CN101603892A - Rock sample/earth sample saturation device by chemical solution - Google Patents

Rock sample/earth sample saturation device by chemical solution Download PDF

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Publication number
CN101603892A
CN101603892A CNA200910063202XA CN200910063202A CN101603892A CN 101603892 A CN101603892 A CN 101603892A CN A200910063202X A CNA200910063202X A CN A200910063202XA CN 200910063202 A CN200910063202 A CN 200910063202A CN 101603892 A CN101603892 A CN 101603892A
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China
Prior art keywords
glass
interface
chemical solution
sample
rock sample
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Granted
Application number
CNA200910063202XA
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Chinese (zh)
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CN101603892B (en
Inventor
周辉
杨鑫
程昌炳
张凯
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Wuhan Institute of Rock and Soil Mechanics of CAS
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Wuhan Institute of Rock and Soil Mechanics of CAS
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Application filed by Wuhan Institute of Rock and Soil Mechanics of CAS filed Critical Wuhan Institute of Rock and Soil Mechanics of CAS
Priority to CN200910063202XA priority Critical patent/CN101603892B/en
Publication of CN101603892A publication Critical patent/CN101603892A/en
Application granted granted Critical
Publication of CN101603892B publication Critical patent/CN101603892B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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  • Drying Of Solid Materials (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

The invention discloses a kind of rock sample/earth sample saturation device by chemical solution, relate to a kind of rock sample/earth sample laboratory equipment.Structure of the present invention is: vacuum drying ware (1) joins with first interface of vacuum meter (2) and glass three interface shunts (3) respectively, and second and third interface of glass three interface shunts (3) joins with glass jar (8) and vacuum pump (7) respectively by grass tube (9); First, second and third interface at glass three interface shunts (3) is respectively arranged with first, second and third glass switch (4,5,6).The present invention can prevent the corrosion of chemical solution to device; Saturated polylith rock sample simultaneously, and the use amount of chemical solution is few, saves cost; The vacuum tightness situation of finder inside at any time when vacuumizing exhausts and turns off all valves after vacuum sucks chemical solution, can make rock sample saturated more thoroughly, quick; Be applicable to that water, the chemical solution to rock sample/earth sample is saturated in the laboratory.

Description

Rock sample/earth sample saturation device by chemical solution
Technical field
The present invention relates to a kind of rock sample/earth sample laboratory equipment, relate in particular to the rock sample/earth sample saturation device by chemical solution that a kind of laboratory is used.
Background technology
We can study the different conditions of rock sample/earth sample when rock sample/earth sample is studied usually, as the rock sample under the rock sample of drying, saturated fully rock sample, the different state of saturation with other of rock sample under the state of nature; Thereby obtain the performance parameter of rock sample/earth sample under the different conditions.
Rock sample is carried out saturated processing, dual mode is arranged in the laboratory:
First kind of mode is to utilize vacuum pump+irony sample storage container, and this container general water in the laboratory comes rock sample/earth sample is vacuumized saturated;
The second way is exactly directly to soak, and rock sample is placed directly in the water soaks until saturated.
The advantage of first kind of mode be can well rock sample/earth sample be carried out water or solution saturated, but that this kind device is not suitable for that rock sample is carried out chemical solution is saturated, because chemical solution corrodes the sample storage container easily, and corrodes vacuum pump more or less.Though it is saturated that the second way can be carried out rock sample chemistry, the time is short to be not easy saturatedly, because residual gas is difficult for discharging in the rock sample, wants saturatedly fully, in fact is difficult to realize.
Therefore, rock sample/earth sample is carried out the specific saturation device of the saturated needs of chemical solution.
Summary of the invention
Purpose of the present invention is intended to overcome the shortcoming and defect that prior art exists, provide a kind of can to rock mass/soil body carry out chemical solution saturated, to container unaffected, safe lab setup under the corrosivity condition, a kind of rock sample/earth sample saturation device by chemical solution promptly is provided.
The object of the present invention is achieved like this:
The present invention includes vacuum drying ware, vacuum meter, glass three interface shunts, first glass switch, second glass switch, the 3rd glass switch, vacuum pump, glass jar and grass tube;
The vacuum drying ware joins with first interface of vacuum meter and glass three interface shunts respectively, and second and third interface of glass three interface shunts joins with glass jar and vacuum pump respectively by grass tube;
First, second and third interface at glass three interface shunts is respectively arranged with first, second and third glass switch.
Principle of work of the present invention is:
At first will need saturated rock sample/earth sample to be put in the vacuum drying ware sets, then second glass switch is transferred to buttoned-up status, first glass switch and the 3rd glass switch are transferred to full-gear, open vacuum pump, reach setting until the reading of vacuum meter; Close vacuum pump, close the 3rd glass switch simultaneously; Open second glass switch again, the negative pressure of vacuum drying ware can absorb the chemical solution in the glass jar in the vacuum drying ware automatically, after chemical solution soaks rock sample/earth sample fully, close first glass switch and and second glass switch, saturated until rock sample/earth sample.
The present invention has following advantage and good effect:
1. it is saturated rock sample/earth sample to be carried out chemical solution, can prevent the corrosion of chemical solution to device.
2. carry out rock sample/earth sample saturated in, saturated polylith rock sample simultaneously, and the use amount of chemical solution is few, saves cost.
3. the vacuum tightness situation of finder inside at any time when vacuumizing exhausts and turns off all valves after vacuum sucks chemical solution, can make rock sample saturated more thoroughly, quick.
Be applicable to that water, the chemical solution to rock sample/earth sample is saturated in the laboratory.
Description of drawings
Fig. 1 is a structural representation of the present invention.
Wherein:
The glass evacuated drying basin of 1-; The 2-vacuum meter; 3-glass three interface shunts;
4-first glass switch; 5-second glass switch; 6-the 3rd glass switch;
The 7-vacuum pump; The 8-glass jar; The 9-grass tube.
Embodiment
Below in conjunction with drawings and Examples to the detailed description of the invention:
One, overall
As Fig. 1, the present invention includes vacuum drying ware 1, vacuum meter 2, glass three interface shunts 3, first glass switch 4, second glass switch 5, the 3rd glass switch 6, vacuum pump 7, glass jar 8 and grass tube 9;
Vacuum drying ware 1 joins with first interface of vacuum meter 2 and glass three interface shunts 3 respectively, and second and third interface of glass three interface shunts 3 joins with glass jar 8 and vacuum pump 7 respectively by grass tube 9;
First, second and third interface at glass three interface shunts 3 is respectively arranged with first, second and third glass switch 4,5,6.
First interface and then the control vacuum drying ware 1 of first glass switch, 4 control glass, three interface shunts 3; Second glass switch 5 is controlled by the inflow of the chemical solution in 9 pairs of glass jars 8 of grass tube; The 3rd glass switch 6 vacuumizes by grass tube 9 and 7 pairs of vacuum drying wares 1 of vacuum pump and controls.
Two, functional part
1, the vacuum drying ware 1
Vacuum drying ware 1 is engaged by ground by glass lid and glass cylinder body and forms;
The top of glass lid is connected with vacuum meter 2, can observe the variation of vacuum tightness in the vacuum drying ware 1 at any time by vacuum meter 2;
First interface of three mouthfuls of shunts 3 of the waist of glass cylinder body and glass is connected.
2, vacuum meter 2
Vacuum meter 2 is a kind of parts commonly used, reacts the variation of vacuum tightness in the vacuum drying ware 1 at any time.
3, three mouthfuls of shunts 3 of glass
Three mouthfuls of shunts 3 of glass are a kind of parts commonly used.
4, first glass switch 4
First glass switch 4 is the supporting parts commonly used of a kind of and three mouthfuls of shunts of glass 3; Control vacuumizing or suck chemical solution in the vacuum drying ware 1.
5, second glass switch 5
Second glass switch 5 is the supporting parts commonly used of a kind of and three mouthfuls of shunts of glass 3; Inflow by the chemical solution in 9 pairs of glass jars 8 of grass tube is controlled.
6, the 3rd glass switch 6
The 3rd glass switch 6 is the supporting parts commonly used of a kind of and three mouthfuls of shunts of glass 3; Vacuumize by grass tube 9 and 7 pairs of vacuum drying wares 1 of vacuum pump and to control.
7, vacuum pump 7
Vacuum pump 7 is a kind of parts commonly used; Vacuumize processing by first glass switch 4 and 6 pairs of vacuum drying wares 1 of the 3rd glass switch.Require vacuum pump 7 energy acid and alkali-resistances, can reach negative atmospheric pressure when vacuumizing, and stable performance.
8, glass jar 8
Glass jar 8 is a kind of glass containers commonly used; Be used for holding chemical solution.
9, grass tube 9
Grass tube is a kind of part commonly used.

Claims (2)

1, a kind of rock sample/earth sample saturation device by chemical solution is characterized in that:
Comprise vacuum drying ware (1), vacuum meter (2), glass three interface shunts (3), first glass switch (4), second glass switch (5), the 3rd glass switch (6), vacuum pump (7), glass jar (8) and grass tube (9);
Vacuum drying ware (1) joins with first interface of vacuum meter (2) and glass three interface shunts (3) respectively, and second and third interface of glass three interface shunts (3) joins with glass jar (8) and vacuum pump (7) respectively by grass tube (9);
First, second and third interface at glass three interface shunts (3) is respectively arranged with first, second and third glass switch (4,5,6).
2, by the described a kind of rock sample/earth sample saturation device by chemical solution of claim 1, it is characterized in that:
Vacuum drying ware (1) is engaged by ground by glass lid and glass cylinder body and forms;
The top of glass lid is connected with vacuum meter (2);
The waist of glass cylinder body is connected with first interface of three mouthfuls of shunts of glass (3).
CN200910063202XA 2009-07-17 2009-07-17 Rock sample/earth sample saturation device by chemical solution Expired - Fee Related CN101603892B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN200910063202XA CN101603892B (en) 2009-07-17 2009-07-17 Rock sample/earth sample saturation device by chemical solution

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN200910063202XA CN101603892B (en) 2009-07-17 2009-07-17 Rock sample/earth sample saturation device by chemical solution

Publications (2)

Publication Number Publication Date
CN101603892A true CN101603892A (en) 2009-12-16
CN101603892B CN101603892B (en) 2011-11-30

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CN200910063202XA Expired - Fee Related CN101603892B (en) 2009-07-17 2009-07-17 Rock sample/earth sample saturation device by chemical solution

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103323315A (en) * 2013-06-24 2013-09-25 太原理工大学 Undisturbed soil vacuum soaking device and method for preparing sheet for SEM analysis
CN110470513A (en) * 2019-07-25 2019-11-19 山西大学 A kind of saturation device by chemical solution and its application method for Polluted Soil

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ATE528659T1 (en) * 2004-10-29 2011-10-15 Green Imaging Technologies Inc METHOD AND APPARATUS FOR MEASURING CAPILLARY PRESSURE IN A SAMPLE
CN100510727C (en) * 2006-03-24 2009-07-08 中国科学院南京土壤研究所 Method for measuring clay dispersion average binding free energy and adsorption free energy to cation
CN201454550U (en) * 2009-07-17 2010-05-12 中国科学院武汉岩土力学研究所 Rock sample/soil sample chemical solution saturation device

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103323315A (en) * 2013-06-24 2013-09-25 太原理工大学 Undisturbed soil vacuum soaking device and method for preparing sheet for SEM analysis
CN103323315B (en) * 2013-06-24 2015-07-15 太原理工大学 Undisturbed soil vacuum soaking device and method for preparing sheet for SEM analysis
CN110470513A (en) * 2019-07-25 2019-11-19 山西大学 A kind of saturation device by chemical solution and its application method for Polluted Soil
CN110470513B (en) * 2019-07-25 2021-05-14 山西大学 Chemical solution saturation device for polluted soil and use method thereof

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Granted publication date: 20111130

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