zinc chloride for feed |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104108741B (en) * | 2014-07-14 | 2016-02-03 | 上海理工大学 | A kind of preparation method of basic zinc chloride particle |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ES2072191B1 (en) * | 1993-04-05 | 1996-02-01 | Univ Madrid Complutense | PROCEDURE FOR OBTAINING ZINC HYDROXYCHLORIDE, ZN5 (OH) 8 CL2.H20 AND ITS USE AS A ZINC CORRECTOR. |
-
2009
- 2009-11-25 CN CN2009103104209A patent/CN101712485B/en active Active
Cited By (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102502783A (en) * | 2011-10-14 | 2012-06-20 | 中国科学院上海硅酸盐研究所 | Method for preparing alkali zinc chloride nano-powder in hexagonal flake structures |
CN102745737A (en) * | 2012-07-27 | 2012-10-24 | 大连交通大学 | Synthesis method of basic zinc chloride monocrystal nanorods |
CN102745737B (en) * | 2012-07-27 | 2014-04-09 | 大连交通大学 | Synthesis method of basic zinc chloride monocrystal nanorods |
CN102976390A (en) * | 2012-12-10 | 2013-03-20 | 常州大学 | Blue-violet fluorescent nano-material and preparation method thereof |
WO2014139193A1 (en) * | 2013-03-11 | 2014-09-18 | 深圳市危险废物处理站有限公司 | Method for preparing basic zinc chloride |
CN104276595A (en) * | 2014-10-28 | 2015-01-14 | 东江环保股份有限公司 | Preparation method of basic zinc chloride |
WO2016065950A1 (en) * | 2014-10-28 | 2016-05-06 | 东江环保股份有限公司 | Method for preparing basic zinc chloride |
CN104276595B (en) * | 2014-10-28 | 2016-08-17 | 东江环保股份有限公司 | A kind of preparation method of basic zinc chloride |
CN107324375A (en) * | 2017-06-16 | 2017-11-07 | 河北奥新金属材料科技有限公司 | A kind of preparation method of basic zinc chloride |
CN110484730A (en) * | 2019-08-14 | 2019-11-22 | 广州科城环保科技有限公司 | A method of recycling feed grade basic zinc chloride from zinc-containing sludge |
CN110980799A (en) * | 2019-12-26 | 2020-04-10 | 江西省愚人纳米科技有限公司 | Preparation method of basic zinc chloride for feed |
CN110980799B (en) * | 2019-12-26 | 2022-05-31 | 江西省愚人纳米科技有限公司 | Preparation method of basic zinc chloride for feed |
Also Published As
Publication number | Publication date |
---|---|
CN101712485B (en) | 2012-06-27 |
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Owner name: CHANGSHA XINGJIA BIO-ENGINEERING CO., LTD. Free format text: FORMER OWNER: CHANGSHA XINGJIATIANHUA AGRICULTURAL DEVELOPMENT CO., LTD. Effective date: 20120817 |
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Effective date of registration: 20120817 Address after: 1017-1025, room 1, building 410011, Xiang Zhong central 235, Wuyi Road, Hunan, Changsha Patentee after: Changsha Xingjia Bio-engineering Co., Ltd. Address before: 410147 Hunan Province, Changsha County Qingshan Pu Zhen Tian Hua Cun Patentee before: Changsha Xingjia Tianhua Agricultural Development Co., Ltd. |
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Denomination of invention: Preparation method of basic zinc chloride Effective date of registration: 20170505 Granted publication date: 20120627 Pledgee: Hunan Jinxin Company Limited by Guarantee Pledgor: Changsha Xingjia Bio-engineering Co., Ltd. Registration number: 2017430000025 |
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Date of cancellation: 20170713 Granted publication date: 20120627 Pledgee: Hunan Jinxin Company Limited by Guarantee Pledgor: Changsha Xingjia Bio-engineering Co., Ltd. Registration number: 2017430000025 |
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PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
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Denomination of invention: Preparation method of basic zinc chloride Effective date of registration: 20170915 Granted publication date: 20120627 Pledgee: Hunan Jinxin Company Limited by Guarantee Pledgor: Changsha Xingjia Bio-engineering Co., Ltd. Registration number: 2017430000064 |
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Date of cancellation: 20171222 Granted publication date: 20120627 Pledgee: Hunan Jinxin Company Limited by Guarantee Pledgor: Changsha Xingjia Bio-engineering Co., Ltd. Registration number: 2017430000064 |
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Address after: Kang Ning Lu Hunan province 410300 Changsha Changsha Liuyang national biological industry base No. 370 Patentee after: CHANGSHA XINGJIA BIO-ENGINEERING Co.,Ltd. Address before: 1017-1025, room 1, building 410011, Xiang Zhong central 235, Wuyi Road, Hunan, Changsha Patentee before: CHANGSHA XINGJIA BIO-ENGINEERING Co.,Ltd. |
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