CN101591815B - Method for preparing functional nanometer textile - Google Patents
Method for preparing functional nanometer textile Download PDFInfo
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- CN101591815B CN101591815B CN2009100165450A CN200910016545A CN101591815B CN 101591815 B CN101591815 B CN 101591815B CN 2009100165450 A CN2009100165450 A CN 2009100165450A CN 200910016545 A CN200910016545 A CN 200910016545A CN 101591815 B CN101591815 B CN 101591815B
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Abstract
The present invention relates to a method for preparing a functional nanometer textile. The method comprises the following steps: mixing SiO2, Al2O3, ZrO2 and MgO nanometer materials, and adding a dispersing agent into the mixed nanometer materials to form a dispersing nanometer mixing material, wherein the weight percentage of the dispersing agent is 12 to 16 percent; adding the dispersing nanometer mixing material into a textile master batch, wherein the weight percentage of the dispersing nanometer mixing material is 8 to 10 percent; preparing a compound film by a fiber mixing mechanism; stretching the compound film to obtain the functional nanometer compound fiber; and spinning and weaving the functional nanometer compound fiber to obtain the functional nanometer textile. The normal emissivity of the microelement biochemical wave of the functional nanometer textile is more than 90 percent. The release rate of negative ions is more than 6,700 ions/Cm<2>. The functional nanometer textile has long-lasting and strong functionality; and the method has the advantages of simple preparation and high preparation efficiency, and is an ideal method for preparing the functional nanometer textile.
Description
Technical field
The present invention relates to a kind of preparation method of textiles, specifically is a kind of preparation method of functional nanometer textile.
Background technology
We know, the prior function textiles is that common fabric is immersed in a kind of cationic functional solution, take out oven dry then and make the function textile of doing, this textiles is because cationic functional solution has stronger oxidisability, though have a bit functional when new, but strong oxidizer also can bring side effect to health, is adding that fabric is to be immersed in oven dry processing in back in the cationic functional solution, and who the washing of using, the very fast disappearance of the functional meeting of textiles becomes common fabric
Summary of the invention
Technical problem to be solved by this invention is to overcome above-mentioned the deficiencies in the prior art, provides a kind of functional permanent, functional strong, the normal emittance of textiles microelement biological ripple greater than 90%, the anion release rate is greater than 6700/C m
2, without any the preparation method of the functional nanometer textile of side effect.
The technical scheme that the present invention solves the problems of the technologies described above employing is: a kind of preparation method of functional nanometer textile is characterized in that: at first with SiO
2, Al
2O
3, ZrO
2, the MgO nano material by weight percentage 26%-30%, 20%-25%, 18%-22%, 26-30% mix, obtain mixing nano material; Then add dispersant to mixing nano material, stir, form the dispersing nanometer compound, wherein the weight percentage of dispersant is 12%-16%; Again the dispersing nanometer compound is joined in the textiles masterbatch, wherein the weight percentage of dispersing nanometer compound is 8%-10%, the textiles masterbatch weight percentage be 90%-92%, in airtight container, fully mix and heat, make laminated film through three-dimensional mixer, then laminated film is stretched, obtain the function nano composite fibre, it makes functional nanometer textile through spinning, weaving cotton cloth.
The said dispersant of the present invention is the organosilicon oxireme.Said textiles masterbatch is polypropylene fibre master batch or nylon master batch or ethene master batch.
The present invention adds functional dispersing nanometer compound in the textiles masterbatch, utilize and bring into play the performance and the effect of various nano materials, gives nano-fabric with good function.The normal emittance of the textiles microelement biological ripple that makes after tested greater than 90%, the anion release rate is greater than 6700/C m
2, without any side effect, and functional permanent, functional strong.Against existing technologies, the present invention makes simply, and the preparation efficiency height is a kind of preparation method of desirable functional nanometer textile.
The specific embodiment
The present invention will be further described below in conjunction with embodiment:
The preparation method of a kind of functional nanometer textile of the present invention, it is at first with SiO
2, Al
2O
3, ZrO
2, the MgO nano material by weight percentage 26%-30%, 20%-25%, 18%-22%, 26-30% mix, obtain mixing nano material; Then add dispersant to mixing nano material, stir, form the dispersing nanometer compound, wherein the weight percentage of dispersant is 12%-16%; Again the dispersing nanometer compound is joined in the textiles masterbatch, wherein the weight percentage of dispersing nanometer compound is 8%-10%, the textiles masterbatch weight percentage be 90%-92%, in airtight container, fully mix and heat, make laminated film through three-dimensional mixer, then laminated film is stretched, obtain the function nano composite fibre, it makes functional nanometer textile through spinning, weaving cotton cloth.The preparation of laminated film, stretching, the spinning of function nano composite fibre, weaving cotton cloth belongs to prior art, no longer describes in detail.
Embodiment 1:
A kind of preparation method of functional nanometer textile is at first with SiO
2, Al
2O
3, ZrO
2, the MgO nano material 26%, 22%, 22%, 30% mixes by weight percentage, obtains mixing nano material.SiO wherein
2, Al
2O
3, ZrO
2, MgO nano material particle diameter＜100nm.Then add dispersant to mixing nano material, said dispersant is the organosilicon oxireme.Stir, form the dispersing nanometer compound, wherein the weight percentage of dispersant is 16%.The step that specifically is mixed with of dispersing nanometer compound is: inject earlier SiO in airtight container in proportion
2Nano material adds a certain proportion of dispersant then, treats SiO
2After nano material is scattered, inject Al more in proportion
2O
3Nano material adds dispersant again, treats Al
2O
3After nano material is scattered, add ZrO in proportion
2Nano material adds remaining in proportion dispersant again, treats nanometer ZrO
2After scattered, add the MgO nano material in proportion, fully mix, form the dispersing nanometer compound at last.The amount of above-mentioned each adding dispersant accounts for 1/3rd of dispersant total amount.
The dispersing nanometer compound is joined in the textiles masterbatch, said textiles masterbatch is the polypropylene fibre master batch again.Wherein the weight percentage of dispersing nanometer compound is 10%, the textiles masterbatch weight percentage be 90%%, in airtight container, fully mix and heat, make the polypropylene fibre laminated film that contains nano material through three-dimensional mixer, then the polypropylene fibre laminated film is stretched, make it split into the netted of fibrillar structure, obtain the function nano composite fibre, it makes function nano polypropylene fibre textiles through spinning, weaving cotton cloth.
The present invention spins cotton and weave cloth the function nano polypropylene fiber and makes function textile.The normal emittance of functional nanometer textile microelement biological ripple of the present invention is greater than 90%.The anion release rate is greater than 6700/Cm
2
Embodiment 2:
A kind of preparation method of functional nanometer textile is at first with SiO
2, Al
2O
3, ZrO
2, the MgO nano material 30%, 23%, 18%, 29% mixes by weight percentage, obtains mixing nano material; Then add dispersant to mixing nano material, said dispersant is the organosilicon oxireme.Stir, form the dispersing nanometer compound, wherein the weight percentage of dispersant is 12%; The dispersing nanometer compound is joined in the textiles masterbatch, said textiles masterbatch is the nylon master batch again.Wherein the weight percentage of dispersing nanometer compound is 8%, the textiles masterbatch weight percentage be 92%, in airtight container, fully mix and heat, make the nylon laminated film through three-dimensional mixer, then the nylon laminated film is stretched, obtain the function nano composite fibre, it makes function nano nylon shioze fabric through spinning, weaving cotton cloth.
Embodiment 3:
A kind of preparation method of functional nanometer textile is at first with SiO
2, Al
2O
3, ZrO
2, the MgO nano material 28%, 25%, 20%, 27% mixes by weight percentage, obtains mixing nano material; Then add dispersant to mixing nano material, said dispersant is the organosilicon oxireme.Stir, form the dispersing nanometer compound, wherein the weight percentage of dispersant is 15%; The dispersing nanometer compound is joined in the textiles masterbatch, said textiles masterbatch is the ethene master batch again.Wherein the weight percentage of dispersing nanometer compound is 9%, the textiles masterbatch weight percentage be 91%, in airtight container, fully mix and heat, make laminated film through three-dimensional mixer, then laminated film is stretched, obtain the function nano composite fibre, it makes functional nanometer textile through spinning, weaving cotton cloth.
Claims (3)
1. the preparation method of a functional nanometer textile, its feature may further comprise the steps: at first with SiO
2, Al
2O
3, ZrO
2, the MgO nano material by weight percentage 26%-30%, 20%-25%, 18%-22%, 26-30% mix, obtain mixing nano material; Then add dispersant to mixing nano material, stir, form the dispersing nanometer compound, wherein the weight percentage of dispersant is 12%-16%; Again the dispersing nanometer compound is joined in the textiles masterbatch, wherein the weight percentage of dispersing nanometer compound is 8%-10%, the weight percentage of textiles masterbatch is 90%-92%, in airtight container, fully mix and heat, make laminated film through three-dimensional mixer, then laminated film is stretched, obtain the function nano composite fibre, it makes functional nanometer textile through spinning, weaving cotton cloth.
2. according to the preparation method of the described functional nanometer textile of claim 1, it is characterized in that: said dispersant is the organosilicon oxireme.
3. according to the preparation method of the described functional nanometer textile of claim 1, it is characterized in that: said textiles masterbatch is polypropylene fibre master batch or nylon master batch or ethene master batch.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009100165450A CN101591815B (en) | 2009-06-19 | 2009-06-19 | Method for preparing functional nanometer textile |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009100165450A CN101591815B (en) | 2009-06-19 | 2009-06-19 | Method for preparing functional nanometer textile |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101591815A CN101591815A (en) | 2009-12-02 |
| CN101591815B true CN101591815B (en) | 2011-07-20 |
Family
ID=41406687
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2009100165450A Active CN101591815B (en) | 2009-06-19 | 2009-06-19 | Method for preparing functional nanometer textile |
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Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103881293B (en) * | 2014-03-15 | 2015-09-02 | 宿州学院 | A kind of high-adhesion composite modified master batch |
| CN106544870B (en) * | 2015-09-23 | 2018-10-23 | 上海沪正纳米科技有限公司 | A kind of functional textile auxiliary agent and preparation method thereof |
-
2009
- 2009-06-19 CN CN2009100165450A patent/CN101591815B/en active Active
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| Publication number | Publication date |
|---|---|
| CN101591815A (en) | 2009-12-02 |
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