CN101613446B - Method for producing bisphenol A modified phenolic resin - Google Patents
Method for producing bisphenol A modified phenolic resin Download PDFInfo
- Publication number
- CN101613446B CN101613446B CN200910100857XA CN200910100857A CN101613446B CN 101613446 B CN101613446 B CN 101613446B CN 200910100857X A CN200910100857X A CN 200910100857XA CN 200910100857 A CN200910100857 A CN 200910100857A CN 101613446 B CN101613446 B CN 101613446B
- Authority
- CN
- China
- Prior art keywords
- add
- phenol
- formaldehyde
- bisphenol
- phenolic resin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 16
- IISBACLAFKSPIT-UHFFFAOYSA-N Bisphenol A Natural products C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 title claims abstract description 15
- -1 bisphenol A modified phenolic resin Chemical class 0.000 title claims abstract description 6
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims abstract description 39
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims abstract description 27
- 238000000034 method Methods 0.000 claims abstract description 14
- 239000002994 raw material Substances 0.000 claims abstract description 13
- 238000006243 chemical reaction Methods 0.000 claims abstract description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 11
- MNAHQWDCXOHBHK-UHFFFAOYSA-N 1-phenylpropane-1,1-diol Chemical compound CCC(O)(O)C1=CC=CC=C1 MNAHQWDCXOHBHK-UHFFFAOYSA-N 0.000 claims description 13
- 238000009413 insulation Methods 0.000 claims description 9
- 238000010792 warming Methods 0.000 claims description 9
- 238000003756 stirring Methods 0.000 claims description 6
- 239000000126 substance Substances 0.000 claims description 4
- 238000007664 blowing Methods 0.000 claims description 3
- 229920001568 phenolic resin Polymers 0.000 abstract description 6
- 239000005011 phenolic resin Substances 0.000 abstract description 6
- KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 abstract description 5
- 229920005989 resin Polymers 0.000 abstract description 5
- 239000011347 resin Substances 0.000 abstract description 5
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract description 4
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 abstract description 3
- 239000002023 wood Substances 0.000 abstract description 2
- RQPZNWPYLFFXCP-UHFFFAOYSA-L barium dihydroxide Chemical compound [OH-].[OH-].[Ba+2] RQPZNWPYLFFXCP-UHFFFAOYSA-L 0.000 abstract 2
- 239000011230 binding agent Substances 0.000 abstract 2
- 239000007859 condensation product Substances 0.000 abstract 2
- 230000003647 oxidation Effects 0.000 abstract 2
- 238000007254 oxidation reaction Methods 0.000 abstract 2
- 229910001863 barium hydroxide Inorganic materials 0.000 abstract 1
- 238000006555 catalytic reaction Methods 0.000 abstract 1
- 125000004029 hydroxymethyl group Chemical group [H]OC([H])([H])* 0.000 abstract 1
- 239000003607 modifier Substances 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
- 229920003987 resole Polymers 0.000 description 8
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 description 3
- 150000003505 terpenes Chemical class 0.000 description 3
- 235000007586 terpenes Nutrition 0.000 description 3
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 description 2
- 235000017166 Bambusa arundinacea Nutrition 0.000 description 2
- 235000017491 Bambusa tulda Nutrition 0.000 description 2
- 241001330002 Bambuseae Species 0.000 description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical class OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 2
- 235000015334 Phyllostachys viridis Nutrition 0.000 description 2
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 description 2
- 239000011425 bamboo Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000009833 condensation Methods 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 238000006482 condensation reaction Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 2
- RCHKEJKUUXXBSM-UHFFFAOYSA-N n-benzyl-2-(3-formylindol-1-yl)acetamide Chemical compound C12=CC=CC=C2C(C=O)=CN1CC(=O)NCC1=CC=CC=C1 RCHKEJKUUXXBSM-UHFFFAOYSA-N 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 125000004151 quinonyl group Chemical group 0.000 description 2
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 description 2
- KZMGYPLQYOPHEL-UHFFFAOYSA-N Boron trifluoride etherate Chemical compound FB(F)F.CCOCC KZMGYPLQYOPHEL-UHFFFAOYSA-N 0.000 description 1
- 206010013647 Drowning Diseases 0.000 description 1
- 241000779819 Syncarpia glomulifera Species 0.000 description 1
- 238000007259 addition reaction Methods 0.000 description 1
- 229940100198 alkylating agent Drugs 0.000 description 1
- 239000002168 alkylating agent Substances 0.000 description 1
- 238000005804 alkylation reaction Methods 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000032050 esterification Effects 0.000 description 1
- 238000005886 esterification reaction Methods 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- XGZVUEUWXADBQD-UHFFFAOYSA-L lithium carbonate Chemical compound [Li+].[Li+].[O-]C([O-])=O XGZVUEUWXADBQD-UHFFFAOYSA-L 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 125000001434 methanylylidene group Chemical group [H]C#[*] 0.000 description 1
- 229930003658 monoterpene Natural products 0.000 description 1
- 150000002773 monoterpene derivatives Chemical class 0.000 description 1
- 235000002577 monoterpenes Nutrition 0.000 description 1
- 239000001739 pinus spp. Substances 0.000 description 1
- 229930004725 sesquiterpene Natural products 0.000 description 1
- 150000004354 sesquiterpene derivatives Chemical class 0.000 description 1
- 229940036248 turpentine Drugs 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
Landscapes
- Phenolic Resins Or Amino Resins (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Description
Claims (1)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN200910100857XA CN101613446B (en) | 2009-07-13 | 2009-07-13 | Method for producing bisphenol A modified phenolic resin |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN200910100857XA CN101613446B (en) | 2009-07-13 | 2009-07-13 | Method for producing bisphenol A modified phenolic resin |
Publications (2)
Publication Number | Publication Date |
---|---|
CN101613446A CN101613446A (en) | 2009-12-30 |
CN101613446B true CN101613446B (en) | 2011-01-05 |
Family
ID=41493347
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN200910100857XA Expired - Fee Related CN101613446B (en) | 2009-07-13 | 2009-07-13 | Method for producing bisphenol A modified phenolic resin |
Country Status (1)
Country | Link |
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CN (1) | CN101613446B (en) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102732196B (en) * | 2011-04-01 | 2013-12-18 | 浙江安吉永生胶粘剂有限公司 | Environment-friendly type anticorrosive and antimildew phenolic glue and manufacturing method thereof |
CN102417570B (en) * | 2011-11-17 | 2013-02-13 | 江苏省新型复合研磨材料及制品工程技术研究中心 | Preparation method of environmentally-friendly phenolic resin |
JP2014208769A (en) | 2013-03-27 | 2014-11-06 | 住友ベークライト株式会社 | Resin composition for wet friction material, phenolic resin for wet friction material, and wet friction material |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101274976A (en) * | 2007-03-30 | 2008-10-01 | 上海友存实业有限公司 | Preparation for multicomponent copolycondensation phenolic resin |
-
2009
- 2009-07-13 CN CN200910100857XA patent/CN101613446B/en not_active Expired - Fee Related
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101274976A (en) * | 2007-03-30 | 2008-10-01 | 上海友存实业有限公司 | Preparation for multicomponent copolycondensation phenolic resin |
Non-Patent Citations (1)
Title |
---|
赵春玲等.双酚A改性甲阶酚醛树脂的合成和表征.《粘接》.2002,第23卷(第5期),9-11,21. * |
Also Published As
Publication number | Publication date |
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CN101613446A (en) | 2009-12-30 |
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C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
C41 | Transfer of patent application or patent right or utility model | ||
TR01 | Transfer of patent right |
Effective date of registration: 20111221 Address after: 311300 No. 63 East Road, Zhejiang, Ling'an Patentee after: Zhejiang A & F University Address before: 311300 Zhejiang Province, Ling'an City Ring Road No. 88 Patentee before: Zhejiang Forestry University |
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EE01 | Entry into force of recordation of patent licensing contract |
Application publication date: 20091230 Assignee: Zhejiang Anji Yongsheng Adhesive Co., Ltd. Assignor: Zhejiang A & F University Contract record no.: 2016330000047 Denomination of invention: Method for producing bisphenol A modified phenolic resin Granted publication date: 20110105 License type: Common License Record date: 20160324 |
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LICC | Enforcement, change and cancellation of record of contracts on the licence for exploitation of a patent or utility model | ||
CF01 | Termination of patent right due to non-payment of annual fee | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20110105 Termination date: 20170713 |