CN101659755A - Purification treatment technology and equipment of exhaust gas of devulcanizer used in rubber regeneration by washing separation method - Google Patents
Purification treatment technology and equipment of exhaust gas of devulcanizer used in rubber regeneration by washing separation method Download PDFInfo
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- CN101659755A CN101659755A CN200910064185A CN200910064185A CN101659755A CN 101659755 A CN101659755 A CN 101659755A CN 200910064185 A CN200910064185 A CN 200910064185A CN 200910064185 A CN200910064185 A CN 200910064185A CN 101659755 A CN101659755 A CN 101659755A
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- Prior art keywords
- condensation
- purification treatment
- treatment technology
- devulcanizer
- recovery
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- 238000005406 washing Methods 0.000 title claims abstract description 20
- 238000005516 engineering processes Methods 0.000 title claims abstract description 10
- 238000000926 separation method Methods 0.000 title claims abstract description 6
- 238000000746 purification Methods 0.000 title claims description 7
- 230000008929 regeneration Effects 0.000 title abstract description 5
- 239000007789 gases Substances 0.000 claims abstract description 18
- 238000000034 methods Methods 0.000 claims abstract description 15
- 239000007788 liquids Substances 0.000 claims abstract description 7
- 238000009833 condensation Methods 0.000 claims description 28
- 230000005494 condensation Effects 0.000 claims description 28
- 239000011901 water Substances 0.000 claims description 18
- 239000000843 powders Substances 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound data:image/svg+xml;base64,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 data:image/svg+xml;base64,PD94bWwgdmVyc2lvbj0nMS4wJyBlbmNvZGluZz0naXNvLTg4NTktMSc/Pgo8c3ZnIHZlcnNpb249JzEuMScgYmFzZVByb2ZpbGU9J2Z1bGwnCiAgICAgICAgICAgICAgeG1sbnM9J2h0dHA6Ly93d3cudzMub3JnLzIwMDAvc3ZnJwogICAgICAgICAgICAgICAgICAgICAgeG1sbnM6cmRraXQ9J2h0dHA6Ly93d3cucmRraXQub3JnL3htbCcKICAgICAgICAgICAgICAgICAgICAgIHhtbG5zOnhsaW5rPSdodHRwOi8vd3d3LnczLm9yZy8xOTk5L3hsaW5rJwogICAgICAgICAgICAgICAgICB4bWw6c3BhY2U9J3ByZXNlcnZlJwp3aWR0aD0nODVweCcgaGVpZ2h0PSc4NXB4JyB2aWV3Qm94PScwIDAgODUgODUnPgo8IS0tIEVORCBPRiBIRUFERVIgLS0+CjxyZWN0IHN0eWxlPSdvcGFjaXR5OjEuMDtmaWxsOiNGRkZGRkY7c3Ryb2tlOm5vbmUnIHdpZHRoPSc4NScgaGVpZ2h0PSc4NScgeD0nMCcgeT0nMCc+IDwvcmVjdD4KPHRleHQgZG9taW5hbnQtYmFzZWxpbmU9ImNlbnRyYWwiIHRleHQtYW5jaG9yPSJlbmQiIHg9JzYxLjAyOTcnIHk9JzQ3LjAzMTEnIHN0eWxlPSdmb250LXNpemU6MzBweDtmb250LXN0eWxlOm5vcm1hbDtmb250LXdlaWdodDpub3JtYWw7ZmlsbC1vcGFjaXR5OjE7c3Ryb2tlOm5vbmU7Zm9udC1mYW1pbHk6c2Fucy1zZXJpZjtmaWxsOiNFODQyMzUnID48dHNwYW4+SDwvdHNwYW4+PHRzcGFuIHN0eWxlPSdiYXNlbGluZS1zaGlmdDpzdWI7Zm9udC1zaXplOjIyLjVweDsnPjI8L3RzcGFuPjx0c3Bhbj5PPC90c3Bhbj48L3RleHQ+Cjwvc3ZnPgo= O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 238000005204 segregation Methods 0.000 claims description 4
- 238000007689 inspection Methods 0.000 claims description 3
- 239000003921 oils Substances 0.000 claims description 3
- 239000007921 sprays Substances 0.000 claims description 3
- 238000010521 absorption reactions Methods 0.000 claims description 2
- 239000003610 charcoal Substances 0.000 claims description 2
- 238000010438 heat treatment Methods 0.000 claims 2
- 230000001172 regenerating Effects 0.000 claims 2
- 238000001816 cooling Methods 0.000 abstract description 5
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 239000002351 wastewater Substances 0.000 abstract description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N carbon Chemical compound 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[C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 1
- 229910052799 carbon Inorganic materials 0.000 abstract 1
- 239000002912 waste gases Substances 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 3
- 229940108066 Coal Tar Drugs 0.000 description 2
- 238000006243 chemical reactions Methods 0.000 description 2
- 239000011280 coal tar Substances 0.000 description 2
- 239000002826 coolants Substances 0.000 description 2
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- 238000007599 discharging Methods 0.000 description 1
- UFWIBTONFRDIAS-UHFFFAOYSA-N naphthalene Chemical compound 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C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 1
- CTQNGGLPUBDAKN-UHFFFAOYSA-N o-xylene Chemical compound 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CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 1
- 125000001997 phenyl group Chemical group 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- YXFVVABEGXRONW-UHFFFAOYSA-N toluene Chemical compound 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CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 1
- 239000002699 waste materials Substances 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/62—Plastics recycling; Rubber recycling
Abstract
The invention discloses a technology and equipment for recovering and purifying gas emitted from a devulcanizer in the production process of rubber regeneration. High-temperature gases emitted from the devulcanizer is treated by heat recovery, circulated cooling and washing with condensing liquid, terminal treatment (active carbon adsorption or combustion-supporting incineration) and condensationrecycling, thereby realizing standard waste gas emission and zero wastewater discharge. The technology and the equipment have the advantages of environmental protection, energy saving, quick gas emission, no block, low gas emission resistance, thorough gas emission, less atmospheric gas emission of a devulcanizer port, separation-recovery-separation process of rubber power and organic matters, less investment, less occupied area and the like.
Description
One. technical field
The present invention relates in regenerated rubber (reclaimed rubber) production process, recovery, the purifying treatment of digester institute emission gases reach the purpose of energy-conserving and environment-protective.Belong to field of environment protection.
Two. technical background
The rubber regeneration method of desulfurization in the vulcanizer.After reaction finishes, emit a jar interior gas, for containing multiple organic high-temperature water vapor, wherein have on a small quantity with what various auxiliary agents (coal tar, Stockholm tar, activator etc.) entered that jar internal reaction generates and be phenyl ring and heterogeneous ring compounds such as the benzene,toluene,xylene of solid or liquid, naphthalene at normal temperatures, and the hydrogen sulfide of few part, the taste people that chokes, wastes energy at the serious harm environment.
Treatment process amount commonly used at present: with the mode of high-temperature body by direct condensation in shell and tube heat exchanger condensation or the feeding pond.Exist that the steam discharge resistance is big, steam discharge is incomplete; Condensation is not thorough, system is easily stopped up; The indissociable shortcoming of organism.
Task of the present invention is to develop low resistance, does not have the exhaust treatment system one exhaust gas of devulcanizer used in rubber regeneration by washing separation method purification treatment technology and the equipment of pressing full condensation, phlegma to recycle.Realize up to standard, the wastewater zero discharge of exhaust gas emission.
Three. summary of the invention
A. technology contents
Task of the present invention is finished in the following manner:
By accompanying drawing () as can be known, the present invention is separated by rubber powder separation, heat recuperation, condensation washing, and main process such as terminal process is formed.
The high-temperature steam that digester is discharged at first enters rubber powder separator (1), isolates the foreign material such as rubber powder carried secretly in the gas, avoids blocking pipe; Isolate the high temperature gas behind the rubber powder, enter heat recoverer (2) material that domestic water, boiler feed water or coal tar wet goods need heat is heated, reclaim heat; Enter condensation washing knockout tower (5) again, in this tower, contact with end temperature circulating condensing liquid under the spray, heat exchange, washing, high-temperature steam is got off by total condensation, most of organism of discharging with the high temperature gas also is condensed simultaneously, enter in the disengagement chamber of this equipment bottom, isolate greasy dirt impurity such as (organism).High temperature phlegma after temperature raises enters by recycle pump (10) and recycles after primary cooler (6) and time water cooler (7) and water coolant heat-shift reduce temperature.Unnecessary water of condensation enters water of condensation manifold (4) by upflow tube, sends digester back to by condensate pump (9) then and reuses.
The used water coolant of primary cooler (6) recycles after (11) through cooling tower (8), cooling water circulating pump; Inferior water cooler (7) feeds phreatic water or chilled brine when summer high temperature, circulating condensing liquid is carried out further cooling of degree of depth cooling, improves the system handles effect.
A small amount of incondensable gas enters terminal process device (3), the situation different according to the user, take charcoal absorption/combustion-supporting burning mode finally to handle, remove the gas that hydrogen sulfide, organism etc. are poisonous, be harmful to, have the people's taste of choking, discharge after meeting the environment protection emission requirement.
B. major equipment
Condensation washing knockout tower is the key equipment of present technique.By accompanying drawing (two) as can be known: this equipment is two cylindrical section shape tower type containers, and epimere is the condensation washing section, and hypomere is for storing segregation section.There is dividing plate upper and lower section centre, has riser to communicate on the dividing plate, guarantees upper and lower section pressure equilibrium.
Contain organic high-temperature water vapor and enter top condensation washing section from steam inlet (1), contact with the cryogenic condensation liquid of each nozzle of top (6) spray and to carry out heat exchange, water vapor and organism wherein are condensed, and flow into the bottom by downtake (8) and store segregation section.At this, the organism that proportion is lighter floats to top, can discharge from oil discharge outlet (9), and heavy sinking at the bottom of the tower regularly cleared up away from inspection port (10); Unnecessary water of condensation flows out from overflow port (2) to be reused.A small amount of incondensable gas is discharged from steam drain (5).
One section porcelain ring filler (4) is equipped with on condensation washing section top, and during summer high temperature, this packing section upper nozzle ejection is through time water cooler degree of depth refrigerative circulating condensing liquid.Gas is further cooled off washing, improve treatment effect.
Nozzle (6) is spiral spiral case nozzle, is evenly distributed, atomizing effect is good, be difficult for to stop up.
Store segregation section and be provided with safety tube (7), when the equipment internal pressure was too high, water from then on pipe overflowed.
Four. description of drawings
Accompanying drawing (one) is technological process signal of the present invention.
Among the figure:
(1) rubber powder separator
(2) heat recoverer
(3) terminal process device
(4) water of condensation manifold
(5) condensation washing knockout tower
(6) primary cooler
(7) inferior water cooler
(8) cooling tower
(9) condensate pump
(10) recycle pump
(11) cooling water circulating pump
Accompanying drawing (two) is key equipment condensation washing tower signal of the present invention.
Among the figure:
(1) steam inlet
(2) overflow port
(3) dividing plate
(4) porcelain ring filler
(5) steam outlet
(6) nozzle
(7) safety tube
(8) downtake
(9) oil exit pipe
(10) inspection port
(11) condensate outlet
Claims (5)
1. one kind in the vulcanizer internal heating regenerative process, recovery, the purification treatment technology of institute's emission gases.It is characterized in that being separated by rubber powder separation, heat recuperation, condensation washing, processes such as terminal process are formed.
2. by the described recovery of claim 1, purification treatment technology, it is characterized in that vulcanizer internal heating regenerative process institute emission gases enters rubber powder separator (1) successively, heat recoverer (2), condensation washing knockout tower (5), terminal process device (3), according to different situations, take charcoal absorption/combustion-supporting burning mode finally to handle.
3. by the described recovery of claim 1, purification treatment technology, it is characterized in that passing through recycle pump (10), primary cooler (6), inferior water cooler (7) successively by the phlegma of condensation washing knockout tower (5) bottom.
4. by the described recovery of claim 1, purification treatment technology, it is characterized in that entering water of condensation manifold (4), send digester back to by condensate pump (9) and reuse by condensation washing knockout tower (5) overflow water of condensation.
5. by claim 2,3 or 4 described condensation washing knockout towers (5), it is characterized in that containing organic high-temperature water vapor and enter top condensation washing section from steam inlet (1), contact with the cryogenic condensation liquid of each nozzle of top (6) spray and to carry out heat exchange, water vapor and organism wherein are condensed, and flow into the bottom by downtake (8) and store segregation section.At this, the organism that proportion is lighter floats to top, can discharge from oil discharge outlet (9), and heavy sinking at the bottom of the tower regularly cleared up away from inspection port (10); Unnecessary water of condensation flows out from overflow port (2) to be reused.A small amount of incondensable gas is discharged from steam drain (5).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910064185A CN101659755A (en) | 2009-02-06 | 2009-02-06 | Purification treatment technology and equipment of exhaust gas of devulcanizer used in rubber regeneration by washing separation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910064185A CN101659755A (en) | 2009-02-06 | 2009-02-06 | Purification treatment technology and equipment of exhaust gas of devulcanizer used in rubber regeneration by washing separation method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN101659755A true CN101659755A (en) | 2010-03-03 |
Family
ID=41788017
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN200910064185A CN101659755A (en) | 2009-02-06 | 2009-02-06 | Purification treatment technology and equipment of exhaust gas of devulcanizer used in rubber regeneration by washing separation method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101659755A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102462974A (en) * | 2010-11-09 | 2012-05-23 | 萍乡市飞虎炭黑有限公司 | Waste gas treatment facility, device and method |
| CN108127382A (en) * | 2017-12-05 | 2018-06-08 | 北京星航机电装备有限公司 | A kind of assembly method of cover-plate type TPS structures |
-
2009
- 2009-02-06 CN CN200910064185A patent/CN101659755A/en not_active Application Discontinuation
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102462974A (en) * | 2010-11-09 | 2012-05-23 | 萍乡市飞虎炭黑有限公司 | Waste gas treatment facility, device and method |
| CN108127382A (en) * | 2017-12-05 | 2018-06-08 | 北京星航机电装备有限公司 | A kind of assembly method of cover-plate type TPS structures |
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Application publication date: 20100303 |