CN101589764B - 一种饲料级一水硫酸亚铁的包被方法 - Google Patents
一种饲料级一水硫酸亚铁的包被方法 Download PDFInfo
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- CN101589764B CN101589764B CN2009100407869A CN200910040786A CN101589764B CN 101589764 B CN101589764 B CN 101589764B CN 2009100407869 A CN2009100407869 A CN 2009100407869A CN 200910040786 A CN200910040786 A CN 200910040786A CN 101589764 B CN101589764 B CN 101589764B
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- Prior art keywords
- ferrous sulfate
- sulfate monohydrate
- feed grade
- grade ferrous
- coating agent
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- XBDUTCVQJHJTQZ-UHFFFAOYSA-L iron(2+) sulfate monohydrate Chemical compound O.[Fe+2].[O-]S([O-])(=O)=O XBDUTCVQJHJTQZ-UHFFFAOYSA-L 0.000 title claims abstract description 115
- 239000011248 coating agent Substances 0.000 title claims abstract description 62
- 238000000034 method Methods 0.000 title claims abstract description 17
- 238000000576 coating method Methods 0.000 title claims abstract description 11
- 238000003756 stirring Methods 0.000 claims abstract description 11
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 64
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 claims description 32
- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 32
- 239000000377 silicon dioxide Substances 0.000 claims description 32
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 claims description 32
- 229920001027 sodium carboxymethylcellulose Polymers 0.000 claims description 32
- 229920002472 Starch Polymers 0.000 claims description 22
- 235000019698 starch Nutrition 0.000 claims description 22
- 239000008107 starch Substances 0.000 claims description 22
- 229910021536 Zeolite Inorganic materials 0.000 claims description 21
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims description 21
- 239000000843 powder Substances 0.000 claims description 21
- 239000010457 zeolite Substances 0.000 claims description 21
- 239000000203 mixture Substances 0.000 abstract description 10
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 8
- FPIPGXGPPPQFEQ-UHFFFAOYSA-N 13-cis retinol Natural products OCC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-UHFFFAOYSA-N 0.000 abstract description 5
- FPIPGXGPPPQFEQ-BOOMUCAASA-N Vitamin A Natural products OC/C=C(/C)\C=C\C=C(\C)/C=C/C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-BOOMUCAASA-N 0.000 abstract description 5
- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 abstract description 5
- 239000002131 composite material Substances 0.000 abstract description 5
- 238000004519 manufacturing process Methods 0.000 abstract description 5
- 230000008569 process Effects 0.000 abstract description 5
- 235000019155 vitamin A Nutrition 0.000 abstract description 5
- 239000011719 vitamin A Substances 0.000 abstract description 5
- 229940045997 vitamin a Drugs 0.000 abstract description 5
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 abstract description 4
- 229930003268 Vitamin C Natural products 0.000 abstract description 4
- 235000019154 vitamin C Nutrition 0.000 abstract description 4
- 239000011718 vitamin C Substances 0.000 abstract description 4
- 230000006378 damage Effects 0.000 abstract description 3
- 238000006479 redox reaction Methods 0.000 abstract description 3
- 230000004888 barrier function Effects 0.000 abstract description 2
- 230000008901 benefit Effects 0.000 abstract description 2
- 230000002776 aggregation Effects 0.000 abstract 1
- 238000004220 aggregation Methods 0.000 abstract 1
- 230000002209 hydrophobic effect Effects 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
- 239000011573 trace mineral Substances 0.000 abstract 1
- 235000013619 trace mineral Nutrition 0.000 abstract 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 17
- 235000003891 ferrous sulphate Nutrition 0.000 description 17
- 239000011790 ferrous sulphate Substances 0.000 description 17
- SURQXAFEQWPFPV-UHFFFAOYSA-L iron(2+) sulfate heptahydrate Chemical compound O.O.O.O.O.O.O.[Fe+2].[O-]S([O-])(=O)=O SURQXAFEQWPFPV-UHFFFAOYSA-L 0.000 description 11
- 235000013312 flour Nutrition 0.000 description 10
- 229910000359 iron(II) sulfate Inorganic materials 0.000 description 10
- 239000004575 stone Substances 0.000 description 9
- 239000000463 material Substances 0.000 description 8
- UHZZMRAGKVHANO-UHFFFAOYSA-M chlormequat chloride Chemical compound [Cl-].C[N+](C)(C)CCCl UHZZMRAGKVHANO-UHFFFAOYSA-M 0.000 description 6
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 4
- 238000007792 addition Methods 0.000 description 4
- 239000010949 copper Substances 0.000 description 4
- VTLYFUHAOXGGBS-UHFFFAOYSA-N Fe3+ Chemical compound [Fe+3] VTLYFUHAOXGGBS-UHFFFAOYSA-N 0.000 description 3
- 241001465754 Metazoa Species 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 229910052802 copper Inorganic materials 0.000 description 3
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 description 3
- 238000002425 crystallisation Methods 0.000 description 3
- 230000008025 crystallization Effects 0.000 description 3
- BVTBRVFYZUCAKH-UHFFFAOYSA-L disodium selenite Chemical compound [Na+].[Na+].[O-][Se]([O-])=O BVTBRVFYZUCAKH-UHFFFAOYSA-L 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 239000004519 grease Substances 0.000 description 3
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 3
- 235000021590 normal diet Nutrition 0.000 description 3
- 230000003647 oxidation Effects 0.000 description 3
- 238000007254 oxidation reaction Methods 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 235000015921 sodium selenite Nutrition 0.000 description 3
- 239000011781 sodium selenite Substances 0.000 description 3
- 229960001471 sodium selenite Drugs 0.000 description 3
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 description 2
- 229930003427 Vitamin E Natural products 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 2
- ICIWUVCWSCSTAQ-UHFFFAOYSA-M iodate Chemical compound [O-]I(=O)=O ICIWUVCWSCSTAQ-UHFFFAOYSA-M 0.000 description 2
- 230000014759 maintenance of location Effects 0.000 description 2
- ISPYRSDWRDQNSW-UHFFFAOYSA-L manganese(II) sulfate monohydrate Chemical compound O.[Mn+2].[O-]S([O-])(=O)=O ISPYRSDWRDQNSW-UHFFFAOYSA-L 0.000 description 2
- 230000000050 nutritive effect Effects 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 235000019165 vitamin E Nutrition 0.000 description 2
- 229940046009 vitamin E Drugs 0.000 description 2
- 239000011709 vitamin E Substances 0.000 description 2
- 239000004151 Calcium iodate Substances 0.000 description 1
- 206010023126 Jaundice Diseases 0.000 description 1
- 244000046052 Phaseolus vulgaris Species 0.000 description 1
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 1
- 240000008042 Zea mays Species 0.000 description 1
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 1
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000003674 animal food additive Substances 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- UHWJJLGTKIWIJO-UHFFFAOYSA-L calcium iodate Chemical compound [Ca+2].[O-]I(=O)=O.[O-]I(=O)=O UHWJJLGTKIWIJO-UHFFFAOYSA-L 0.000 description 1
- 235000019390 calcium iodate Nutrition 0.000 description 1
- 229910000366 copper(II) sulfate Inorganic materials 0.000 description 1
- 235000005822 corn Nutrition 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000003862 health status Effects 0.000 description 1
- 230000003053 immunization Effects 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 230000003859 lipid peroxidation Effects 0.000 description 1
- 239000011572 manganese Substances 0.000 description 1
- 229940099596 manganese sulfate Drugs 0.000 description 1
- 235000007079 manganese sulphate Nutrition 0.000 description 1
- 239000011702 manganese sulphate Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000013112 stability test Methods 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 description 1
- 229960001763 zinc sulfate Drugs 0.000 description 1
- 229910000368 zinc sulfate Inorganic materials 0.000 description 1
- RNZCSKGULNFAMC-UHFFFAOYSA-L zinc;hydrogen sulfate;hydroxide Chemical compound O.[Zn+2].[O-]S([O-])(=O)=O RNZCSKGULNFAMC-UHFFFAOYSA-L 0.000 description 1
Landscapes
- Medicinal Preparation (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Fodder In General (AREA)
Abstract
Description
种类 | 第1天 | 第10天 | 第30天 |
包被FeSO4·H2O+石粉,1∶1 | 15.02 | 14.99 | 14.97 |
普通FeSO4·H2O+石粉,1∶1 | 15.30 | 14.95 | 14.83 |
种类 | 第1天 | 第10天 | 第30天 |
包被FeSO4·H2O+石粉,1∶1 | 100 | 99.80 | 99.67 |
普通FeSO4·H2O+石粉,1∶1 | 100 | 97.71 | 96.93 |
原料 | 规格(%) | 用量(kg/t) |
硫酸铜 | Cu:25 | 200 |
硫酸亚铁 | Fe:30 | 360 |
硫酸锌 | Zn:34.5 | 231.5 |
硫酸锰 | Mn:31.8 | 47 |
碘酸钙 | I:5 | 10 |
亚硒酸钠 | Se:1 | 16.5 |
载体 | 135 |
Claims (3)
Priority Applications (1)
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CN2009100407869A CN101589764B (zh) | 2009-07-03 | 2009-07-03 | 一种饲料级一水硫酸亚铁的包被方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN2009100407869A CN101589764B (zh) | 2009-07-03 | 2009-07-03 | 一种饲料级一水硫酸亚铁的包被方法 |
Publications (2)
Publication Number | Publication Date |
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CN101589764A CN101589764A (zh) | 2009-12-02 |
CN101589764B true CN101589764B (zh) | 2011-09-28 |
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CN2009100407869A Active CN101589764B (zh) | 2009-07-03 | 2009-07-03 | 一种饲料级一水硫酸亚铁的包被方法 |
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Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101836697A (zh) * | 2010-05-17 | 2010-09-22 | 赣州八维生物科技有限公司 | 聚乙二醇包被碘化钾及其制备方法 |
CN101836696A (zh) * | 2010-05-17 | 2010-09-22 | 赣州八维生物科技有限公司 | 聚乙二醇包被硫酸亚铁及其制备方法 |
CN101912049A (zh) * | 2010-07-27 | 2010-12-15 | 广州市正百饲料科技有限公司 | 包被微量元素预混料及其制备方法 |
CN106417921A (zh) * | 2016-08-31 | 2017-02-22 | 成都蜀星饲料有限公司 | 一种硫酸铜、硫酸亚铁、硫酸锌包被加工方法 |
CN111631310A (zh) * | 2020-07-13 | 2020-09-08 | 四川大想生物科技有限公司 | 一种动物饲料用替抗添加剂及制备方法 |
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C06 | Publication | ||
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SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right |
Effective date of registration: 20191209 Address after: 510700 Room 102, No. 172, hengshabai new street, Dasha street, Huangpu District, Guangzhou City, Guangdong Province Patentee after: Guangzhou kangruide feed Technology Co.,Ltd. Address before: 510663 No. 8 Cliff Road, Science Town, Guangzhou hi tech Industrial Development Zone, Guangdong, China Patentee before: GUANGZHOU KANRET BIO TECHNOLOGY Co.,Ltd. |
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TR01 | Transfer of patent right | ||
CP01 | Change in the name or title of a patent holder |
Address after: 510700 Room 102, No. 172, Hengsha Baixin street, Dasha street, Huangpu District, Guangzhou City, Guangdong Province Patentee after: Guangzhou kangruide agriculture and animal husbandry technology Co.,Ltd. Address before: 510700 Room 102, No. 172, Hengsha Baixin street, Dasha street, Huangpu District, Guangzhou City, Guangdong Province Patentee before: Guangzhou kangruide feed Technology Co.,Ltd. |
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CP01 | Change in the name or title of a patent holder | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A coating method for feed grade ferrous sulfate monohydrate Effective date of registration: 20231228 Granted publication date: 20110928 Pledgee: Societe Generale Bank Limited by Share Ltd. Guangzhou branch Pledgor: Guangzhou kangruide agriculture and animal husbandry technology Co.,Ltd. Registration number: Y2023980075068 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right |