CN101637201A - Kiwi fruit juice powdered milk and preparation method thereof - Google Patents
Kiwi fruit juice powdered milk and preparation method thereof Download PDFInfo
- Publication number
- CN101637201A CN101637201A CN200910305773A CN200910305773A CN101637201A CN 101637201 A CN101637201 A CN 101637201A CN 200910305773 A CN200910305773 A CN 200910305773A CN 200910305773 A CN200910305773 A CN 200910305773A CN 101637201 A CN101637201 A CN 101637201A
- Authority
- CN
- China
- Prior art keywords
- kiwi
- kiwi berry
- fruit juice
- powder
- juice
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Dairy Products (AREA)
- Non-Alcoholic Beverages (AREA)
Abstract
The invention discloses kiwi fruit juice powdered milk and a preparation method thereof. The preparation method comprises the following steps: adopting a micro embedding technology to micro embed concentrated kiwi fruit juice by edible modified starch which forms external capsules to wrap the concentrated kiwi fruit juice so as to form granules of capsule structures, thereby greatly reducing the loss of nutritive materials in kiwi fruits in the process of processing; then drying mixing the granules with whole milk powder and pure colostrum powder to prepare a finished product. The kiwi fruit juice powdered milk is eaten in the mode of instant drinks, has good taste of fresh fruit, perfectly combines respective unique nutrient characteristics of milk and fruit, has high nutritional value and is easy to digest and absorb.
Description
Technical field
The invention belongs to milk powder processing and manufacturing field, be specifically related to a kind of Kiwi fruit juice powdered milk and preparation method thereof.
Background technology
Kiwi berry is the fruit of Actinidiaceae plant Kiwi berry.Because of its Vit C contents comes out at the top in fruit, a Kiwi berry can provide the twice of people vitamin C demand on the one many, is described as " king of dimension C ", " king of fruit ".Kiwi berry also contains good soluble dietary fiber, and this class material can stimulate intestines peristalsis, but the generation of angiocardiopathies such as the atherosis and coronary heart disease of prevention of arterial; The formation of prevention gall stone.Not only Kiwi berry Vc amount and dietary fibre cellulose content have reached outstanding standard, simultaneously, and Ve in the Kiwi berry and V
kContent is decided to be good, and the Kiwi berry fat content is low and do not have a cholesterol.Different with other fruit is that Kiwi berry contains broad nutritional labeling.Each Kiwi berry can provide folic acid, pantothenic acid, vitamin A and Cobastab
6, copper, calcium, iron, phosphorus and other multivitamin and mineral matter.The prolonged application kiwi-fruit juice also can suppress the generation of melanoma and cutaneum carcinoma; Contain arginine in the kiwifruit fruit, can improve blood flow and stop the formation of thrombus in the arterial blood; Kiwi berry is occupying the 4th aspect the natural inhibitor content; Kiwi berry contains abundant lutein, can prevent multiple canceration; Kiwi berry is rare one of the chlorophyllous fruit that contains when ripe.And milk is a kind of food of high-quality, is called as " white blood ", " near perfect food ", contains multiple vitamin and mineral matter, can satisfy the human body needs, and animal protein content is abundant, easily digests and assimilates comprehensively.How both can be had complementary advantages, two kinds of nutrition that food contained are perfectly combined, be the main direction that we study.
In present existing solid beverage and the fruity milk powder, all be that inspissated juice is prepared burden behind the homogeneous, carry out spray-drying and obtain the fruit powder, last and milk powder mixes.This production technology is comparatively simple, but the nutritional labeling loss is bigger in the fruit juice, and vitamin almost loses over half, and ester class and arene material also volatilize very most of in process, and the original fragrant and sweet smell of fruit juice can not well keep.
Summary of the invention
The purpose of this invention is to provide a kind of nutritional labeling and keep more intact Kiwi fruit juice powdered milk, it can replenish multiple nutrients to human body, has the excellent flavor of fresh fruit and very high nutritive value.
Another object of the present invention provides and a kind ofly can reduce in the Kiwi berry nutriment loss greatly, and can add the preparation method of the Kiwi fruit juice powdered milk of other nutritional labelings.
Contain embedding type Kiwi berry powder in 1 ton of Kiwi berry milk powder of the present invention: 100-180kg, whole milk powder: 750-900kg, bovine colostrum: 10-100kg, citric acid: 5-10g, described embedding type Kiwi berry powder have wrapped up the particle that the Kiwi berry inspissated juice constitutes with converted starch.
The preparation method of described Kiwi fruit juice powdered milk may further comprise the steps:
(1) Kiwi berry pulp squeezes into juice, and vacuum concentrates and obtains the Kiwi berry inspissated juice;
(2) by fluidizer, the Kiwi berry inspissated juice is carried out embedding, obtain embedding type Kiwi berry powder with converted starch;
(3) embedding type Kiwi berry powder and whole milk powder, colostrum dried bean noodles are mixed and get final product.
When the Kiwi berry inspissated juice being carried out the fluidisation spraying embedding of converted starch with converted starch, inlet temperature 60-70 ℃, outlet temperature 53-57 ℃, cold air drying immediately after the spraying embedding.
The part by weight of converted starch and Kiwi berry inspissated juice is 15-25 in the described embedding type Kiwi berry powder particles: 1, and converted starch is a modified food starch.The diameter of embedding type Kiwi berry powder particles is 0.15-0.7mm.
Described concentrated kiwi-fruit juice is that interpolation edible calcium carbonate 5kg, vitamin C 0.5kg, white granulated sugar 15kg final vacuum concentrate and form in the carambola juice that every 500kg squeezes out.
The core technology of project of the present invention is micro-embedded technology, original quality of the new fruit drink of preservation that can be comparatively complete, and make its quality more stable, anti-storage.In existing solid beverage and the fruity milk powder, all be that inspissated juice is prepared burden behind the homogeneous, carry out spray-drying and obtain the fruit powder, last and milk powder mixes, its production technology is comparatively simple, but the nutritional labeling loss is bigger in the fruit juice, and vitamin almost loses over half, ester class and arene material also volatilize very most of in process, and the original fragrant and sweet smell of fruit juice can not well keep.
And the present invention is an adventitia with the modified food starch emulsion, inspissated juice is carried out the technology that microencapsulation is handled, nutritional labeling and original local flavor that can keep fruit juice to greatest extent, reduce vitamin and the loss of trace element in processing and storage, the assurance of very big degree the quality of Kiwi berry inspissated juice.
The present invention finds out the best proportioning of various raw materials through repeatedly test, and the nutritional labeling that can also add other as required simultaneously makes the nutrition of milk powder of the present invention reach balanced, can guarantee the absorption more nutrition.
The nutrient component meter of product of the present invention:
Nutritional labeling | Average content (by every 100g dry powder) |
Protein | ??16.4g |
??IgG | ??160mg |
Fat | ??17.5g |
Carbohydrate | ??55.7g |
Vitamin C | ??≥140mg |
Vitamin D | ??≥8ug |
Calcium | ??≥500mg |
Iron | ??≥5mg |
The nutrient component meter of common whole milk powder
Nutritional labeling | Average content (by every 100g dry powder) |
Protein | ??15g |
Fat | ??18g |
Carbohydrate | ??61.0g |
Vitamin C | ??10mg |
Calcium | ??≥200mg |
The specific embodiment
Following embodiment is intended to further specify the present invention, rather than limitation of the present invention.
1. raw material is selected: select for use fresh pure, the free of contamination Kiwi berry of no scar (wind phoenix Kiwi berry plantation, the western Hunan is preferred), kind is " Mi Liangyi number ".The standard of selecting materials: no insect pest, fruit is big, the shape homogeneous, after in time plucking, classification packing warehouse-in refrigerates 4 ℃ of preservations.
2. raw material handling: remove impurity such as earth, sandstone, and washes clean, get rid of slightly and rot, rotten part (sterilization of 0.1% potassium permanganate, normal temperature clean), the impurity that thorough eccysis Kiwi berry adheres to, the crust of pruning.
3. broken: as to select for use the pulp crushing machine to carry out fragmentation, adopt cold making beating, to keep former fruit local flavor and color and luster, at the citric acid of pulping process adding 0.5%, to adjust the storage rate of its local flavor and its nutriment of raising.
Particle size after cracking is 2-3mm, and it is meticulous that granularity was difficult for slightly also being difficult for, and the meticulous jam that makes forms the paste state, is unfavorable for the outflow of juice, crosses and slightly can cause juice partly to remain in the pulp, loses more.
4. enzyme goes out: make the enzyme deactivation rate in the pulp reach 100%, make pulp softening, dissolving fruit look is heated to 80 ℃ with pulp, boiling 8 minutes in crushing juice rate .2 minute of the raising squeezing.
5. cooling: material by condenser pipe, is cooled to rapidly below 45 ℃, avoids the destruction of long-time high temperature, reduce the loss of nutriment to fruit flesh component.
6. enzyme is handled: contain more pectin in the Kiwi berry, influence crushing juice rate, utilize pectase to handle, (40 ℃ of hydrolysis temperatures, enzyme dosage 5g/L, enzymolysis liquid pH value 4.0-4.5, the processing time is 2h.)
7. press extracting juice (Kiwi berry pulp and pure water were mixed with 1: 2, squeeze).Pomace after squeezing the juice adds 20% clear water, carries out twice pressing.After twice squeezing, crushing juice rate reaches more than 70%.Carambola juice after the squeezing is added batching in proportion.In every 500kg carambola juice, add white granulated sugar 15kg, vitamin C is 0.5kg, and edible calcium carbonate is 5kg.Pump into homogenizer after the batching and carry out homogeneous, homogenization pressure 18mpa, 42 ℃ of homogenizing temperatures.
8. coarse filtration: coarse filtration 2 times, add vibratory sieve with filter cloth and carry out, the filter liquor light transmittance is more than 65%, and filter liquor reduces about 2%.
9. clarification: add gelatin, consumption is 0.01% of a fruit juice weight, carries out light transmittance and reaches more than 80%.
10. ultrafiltration: impurity and granule solid by in the ultrafiltration removal Kiwi berry squeezing juice reach the effect that purifies clear juice.Operating pressure is 3 * 10
5Pa, the aperture of filter membrane is 100 dusts, ultrafiltration 2 to 3 times.
11. vacuum concentrates
Under decompression, lower temperature, concentrate.Vacuum remains on more than the 86kPa. and temperature remains in 58~62 ℃.Concentrate back fruit juice soluble solid content and become 72%, muddy rate>2%.Volume-diminished is original about 1/6.
12. sterilization: 85 ℃ of sterilization temperatures, 5 minutes time.The temperature and time of re-pasteurization is bigger to the kiwi-fruit juice quality influence, and sterilization temperature is high more, and the time is long more, and is big more to the stability and the quality influence of kiwi-fruit juice.Therefore, under the condition of protecting positive bactericidal effect, adopting lower temperature and the certain sterilizing time of control is guarantee product quality important, select this temperature and time to carry out sterilization, by the storage test checking, 25 ℃ of storage temperatures, the good sample of sealing can be deposited more than 2 months, nutriment is preserved better, does not have putrid and deteriorated situation.
13. embedding: the inspissated juice (temperature 80-85 ℃) that sterilization is finished adopts the mode of fluidisation spraying (instrument is the FL Fluidbedgranulatingdrier, and Changzhou sea river drying equipment Co., Ltd makes) modified food starch to carry out embedding.
By the test to multiple embedded material, the embedding external capsule is defined as modified food starch.Modified food starch is a kind of starch through modification.(modified food starch is selected hydroxypropul starch for use, and manufacturer is Divine Land starch Science and Technology Ltd.) this kind starch has some special physicochemical properties, can make after adding in the food formula food have more performance in processing or when edible.Modified food starch has gelatinization point low as the embedding capsule material, good stability, coating rate height, advantages such as capsule Stability Analysis of Structures.
The Kiwi berry inspissated juice is carried out the fluidisation spraying embedding of modified food starch with modified food starch.About 60 to 70 ℃ of inlet temperatures, about 55 ℃ of outlet temperatures.For keeping the stability and the quality of embedding type kiwi-fruit juice, (remove the moisture content about 7% approximately, sample is the dried particles shape, and no thickness does not lump to adopt cold air drying to carry out drying immediately after the spraying embedding.), the particle of formation diameter 0.15~0.7mm, the part by weight of modified food starch and Kiwi berry inspissated juice is 15-25 in the embedding type Kiwi berry powder particles: 1,12 ℃ of temperature are made embedding type Kiwi berry powder finished product, and coating rate is surpassing 98%.
14. dry mixed: embedding type Kiwi berry powder is mixed with whole milk powder and other batching powder, form final products.Whole milk does and mixes that (by producing one ton of embedding type Kiwi berry milk powder, dried to infiltrate the material proportioning be whole milk powder 800kg, embedding type Kiwi berry powder 150kg, bovine colostrum 50kg, citric acid 5g.)
In doing mixed a mixing bowl, fully stir.Compound per ton divides 8 following powder (each 0.125 ton), stirs and is just changeing 2 minutes, reverses 3 minutes, makes the abundant mixing of material, carries out quantitative package by behind vibratory sieve and the filter screen embedding type Kiwi fruit juice powdered milk that mixes being delivered to device of full automatic packaging.
15. vacuum pack with nitrogen: adopt full-automatic nitrogen filling packing machine to pack, be adjusted into every bag of 400g, the holding time can be above 18 months.
Claims (10)
1. Kiwi fruit juice powdered milk, it is characterized in that, contain embedding type Kiwi berry powder in 1 ton of Kiwi berry milk powder: 100-180kg, whole milk powder: 750-900kg, bovine colostrum: 10-100kg, citric acid: 5-10g, described embedding type Kiwi berry powder have wrapped up the particle that the Kiwi berry inspissated juice constitutes with converted starch.
2. Kiwi fruit juice powdered milk according to claim 1 is characterized in that, the part by weight of converted starch and Kiwi berry inspissated juice is 15-25 in the embedding type Kiwi berry powder particles: 1, and the diameter of described embedding type Kiwi berry powder particles is 0.15-0.7mm.
3. Kiwi fruit juice powdered milk according to claim 1 and 2 is characterized in that, described converted starch is a modified food starch.
4. Kiwi fruit juice powdered milk according to claim 1 is characterized in that, described concentrated kiwi-fruit juice is that interpolation edible calcium carbonate 5kg, vitamin C 0.5kg, white granulated sugar 15kg final vacuum concentrate and form in the carambola juice that every 500kg squeezes out.
5. the preparation method of the described Kiwi fruit juice powdered milk of claim 1 is characterized in that, may further comprise the steps:
(1) Kiwi berry pulp squeezes into juice, and vacuum concentrates and obtains the Kiwi berry inspissated juice;
(2) by fluidizer, the Kiwi berry inspissated juice is carried out embedding, obtain embedding type Kiwi berry powder with converted starch;
(3) embedding type Kiwi berry powder and whole milk powder, bovine colostrum, citric acid are done mixed getting final product.
6. the preparation method of Kiwi fruit juice powdered milk according to claim 5 is characterized in that, contains embedding type Kiwi berry powder in 1 ton of Kiwi berry milk powder: 100-180kg, whole milk powder: 750-900kg, bovine colostrum: 10-100kg, citric acid: 5-10g.
7. the preparation method of Kiwi fruit juice powdered milk according to claim 5, it is characterized in that, the part by weight of converted starch and Kiwi berry inspissated juice is 15-25 in the embedding type Kiwi berry powder particles: 1, and the diameter of described embedding type Kiwi berry powder particles is 0.15-0.7mm.
8. the preparation method of Kiwi fruit juice powdered milk according to claim 5, it is characterized in that, the Kiwi berry inspissated juice is carried out the fluidisation spraying embedding of converted starch with converted starch, inlet temperature 60-70 ℃, outlet temperature 53-57 ℃, cold air drying immediately after the spraying embedding, embedding type Kiwi berry powder.
9. according to the preparation method of claim 5 or 7 or 8 described Kiwi fruit juice powdered milks, it is characterized in that described converted starch is a modified food starch.
10. the preparation method of Kiwi fruit juice powdered milk according to claim 5, it is characterized in that described concentrated kiwi-fruit juice is that interpolation edible calcium carbonate 5kg, vitamin C 0.5kg, white granulated sugar 15kg final vacuum concentrate and form in the carambola juice that every 500kg squeezes out.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN200910305773XA CN101637201B (en) | 2009-08-19 | 2009-08-19 | Kiwi fruit juice powdered milk and preparation method thereof |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN200910305773XA CN101637201B (en) | 2009-08-19 | 2009-08-19 | Kiwi fruit juice powdered milk and preparation method thereof |
Publications (2)
Publication Number | Publication Date |
---|---|
CN101637201A true CN101637201A (en) | 2010-02-03 |
CN101637201B CN101637201B (en) | 2011-12-28 |
Family
ID=41612525
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN200910305773XA Expired - Fee Related CN101637201B (en) | 2009-08-19 | 2009-08-19 | Kiwi fruit juice powdered milk and preparation method thereof |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN101637201B (en) |
Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102919370A (en) * | 2012-11-14 | 2013-02-13 | 王梁琴 | Milk powder for strengthening immunity of babies |
CN102972523A (en) * | 2012-11-30 | 2013-03-20 | 内蒙古伊利实业集团股份有限公司 | Yogurt tablet and preparation method thereof |
CN103431409A (en) * | 2013-08-10 | 2013-12-11 | 宫中林 | Kiwi fruit powder for alleviating constipation |
CN103734325A (en) * | 2013-11-28 | 2014-04-23 | 蚌埠海上明珠农业科技发展有限公司 | Kiwifruit fresh milk beverage and preparation method thereof |
CN104305056A (en) * | 2014-11-10 | 2015-01-28 | 重庆食品工业研究所 | Microencapsulated kiwi fruit ultramicropowder and preparation method thereof |
CN106212689A (en) * | 2016-07-29 | 2016-12-14 | 梁忠顺 | A kind of Dragonfruit Juice person in middle and old age's Nutrious milk powder and preparation method thereof |
CN107494743A (en) * | 2017-07-31 | 2017-12-22 | 安徽恋尚你食品有限公司 | A kind of instant Kiwi berry Moringa milk powder |
CN107549566A (en) * | 2017-09-27 | 2018-01-09 | 河南工业大学 | A kind of Kiwi berry solid beverage ferment and preparation method thereof |
WO2019045576A1 (en) * | 2017-09-04 | 2019-03-07 | Innovative Dairy Consultants Limited | Bioactive dairy products and processes for their manufacture |
CN110897118A (en) * | 2019-12-06 | 2020-03-24 | 广东省农业科学院蚕业与农产品加工研究所 | Fruit and vegetable microcapsule powder, fruit and vegetable microcapsule potato powder and preparation methods |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1060947A (en) * | 1990-11-01 | 1992-05-13 | 石河子市牛奶公司 | The preparation method of strawberry sour milk |
CN1263716A (en) * | 1999-10-03 | 2000-08-23 | 尹炳祥 | Fruit-vegetable-milk powder |
CN101073342A (en) * | 2007-06-25 | 2007-11-21 | 吴江市方霞企业信息咨询有限公司 | Carota milk powder |
CN101253894B (en) * | 2008-04-09 | 2010-06-23 | 北京市科威华食品工程技术有限公司 | Chiloe strawberry fruit milk and process technique thereof |
-
2009
- 2009-08-19 CN CN200910305773XA patent/CN101637201B/en not_active Expired - Fee Related
Cited By (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102919370A (en) * | 2012-11-14 | 2013-02-13 | 王梁琴 | Milk powder for strengthening immunity of babies |
CN102972523A (en) * | 2012-11-30 | 2013-03-20 | 内蒙古伊利实业集团股份有限公司 | Yogurt tablet and preparation method thereof |
CN102972523B (en) * | 2012-11-30 | 2014-08-13 | 内蒙古伊利实业集团股份有限公司 | Yogurt tablet and preparation method thereof |
CN103431409A (en) * | 2013-08-10 | 2013-12-11 | 宫中林 | Kiwi fruit powder for alleviating constipation |
CN103431409B (en) * | 2013-08-10 | 2016-03-23 | 宫中林 | A kind of kiwi fruit powder of relief of constipation |
CN103734325A (en) * | 2013-11-28 | 2014-04-23 | 蚌埠海上明珠农业科技发展有限公司 | Kiwifruit fresh milk beverage and preparation method thereof |
CN104305056A (en) * | 2014-11-10 | 2015-01-28 | 重庆食品工业研究所 | Microencapsulated kiwi fruit ultramicropowder and preparation method thereof |
CN106212689A (en) * | 2016-07-29 | 2016-12-14 | 梁忠顺 | A kind of Dragonfruit Juice person in middle and old age's Nutrious milk powder and preparation method thereof |
CN107494743A (en) * | 2017-07-31 | 2017-12-22 | 安徽恋尚你食品有限公司 | A kind of instant Kiwi berry Moringa milk powder |
WO2019045576A1 (en) * | 2017-09-04 | 2019-03-07 | Innovative Dairy Consultants Limited | Bioactive dairy products and processes for their manufacture |
CN107549566A (en) * | 2017-09-27 | 2018-01-09 | 河南工业大学 | A kind of Kiwi berry solid beverage ferment and preparation method thereof |
CN110897118A (en) * | 2019-12-06 | 2020-03-24 | 广东省农业科学院蚕业与农产品加工研究所 | Fruit and vegetable microcapsule powder, fruit and vegetable microcapsule potato powder and preparation methods |
Also Published As
Publication number | Publication date |
---|---|
CN101637201B (en) | 2011-12-28 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN101637201B (en) | Kiwi fruit juice powdered milk and preparation method thereof | |
CN102058124B (en) | Okra beverage and preparation method thereof | |
CN100399946C (en) | Hygienical functional food of blue berry and preparation method | |
CN102987490A (en) | Suaeda glauca wild vegetable juice and production method and application thereof | |
CN101461556A (en) | Seabuckthorn fruit walnut milk and method for producing the same | |
CN102224878A (en) | Rosa roxburghii tratt fruit cake and preparation method thereof | |
CN101632480A (en) | Jew's-ear primary pulp drink health-care nutritional food and preparation method | |
CN107751909A (en) | A kind of Actinidia kolomicta compound nectar and preparation method thereof | |
CN107307359A (en) | A kind of apple jam and preparation method thereof | |
CN104997013A (en) | Preparation method of nutrient gooseberry powder | |
CN110100900A (en) | Composite fruit juice type beans sour-soup drink preparation method | |
CN110122708A (en) | A kind of preparation method of full mulberry beverage | |
CN102987494A (en) | Raspberry and roxburgh rose health drink | |
CN110419654A (en) | A kind of compound juice beverage and its production technology | |
CN103637326A (en) | Full juice fruit vinegar beverage and production method thereof | |
CN104489820A (en) | Method for preparing dragon fruit liquid | |
CN102356896A (en) | Rosa roxburghii, narrow-leaved oleaster and apple composite fruit juice and preparation method thereof | |
CN104223307B (en) | A kind of Maca beverage and preparation method thereof | |
CN105249094A (en) | Lactation promoting pure natural cereal drink and material mixing structure | |
CN102835629B (en) | Fast-food ginger-juice butter milk oatmeal and making method thereof | |
CN109123272A (en) | A kind of processing method of sea buckthorn juice | |
CN101715831B (en) | Liquid dairy product containing corn steep liquor and making method thereof | |
CN107801881A (en) | A kind of preparation method of concentrated strawberry slurry | |
CN107296143A (en) | A kind of passion fruit fruitcake and its processing method | |
CN103385503B (en) | Pite pear and carrot juice drink |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
CF01 | Termination of patent right due to non-payment of annual fee | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20111228 Termination date: 20160819 |