CN101592570A - A kind of metallurgical phase complex film - Google Patents
A kind of metallurgical phase complex film Download PDFInfo
- Publication number
- CN101592570A CN101592570A CNA2009100745812A CN200910074581A CN101592570A CN 101592570 A CN101592570 A CN 101592570A CN A2009100745812 A CNA2009100745812 A CN A2009100745812A CN 200910074581 A CN200910074581 A CN 200910074581A CN 101592570 A CN101592570 A CN 101592570A
- Authority
- CN
- China
- Prior art keywords
- present
- phase complex
- metallurgical phase
- complex film
- acetate fiber
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Manufacture Of Macromolecular Shaped Articles (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The present invention relates to a kind of metallurgical phase complex film, it is the metallurgical phase complex film that adopts following composition to make: (1) adopts acetone 100mml, methyl violet 150mmg and acetate fiber 5-6g under 20-30 ℃ of room temperature condition; (2) under 0-20 ℃ of room temperature condition, adopt acetone 100mml, methyl violet 150mmg and acetate fiber 4-5g, metallurgical phase complex film manufacture craft of the present invention is simple, the thin control easily of multiple thickness, skinning is easy, the present invention adopts the multiple film production material of tradition, material easily to buy, to metal non-corrosiveness, low price etc., the multiple film that utilizes the present invention to fill a prescription to make repeatedly applies in the on-the-spot metal lographic examination work, the metallographic structure of duplicating is true and reliable, consistent with field test and observations, for taking the reliable technique means that provide in the laboratory of on-the-spot metallographic structure.
Description
Technical field
The present invention relates to a kind of metallurgical phase complex film.
Technical background
The metallographic replica is the big workpiece metal lographic examination of non-destructive and important component part of on-the-spot metal lographic examination work, reason owing to check position and workpiece size, its metallographic structure is taken back the laboratory after generally duplicating by replica technique, does further observation analysis and photograph taking at fixed microscopically.The replica quality of metallographic structure has decisive role to the metallographic structure analysis and the judge work in later stage, and the replica material that generally adopts in this key link is multiple film.Acting as under the effect of solvent (being generally acetone) of multiple film fitted with the zone that presents microstructure, duplicates and obtains parts microstructure of metals pattern.At present, the source of multiple film has two kinds: one is outsourcing, and multiple film in the market is imported materials and items, and other industrial materials are few relatively because of its consumption, cost an arm and a leg the shortcoming that is difficult for buying so have; It two is employing standard " DL/T652-1998 metal replica technique technology guide rule " the recommended formula chamber of experimentizing self-control, and this kind method is subjected to temperature condition, operating personnel's technical merit to influence bigger.
Summary of the invention
Technical matters to be solved by this invention is do not influence under the situation of operating characteristic guaranteeing, provides a kind of thickness that can effectively solve in the multiple film production process thin wayward, the skinning difficult problem, be made into the high metallurgical phase complex film of power.
The present invention adopts following technical scheme:
The present invention is the metallurgical phase complex film that adopts following composition to make:
(1) under 20-30 ℃ of room temperature condition, adopts acetone 100mml, methyl violet 150mmg and acetate fiber 5-6g;
(2) under 0-20 ℃ of room temperature condition, adopt acetone 100mml, methyl violet 150mmg and acetate fiber 4-5g.
Beneficial effect of the present invention:
Metallurgical phase complex film manufacture craft of the present invention is simple, the thin control easily of multiple thickness, and skinning is easy, and the present invention adopts the multiple film production material of tradition, material easily to buy, to metal non-corrosiveness, low price etc.
Standard " DL/T652-1998 metal replica technique technology guide rule " recommended formula is: acetone: 60ml, acetate fiber: 3g, methyl violet: 100mg, triphenyl phosphate: 1.5g.Triphenyl phosphate is a kind of superpolymer damping plastic agent, and it adds the toughness of purpose for the multiple film of increase, but also plays the reduction surface tension simultaneously in multiple film production process, strengthens again the effect of the adhesion of film and glass plate, has increased the skinning difficulty.The composition of the multiple film of the present invention mainly is acetone, acetate fiber and methyl violet, in having removed standard recipe on the triphenyl phosphate basis, the multiple film formulation of the present invention is at skinning difficulty in the multiple film formulation manufacturing process of tradition, and the uppity difficult problem of the thickness of film is adjusted former multiple film formulation.The present invention has removed the triphenyl phosphate composition, adjusts the content of acetate fiber according to room temperature condition, can obtain the multiple film that quality meets request for utilization.The present invention fills a prescription and has considered Temperature Influence, through practical operation, has the thin control easily of multiple thickness, and skinning is easy to characteristics, by adjusting acetate fiber content, can obtain desirable multiple film.
The multiple film that utilizes the present invention to fill a prescription to make repeatedly applies in the on-the-spot metal lographic examination work, and the metallographic structure of duplicating is true and reliable, and is consistent with field test and observations, for taking the reliable technique means that provide in the laboratory of on-the-spot metallographic structure.
Embodiment
Manufacturing process of the present invention is identical with traditional of the prior art multiple film production process, just no longer adds triphenyl phosphate, and the Dichlorodiphenyl Acetate fiber content is adjusted simultaneously.Manufacturing process of the present invention is as follows: with 150mg methyl violet pulverize, pour in the bottle that 100ml acetone is housed, treat that methyl violet is fully dissolved after, add acetate fiber, if room temperature under 20-30 ℃ of condition, adds acetate fiber 5-6g; If room temperature under 0-20 ℃ of condition, adds acetate fiber 4-5g, stir, treat that it fully dissolves, pour on the clean no marking glass plate, rock glass plate it is evenly scattered, then it is covered, get final product skinning after 24 hours.
Embodiment one
The present invention is the metallurgical phase complex film that adopts following composition to make:
(1) under 20 ℃ of room temperature conditions, adopts acetone 100mml, methyl violet 150mmg and acetate fiber 5g;
(2) under 0 ℃ of room temperature condition, adopt acetone 100mml, methyl violet 150mmg and acetate fiber 4g.
Embodiment two
The present invention is the metallurgical phase complex film that adopts following composition to make:
(1) under 30 ℃ of room temperature conditions, adopts acetone 100mml, methyl violet 150mmg and acetate fiber 6g;
(2) under 10 ℃ of room temperature conditions, adopt acetone 100mml, methyl violet 150mmg and acetate fiber 5g.
Embodiment three
The present invention is the metallurgical phase complex film that adopts following composition to make:
(1) under 25 ℃ of room temperature conditions, adopts acetone 100mml, methyl violet 150mmg and acetate fiber 5.5g;
(2) under 20 ℃ of room temperature conditions, adopt acetone 100mml, methyl violet 150mmg and acetate fiber 4.5g.
Claims (1)
1, a kind of metallurgical phase complex film is characterized in that it is the metallurgical phase complex film that adopts following composition to make:
(1) under 20-30 ℃ of room temperature condition, adopts acetone 100mml, methyl violet 150mmg and acetate fiber 5-6g;
(2) under 0-20 ℃ of room temperature condition, adopt acetone 100mml, methyl violet 150mmg and acetate fiber 4-5g.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2009100745812A CN101592570A (en) | 2009-07-02 | 2009-07-02 | A kind of metallurgical phase complex film |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2009100745812A CN101592570A (en) | 2009-07-02 | 2009-07-02 | A kind of metallurgical phase complex film |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN101592570A true CN101592570A (en) | 2009-12-02 |
Family
ID=41407340
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNA2009100745812A Pending CN101592570A (en) | 2009-07-02 | 2009-07-02 | A kind of metallurgical phase complex film |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101592570A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103439156A (en) * | 2013-07-30 | 2013-12-11 | 国家电网公司 | Preparation method of laminating film for on-site metallographic examination of tower material |
| CN103454217A (en) * | 2012-06-05 | 2013-12-18 | 上海宝冶工程技术有限公司 | Metallographic coated test paper and preparation method thereof |
| CN109187541A (en) * | 2018-09-19 | 2019-01-11 | 西安热工研究院有限公司 | A kind of scene metallurgic replica method |
| CN109520815A (en) * | 2018-11-22 | 2019-03-26 | 大唐东北电力试验研究院有限公司 | A kind of metallurgic replica membrane preparation device |
| CN112280250A (en) * | 2020-10-30 | 2021-01-29 | 国电锅炉压力容器检验有限公司 | Metallographic replica material, preparation method and replica process thereof |
-
2009
- 2009-07-02 CN CNA2009100745812A patent/CN101592570A/en active Pending
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103454217A (en) * | 2012-06-05 | 2013-12-18 | 上海宝冶工程技术有限公司 | Metallographic coated test paper and preparation method thereof |
| CN103439156A (en) * | 2013-07-30 | 2013-12-11 | 国家电网公司 | Preparation method of laminating film for on-site metallographic examination of tower material |
| CN109187541A (en) * | 2018-09-19 | 2019-01-11 | 西安热工研究院有限公司 | A kind of scene metallurgic replica method |
| CN109520815A (en) * | 2018-11-22 | 2019-03-26 | 大唐东北电力试验研究院有限公司 | A kind of metallurgic replica membrane preparation device |
| CN109520815B (en) * | 2018-11-22 | 2024-04-02 | 大唐东北电力试验研究院有限公司 | Metallographic phase replica film preparation device |
| CN112280250A (en) * | 2020-10-30 | 2021-01-29 | 国电锅炉压力容器检验有限公司 | Metallographic replica material, preparation method and replica process thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Qi et al. | Biomass-derived nitrogen-doped carbon quantum dots: highly selective fluorescent probe for detecting Fe3+ ions and tetracyclines | |
| CN101592570A (en) | A kind of metallurgical phase complex film | |
| CN108489812B (en) | Material microstructure mechanical property characterization experimental device | |
| TW200601950A (en) | Heat dissipation apparatus with microstructure layer and manufacture method thereof | |
| CN102788788B (en) | Polymer-based detection agent for fast detection of heavy metal lead and its preparation method and use | |
| Zhang et al. | Silk sericin/poly (NIPAM/LMSH) nanocomposite hydrogels: Rapid thermo-responsibility and good carrier for cell proliferation | |
| CN205138928U (en) | Oral cavity combinational environment fatigue test device | |
| US20210172730A1 (en) | Method for fabricating speckle for high temperature deformation measurement of shaped refractory material | |
| CN101402217B (en) | Process for producing furniture | |
| CN105084340B (en) | Method for preparing thermal rectification parts and components from biological material | |
| Elkaseer et al. | FDM Process Optimisation for Low Surface Roughness and Energy Consumption | |
| CN107843495A (en) | One kind test flexible method of color printing film-covered iron face coat | |
| RU2014109847A (en) | TWO-WAY FORMING OF PLATES FROM ACRYLIC GLASS PLATE OF LARGE THICKNESS | |
| CN204807583U (en) | LCD test jig | |
| Zhou et al. | Forming process simulation and optimization of nickel-base superalloy turbine disk | |
| Meng et al. | Local melt-interdiffusion-rapid solidification mechanism of the as-milled Mg-Ni amorphous formation. | |
| TW200636234A (en) | Fabrication method for WO3 fine powder, and volatile organic compounds gas sensor made of the same, and the gas sensing material recipe | |
| Maestro-Guijarro et al. | Assessment of silver-based calcium silicate hydrate as a novel SERS sensor | |
| Shen et al. | Research on process testing of heat treatment for precision forming die materials. | |
| CN204666661U (en) | LCD two-sided test frame | |
| Qin et al. | One-step synthesized multisize AuAg alloy nanoparticles with high SERS sensitivity in directly detecting SARS-CoV-2 spike protein | |
| CN111141577A (en) | Coating method of colored gold interference film | |
| CN110283535A (en) | It is a kind of for improving the polishing fluid and preparation method thereof on ABS fused glass pellet surface | |
| RU2011151035A (en) | METHOD FOR PRODUCING NANOSTRUCTURED COAL CARBONATOR FOR CARBONING IRON-CARBON ALLOYS | |
| Kosec et al. | Heat treatment of steel forgings for the automotive industry. |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C12 | Rejection of a patent application after its publication | ||
| RJ01 | Rejection of invention patent application after publication |
Open date: 20091202 |