CN101628735A - Method for preparing bismuth-series chemical product - Google Patents
Method for preparing bismuth-series chemical product Download PDFInfo
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- CN101628735A CN101628735A CN200910305977A CN200910305977A CN101628735A CN 101628735 A CN101628735 A CN 101628735A CN 200910305977 A CN200910305977 A CN 200910305977A CN 200910305977 A CN200910305977 A CN 200910305977A CN 101628735 A CN101628735 A CN 101628735A
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- CN
- China
- Prior art keywords
- bismuth
- preparation
- mother liquor
- oxide
- chemical product
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000000126 substance Substances 0.000 title claims abstract description 43
- 238000000034 method Methods 0.000 title claims abstract description 9
- 229910000416 bismuth oxide Inorganic materials 0.000 claims abstract description 65
- TYIXMATWDRGMPF-UHFFFAOYSA-N dibismuth;oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[Bi+3].[Bi+3] TYIXMATWDRGMPF-UHFFFAOYSA-N 0.000 claims abstract description 65
- 238000006243 chemical reaction Methods 0.000 claims abstract description 60
- 229910052797 bismuth Inorganic materials 0.000 claims abstract description 45
- JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 claims abstract description 44
- 229910000014 Bismuth subcarbonate Inorganic materials 0.000 claims abstract description 16
- MGLUJXPJRXTKJM-UHFFFAOYSA-L bismuth subcarbonate Chemical compound O=[Bi]OC(=O)O[Bi]=O MGLUJXPJRXTKJM-UHFFFAOYSA-L 0.000 claims abstract description 16
- 229940036358 bismuth subcarbonate Drugs 0.000 claims abstract description 16
- 238000007254 oxidation reaction Methods 0.000 claims abstract description 13
- 230000003647 oxidation Effects 0.000 claims abstract description 11
- 239000002070 nanowire Substances 0.000 claims abstract description 10
- KKMOSYLWYLMHAL-UHFFFAOYSA-N 2-bromo-6-nitroaniline Chemical compound NC1=C(Br)C=CC=C1[N+]([O-])=O KKMOSYLWYLMHAL-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000007788 liquid Substances 0.000 claims abstract description 4
- 239000012452 mother liquor Substances 0.000 claims description 53
- 238000002360 preparation method Methods 0.000 claims description 44
- PPNKDDZCLDMRHS-UHFFFAOYSA-N dinitrooxybismuthanyl nitrate Chemical compound [Bi+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O PPNKDDZCLDMRHS-UHFFFAOYSA-N 0.000 claims description 28
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 21
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 20
- 235000012054 meals Nutrition 0.000 claims description 18
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 16
- 239000007787 solid Substances 0.000 claims description 14
- 239000003795 chemical substances by application Substances 0.000 claims description 12
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 11
- 229910017604 nitric acid Inorganic materials 0.000 claims description 11
- QGWDKKHSDXWPET-UHFFFAOYSA-E pentabismuth;oxygen(2-);nonahydroxide;tetranitrate Chemical compound [OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[O-2].[Bi+3].[Bi+3].[Bi+3].[Bi+3].[Bi+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O QGWDKKHSDXWPET-UHFFFAOYSA-E 0.000 claims description 11
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims description 10
- 239000002253 acid Substances 0.000 claims description 9
- REKWPXFKNZERAA-UHFFFAOYSA-K bismuth;2-carboxyphenolate Chemical compound [Bi+3].OC1=CC=CC=C1C([O-])=O.OC1=CC=CC=C1C([O-])=O.OC1=CC=CC=C1C([O-])=O REKWPXFKNZERAA-UHFFFAOYSA-K 0.000 claims description 9
- 238000001816 cooling Methods 0.000 claims description 9
- 150000003839 salts Chemical class 0.000 claims description 9
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims description 8
- 239000000843 powder Substances 0.000 claims description 8
- 241001005836 Euchloe ausonia Species 0.000 claims description 7
- 235000012538 ammonium bicarbonate Nutrition 0.000 claims description 7
- JHXKRIRFYBPWGE-UHFFFAOYSA-K bismuth chloride Chemical compound Cl[Bi](Cl)Cl JHXKRIRFYBPWGE-UHFFFAOYSA-K 0.000 claims description 7
- ZREIPSZUJIFJNP-UHFFFAOYSA-K bismuth subsalicylate Chemical compound C1=CC=C2O[Bi](O)OC(=O)C2=C1 ZREIPSZUJIFJNP-UHFFFAOYSA-K 0.000 claims description 7
- 229960000782 bismuth subsalicylate Drugs 0.000 claims description 7
- CUBCNYWQJHBXIY-UHFFFAOYSA-N benzoic acid;2-hydroxybenzoic acid Chemical compound OC(=O)C1=CC=CC=C1.OC(=O)C1=CC=CC=C1O CUBCNYWQJHBXIY-UHFFFAOYSA-N 0.000 claims description 6
- 238000000227 grinding Methods 0.000 claims description 6
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims description 5
- 230000005587 bubbling Effects 0.000 claims description 5
- 239000004310 lactic acid Substances 0.000 claims description 5
- 235000014655 lactic acid Nutrition 0.000 claims description 5
- 229940095064 tartrate Drugs 0.000 claims description 5
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 4
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 claims description 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 2
- 229910021529 ammonia Inorganic materials 0.000 claims description 2
- 235000011089 carbon dioxide Nutrition 0.000 claims description 2
- 238000006253 efflorescence Methods 0.000 claims description 2
- 229910001338 liquidmetal Inorganic materials 0.000 claims description 2
- 238000003801 milling Methods 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- 206010037844 rash Diseases 0.000 claims description 2
- 230000008929 regeneration Effects 0.000 claims description 2
- 238000011069 regeneration method Methods 0.000 claims description 2
- 238000005507 spraying Methods 0.000 claims description 2
- 239000003153 chemical reaction reagent Substances 0.000 abstract description 4
- 239000002341 toxic gas Substances 0.000 abstract description 4
- 239000002351 wastewater Substances 0.000 abstract description 4
- 229960001482 bismuth subnitrate Drugs 0.000 abstract description 3
- 238000005265 energy consumption Methods 0.000 abstract description 3
- 230000000711 cancerogenic effect Effects 0.000 abstract description 2
- 238000004064 recycling Methods 0.000 abstract description 2
- QBWLKDFBINPHFT-UHFFFAOYSA-L 1,3,2$l^{2}-benzodioxabismin-4-one;hydrate Chemical compound O.C1=CC=C2C(=O)O[Bi]OC2=C1 QBWLKDFBINPHFT-UHFFFAOYSA-L 0.000 abstract 1
- HWSISDHAHRVNMT-UHFFFAOYSA-N Bismuth subnitrate Chemical compound O[NH+]([O-])O[Bi](O[N+]([O-])=O)O[N+]([O-])=O HWSISDHAHRVNMT-UHFFFAOYSA-N 0.000 abstract 1
- -1 bismuth trichlor, bismuth oxychloride Chemical compound 0.000 abstract 1
- RXPAJWPEYBDXOG-UHFFFAOYSA-N hydron;methyl 4-methoxypyridine-2-carboxylate;chloride Chemical compound Cl.COC(=O)C1=CC(OC)=CC=N1 RXPAJWPEYBDXOG-UHFFFAOYSA-N 0.000 abstract 1
- 238000010298 pulverizing process Methods 0.000 abstract 1
- 229960001860 salicylate Drugs 0.000 abstract 1
- 230000035484 reaction time Effects 0.000 description 10
- 238000002425 crystallisation Methods 0.000 description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 9
- 238000001035 drying Methods 0.000 description 8
- 239000000243 solution Substances 0.000 description 8
- 238000001704 evaporation Methods 0.000 description 5
- 230000008020 evaporation Effects 0.000 description 5
- 238000001914 filtration Methods 0.000 description 5
- 240000000203 Salix gracilistyla Species 0.000 description 4
- 230000008025 crystallization Effects 0.000 description 4
- 239000008367 deionised water Substances 0.000 description 4
- 229910021641 deionized water Inorganic materials 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 240000004307 Citrus medica Species 0.000 description 2
- AHUBLGVDRKDHAT-UHFFFAOYSA-N [Bi]=O.[Cl] Chemical compound [Bi]=O.[Cl] AHUBLGVDRKDHAT-UHFFFAOYSA-N 0.000 description 2
- ANERHPOLUMFRDC-UHFFFAOYSA-K bismuth citrate Chemical class [Bi+3].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O ANERHPOLUMFRDC-UHFFFAOYSA-K 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 238000013467 fragmentation Methods 0.000 description 2
- 238000006062 fragmentation reaction Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 239000010413 mother solution Substances 0.000 description 2
- CJJMLLCUQDSZIZ-UHFFFAOYSA-N oxobismuth Chemical class [Bi]=O CJJMLLCUQDSZIZ-UHFFFAOYSA-N 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 229910001220 stainless steel Inorganic materials 0.000 description 2
- 239000010935 stainless steel Substances 0.000 description 2
- 238000001149 thermolysis Methods 0.000 description 2
- 229940104825 bismuth aluminate Drugs 0.000 description 1
- 231100000315 carcinogenic Toxicity 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- PDSAKIXGSONUIX-UHFFFAOYSA-N hexaaluminum;dibismuth;oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Bi+3].[Bi+3] PDSAKIXGSONUIX-UHFFFAOYSA-N 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000002912 waste gas Substances 0.000 description 1
Landscapes
- Inorganic Compounds Of Heavy Metals (AREA)
- Catalysts (AREA)
Abstract
Description
Claims (5)
Priority Applications (1)
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CN2009103059773A CN101628735B (en) | 2009-08-24 | 2009-08-24 | Method for preparing bismuth-series chemical product |
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CN2009103059773A CN101628735B (en) | 2009-08-24 | 2009-08-24 | Method for preparing bismuth-series chemical product |
Publications (2)
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CN101628735A true CN101628735A (en) | 2010-01-20 |
CN101628735B CN101628735B (en) | 2011-11-16 |
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CN2009103059773A Expired - Fee Related CN101628735B (en) | 2009-08-24 | 2009-08-24 | Method for preparing bismuth-series chemical product |
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Cited By (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102690192A (en) * | 2012-06-25 | 2012-09-26 | 上海现代哈森(商丘)药业有限公司 | Bismuth citrate synthesizing method |
CN102942219A (en) * | 2012-11-16 | 2013-02-27 | 西南石油大学 | Method for preparing bismuth oxycarbonate nano tablet at normal temperature |
CN103011285A (en) * | 2012-12-27 | 2013-04-03 | 湖南金旺铋业股份有限公司 | Process for producing pentahydrate bismuth nitrate by employing crude bismuth oxide |
CN103011286A (en) * | 2012-12-27 | 2013-04-03 | 湖南金旺铋业股份有限公司 | Process for producing bismuth subcarbonate with crude bismuth oxide |
CN103145184A (en) * | 2013-03-25 | 2013-06-12 | 湖南金旺铋业股份有限公司 | Process for preparing needle-like bismuth oxide from bismuth by using wet method |
CN103172510A (en) * | 2011-12-20 | 2013-06-26 | 广东先导稀材股份有限公司 | Preparation method of bismuth citrate |
CN103183382A (en) * | 2013-03-25 | 2013-07-03 | 湖南金旺铋业股份有限公司 | Method for preparing acicular bismuth oxide with bismuth metal |
CN103183608A (en) * | 2011-12-30 | 2013-07-03 | 广东先导稀材股份有限公司 | Preparation method of bismuth subsalicylate |
CN103253706A (en) * | 2013-05-17 | 2013-08-21 | 中南大学 | Preparation method of basic bismuth nitrate |
CN103253705A (en) * | 2013-05-17 | 2013-08-21 | 中南大学 | Preparation method of basic bismuth carbonate |
CN108432804A (en) * | 2018-04-12 | 2018-08-24 | 青岛科技大学 | A kind of compound preservative and the preparation method and application thereof |
CN110015687A (en) * | 2019-04-12 | 2019-07-16 | 广东先导稀材股份有限公司 | The production method of five nitric hydrate bismuths |
RU2701013C1 (en) * | 2019-05-24 | 2019-09-24 | Общество с ограниченной ответственностью "Брайт Вэй" | Method of producing bismuth citrate |
CN110357778A (en) * | 2019-08-02 | 2019-10-22 | 湖南柿竹园有色金属有限责任公司 | A kind of preparation method of bismuth citrate |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102976406B (en) * | 2012-12-27 | 2014-07-30 | 湖南金旺铋业股份有限公司 | Process for producing bismuth subnitrate by coarse bismuth oxide |
RU2740292C1 (en) * | 2020-06-19 | 2021-01-12 | Федеральное государственное бюджетное учреждение науки Институт химии твердого тела и механохимии Сибирского отделения Российской академии наук | Method for producing base bismuth succinate |
-
2009
- 2009-08-24 CN CN2009103059773A patent/CN101628735B/en not_active Expired - Fee Related
Cited By (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103172510A (en) * | 2011-12-20 | 2013-06-26 | 广东先导稀材股份有限公司 | Preparation method of bismuth citrate |
CN103172510B (en) * | 2011-12-20 | 2015-09-30 | 广东先导稀材股份有限公司 | Preparation method of bismuth citrate |
CN103183608A (en) * | 2011-12-30 | 2013-07-03 | 广东先导稀材股份有限公司 | Preparation method of bismuth subsalicylate |
CN103183608B (en) * | 2011-12-30 | 2015-02-04 | 广东先导稀材股份有限公司 | Preparation method of bismuth subsalicylate |
CN102690192A (en) * | 2012-06-25 | 2012-09-26 | 上海现代哈森(商丘)药业有限公司 | Bismuth citrate synthesizing method |
CN102942219A (en) * | 2012-11-16 | 2013-02-27 | 西南石油大学 | Method for preparing bismuth oxycarbonate nano tablet at normal temperature |
CN103011286B (en) * | 2012-12-27 | 2014-07-30 | 湖南金旺铋业股份有限公司 | Process for producing bismuth subcarbonate with crude bismuth oxide |
CN103011285A (en) * | 2012-12-27 | 2013-04-03 | 湖南金旺铋业股份有限公司 | Process for producing pentahydrate bismuth nitrate by employing crude bismuth oxide |
CN103011286A (en) * | 2012-12-27 | 2013-04-03 | 湖南金旺铋业股份有限公司 | Process for producing bismuth subcarbonate with crude bismuth oxide |
CN103145184A (en) * | 2013-03-25 | 2013-06-12 | 湖南金旺铋业股份有限公司 | Process for preparing needle-like bismuth oxide from bismuth by using wet method |
CN103183382A (en) * | 2013-03-25 | 2013-07-03 | 湖南金旺铋业股份有限公司 | Method for preparing acicular bismuth oxide with bismuth metal |
CN103253705A (en) * | 2013-05-17 | 2013-08-21 | 中南大学 | Preparation method of basic bismuth carbonate |
CN103253706A (en) * | 2013-05-17 | 2013-08-21 | 中南大学 | Preparation method of basic bismuth nitrate |
CN108432804A (en) * | 2018-04-12 | 2018-08-24 | 青岛科技大学 | A kind of compound preservative and the preparation method and application thereof |
CN108432804B (en) * | 2018-04-12 | 2020-06-16 | 青岛科技大学 | Composite bacteriostatic agent and preparation method and application thereof |
CN110015687A (en) * | 2019-04-12 | 2019-07-16 | 广东先导稀材股份有限公司 | The production method of five nitric hydrate bismuths |
RU2701013C1 (en) * | 2019-05-24 | 2019-09-24 | Общество с ограниченной ответственностью "Брайт Вэй" | Method of producing bismuth citrate |
CN110357778A (en) * | 2019-08-02 | 2019-10-22 | 湖南柿竹园有色金属有限责任公司 | A kind of preparation method of bismuth citrate |
CN110357778B (en) * | 2019-08-02 | 2022-02-11 | 湖南柿竹园有色金属有限责任公司 | Preparation method of bismuth citrate |
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CN101628735B (en) | 2011-11-16 |
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