CN101580756B - Process for preparing micro emulsifying essence - Google Patents
Process for preparing micro emulsifying essence Download PDFInfo
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- CN101580756B CN101580756B CN2009100273421A CN200910027342A CN101580756B CN 101580756 B CN101580756 B CN 101580756B CN 2009100273421 A CN2009100273421 A CN 2009100273421A CN 200910027342 A CN200910027342 A CN 200910027342A CN 101580756 B CN101580756 B CN 101580756B
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Abstract
The invention relates to a system and a process for preparing a micro emulsifying essence. The system for preparing the micro emulsifying essence comprises a boiler body provided with a jacket and a circulating pump, wherein a heating-cooling pipeline is arranged in the jacket of the boiler body, and the boiler body is communicated with the circulating pump. A method for preparing the micro emulsifying essence comprises the following steps: using an essence as a base material and propanediol as an auxiliary material; and under the action of an emulsifying agent, performing the processes of material taking, auxiliary material preheating, initial reaction, circular reaction, detection and material discharge to prepare the micro emulsifying essence. The system adopts the heating-cooling pipeline to control the reaction temperature, and the adjustment is convenient and quick; and the production process is simple, the raw material of the emulsifying agent used in the production has a wide source and low cost, and the finally prepared products have stable quality and excellent performance indexes.
Description
Technical field
The invention belongs to essence manufacturing technology field, specifically relate to a kind of micro-emulsified essence preparation system and technology thereof.
Background technology
Essence and daily life relation are very close, are tobacco foodstuffs industry, medical and health industry, daily chemical industry and other industrial indispensable important source material.According to medical evidence, fragrance can Ginseng Extract, and steadily function of human body makes us relaxed and joyful.Along with improving constantly of quality of life standard, people are more and more big to the demand of essence product, and are also more and more high to the requirement of essence quality simultaneously.
The production in flavouring essence for tobacco every year is in great demand.At present there are drawbacks such as use complex process, result of use be not obvious in powder, lotion essence in tobacco processing course.But because of powder, lotion essence unique fragrance and fragrance, make it in tobacco processing course, be in the status that can not be substituted.It is to solve the crucial effective way that powdered flavor itself uses drawback that powdered flavor is changed into liquid essence.
Simple dissolving transforms that not only transformation efficiency is low, and the milk sap thermodynamic instability that forms, and layering easily easily produces precipitation, influences result of use.Adopt micro-emulsion technology can improve transformation efficiency greatly, can form the microemulsion of stable homogeneous, this emulsion becomes Thermodynamically stable milk sap to exist, centrifugal precipitation and the crystallization precipitate of also not producing, size is generally 10 ∽ 100nm, and the spray in the very suitable tobacco processing course uses.Microemulsion can finely improve the jealous of tobacco leaf in pipe tobacco and tobacco sheet, but the special state controlled release of micro emulsion drop and slowly-releasing fragrance make lasting effective lastingly.
Discover, in the material oily, that the water two-phase is immiscible, add a large amount of tensio-active agent and cosurfactant, make the surface tension of oil, water drop to extremely low, even reduce to negative value in moment, make whole system spontaneously form translucent or transparent isotropic liquid system, water is dispersed in as disperse phase and forms the W/O microemulsion in the oil, and the liquid pearl radius of this microemulsion is generally 10-100nm, thermodynamics is highly stable, not stratified, do not precipitate, high temperature resistant, easy storage.
Summary of the invention
The object of the invention is to provide a kind of simple in structure, processing ease, stay-in-grade micro-emulsified essence preparation system and technology thereof, and this technology is simple, the emulsifying agent raw material sources are wide, cost is low, product performance index is good.
Purpose of the present invention realizes by following technical scheme: a kind of micro-emulsified essence preparation system, it is characterized in that comprising: the pot body and the recycle pump that are provided with chuck, described pot body top is provided with opening for feed, sidewall offers heating cooling inlet, the bottom offers the heating coolant outlet, the heating-cooling coil road is housed in the chuck, and described heating-cooling coil road is connected with described heating cooling inlet, heating coolant outlet respectively; In the pot body stirring rake is installed, stirring rake drives by being installed in pot agitator motor that the body top is coupled; The circulation output tube communication loop pump top that the pot body is installed by sidewall, on the circulation output tube cross over valve is housed, described cross over valve control feed liquid is changed between outer circulation and discharging, the recycle pump bottom is communicated in pot body from bottom of pot body by the circulation input tube, and described recycle pump drives by circulation motor.
As further improvement of the utility model, described heating-cooling coil curb pot body periphery is provided with.
A kind of micro-emulsified essence preparation method is a base-material with essence, and propylene glycol is an auxiliary material, under the emulsifying agent effect, gets material, auxiliary material preheating, initial reaction, circulating reaction, detection discharging step through batching and is prepared into micro-emulsified essence, and the detailed process step is as follows:
(1) batching is got material: two (2-ethylhexyl) succsinic acid semi-annular jade pendants acid sodium and tween are composite in 2: 1 ratio, make first auxiliary; Benzyl pool and Yelkin TTS is composite in 2: 1 ratio, make second auxiliary; Take by weighing essence 30-50% by weight percentage, propylene glycol 20-30%, emulsifying agent 20-30%, the first auxiliary 2-3%, the second auxiliary 2-3%;
(2) auxiliary material preheating: the fresh propylene glycol that step (1) is taken by weighing adds in the pot body of described preparation system, feeds steam, is heated to 100 ℃;
(3) initial reaction: the essence that step (1) is taken by weighing adds in the pot body from opening for feed, starts agitator motor and drives stirring rake and stir, and makes propylene glycol after essence and preheating thorough mixing 10～15 minutes under 50-100 ℃ normal pressure;
(4) circulating reaction: the emulsifying agent that step (1) is taken by weighing, first auxiliary, second auxiliary add in the pot body then, open cross over valve and circulation motor, allow feed liquid circulate between pot body and recycle pump, it is more abundant that feed liquid is mixed, essence and propylene glycol circulating reaction 20～30 minutes;
(5) detect discharging: detect every sampling in five minutes, after product index reached respective standard, regulating reversing valve was the discharging state, emits the reaction feed liquid, and cooling gets product.
The present invention compared with prior art adopts heating-cooling coil road control reaction temperature, and is easy to adjust quick; Production technique is simple, and the emulsifying agent raw material sources of using in the production are extensive, with low cost, final finished product steady quality, and every performance index are good.
Description of drawings
Fig. 1 is the structural representation of micro-emulsified essence preparation system of the present invention.
Drawing reference numeral explanation: 1-circulation motor, 2-recycle pump, 3-circulation output tube, 4-cross over valve, 5-stirring rake, 6-agitator motor, 7-heating cooling inlet, 8-chuck, 9-pot body, 10-heating coolant outlet, 11-circulation input tube.
Embodiment
As shown in Figure 1, described micro-emulsified essence preparation system comprises pot body 9 and the recycle pump 2 that is provided with chuck 8, described pot body 9 tops are provided with opening for feed, sidewall offers heating cooling inlet 7, the bottom offers heating coolant outlet 10, the heating-cooling coil road that is provided with along pot body 9 peripheries is housed in the chuck 8, and described heating-cooling coil road is connected with described heating cooling inlet 7, heating coolant outlet 10 respectively; In the pot body 9 stirring rake 5 is installed, stirring rake 5 drives by being installed in the coupled agitator motor in pot body 9 tops 6; Circulation output tube 3 communication loop pumps 2 tops that pot body 9 is installed by sidewall, cross over valve 4 is housed on the circulation output tube 3, described cross over valve 4 control feed liquids are changed between outer circulation and discharging, recycle pump 2 bottoms are communicated in pot body 9 from pot body 9 bottoms by circulation input tube 11, and described recycle pump 2 drives by circulation motor 1.
The invention will be further described below in conjunction with specific embodiment.
Earlier the auxiliary material propylene glycol is added in the pot body 9, start recycle pump 2, ON cycle allows propylene glycol walk jar, after walking jar to finish, emits propylene glycol; Two (2-ethylhexyl) succsinic acid semi-annular jade pendants acid sodium and tween are composite in 2: 1 ratio, make first auxiliary; Benzyl pool and Yelkin TTS is composite in 2: 1 ratio, make second auxiliary.
Embodiment 1: produce flavouring essence for tobacco MM186.
Take by weighing MM125 essence 40g, propylene glycol 25g, emulsifying agent 30g, the first auxiliary 2g, the second auxiliary 3g; The fresh propylene glycol that takes by weighing is added in the pot body 9 of described preparation system, feed steam, be heated to 100 ℃ from heating cooling inlet 7; The essence that takes by weighing is added in the pot body 9 from opening for feed, start agitator motor 6 and drive stirring rakes 5 and stir, make propylene glycol after MM125 and the heating at thorough mixing under 70 ℃ the normal pressure about 10 minutes; Then emulsifying agent, first auxiliary, second auxiliary that takes by weighing added in the pot body 9, open cross over valve 4 and circulation motor 1, allow feed liquid circulate between pot body 9 and recycle pump 2, it is more abundant that feed liquid is mixed, and essence and propylene glycol circulating reaction are about 30 minutes; Detect every sampling in five minutes then, after product index reaches respective standard, regulate reversing valve 4 for the discharging state, emit the reaction feed liquid, cooling promptly gets flavouring essence for tobacco MM186.
Embodiment 2: produce the flavouring essence for tobacco Phytoconcentrol Chamomile.
Take by weighing Phytoconcentrol Chamomile medicinal extract 35g, emulsifying agent 30g, licorice powder 30g, the first auxiliary 3g, the second auxiliary 3g is because Phytoconcentrol Chamomile medicinal extract is liquid, so need not to add propylene glycol; Earlier Phytoconcentrol Chamomile medicinal extract is added in the pot body 9, feed steam, be heated to 100 ℃; Start agitator motor 6 then and drive stirring rake 5 stirrings, slowly add licorice powder and a spot of caramel colorant simultaneously, make Phytoconcentrol Chamomile medicinal extract, licorice powder and caramel colorant thorough mixing under 80 ℃ normal pressure, be stirred to complete dissolved state; Then emulsifying agent, first auxiliary, second auxiliary that takes by weighing added in the pot body 9, open cross over valve 4 and circulation motor 1, allow feed liquid circulate between pot body 9 and recycle pump 2, it is more abundant that feed liquid is mixed, and circulating reaction is about 25 minutes; Detect every sampling in five minutes then, after product index reaches respective standard, regulate reversing valve 4 for the discharging state, emit the reaction feed liquid, cooling promptly gets the flavouring essence for tobacco Phytoconcentrol Chamomile.
Claims (1)
1. the preparation method of a micro-emulsified essence, it is characterized in that: be base-material with essence, propylene glycol is an auxiliary material, under the emulsifying agent effect, get material, auxiliary material preheating, initial reaction, circulating reaction, detection discharging step through batching and be prepared into micro-emulsified essence, the detailed process step is as follows:
(1) batching is got material: two (2-ethylhexyl) succsinic acid semi-annular jade pendants acid sodium and tween are composite in 2: 1 ratio, make first auxiliary; Benzyl pool and Yelkin TTS is composite in 2: 1 ratio, make second auxiliary; Take by weighing essence 30-50% by weight percentage, propylene glycol 20-30%, emulsifying agent 20-30%, the first auxiliary 2-3%, the second auxiliary 2-3%; Each component sum is 100%;
(2) auxiliary material preheating: the fresh propylene glycol that step (1) is taken by weighing adds in the pot body (9) of preparation system, feeds steam, is heated to 100 ℃;
(3) initial reaction: the essence that step (1) is taken by weighing adds in the pot body (9) from opening for feed, starts agitator motor (6) and drives stirring rake (5) and stir, and makes propylene glycol after essence and preheating thorough mixing 10～15 minutes under 50-100 ℃ normal pressure;
(4) circulating reaction: the emulsifying agent that step (1) is taken by weighing, first auxiliary, second auxiliary add in the pot body (9) then, open cross over valve (4) and circulation motor (1), allow feed liquid between pot body (9) and recycle pump (2), circulate, it is more abundant that feed liquid is mixed, essence and propylene glycol circulating reaction 20～30 minutes;
(5) detect discharging: detect every sampling in five minutes, after product index reached respective standard, regulating cross over valve (4) was the discharging state, emits the reaction feed liquid, and cooling gets product.
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| Application Number | Priority Date | Filing Date | Title |
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| CN2009100273421A CN101580756B (en) | 2009-05-31 | 2009-05-31 | Process for preparing micro emulsifying essence |
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| CN2009100273421A CN101580756B (en) | 2009-05-31 | 2009-05-31 | Process for preparing micro emulsifying essence |
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| CN101580756A CN101580756A (en) | 2009-11-18 |
| CN101580756B true CN101580756B (en) | 2011-09-14 |
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Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106962879A (en) * | 2017-05-27 | 2017-07-21 | 徐学 | A kind of emulsified transparent essence and preparation method |
| CN111084405B (en) * | 2020-02-19 | 2022-05-10 | 太湖集友广誉科技有限公司 | Reconstituted tobacco sheet and preparation method thereof |
| CN115322830A (en) * | 2022-08-10 | 2022-11-11 | 东莞市中豪优美实业有限公司 | Micro-emulsified essence and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1994540A (en) * | 2006-11-15 | 2007-07-11 | 陈罘杲 | A novel liquid circulated stirring device |
| CN101002827A (en) * | 2006-12-15 | 2007-07-25 | 江南大学 | Micro-emulsion of mint oil with slow-releasing property, and its preparing method |
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2009
- 2009-05-31 CN CN2009100273421A patent/CN101580756B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1994540A (en) * | 2006-11-15 | 2007-07-11 | 陈罘杲 | A novel liquid circulated stirring device |
| CN101002827A (en) * | 2006-12-15 | 2007-07-25 | 江南大学 | Micro-emulsion of mint oil with slow-releasing property, and its preparing method |
Non-Patent Citations (2)
| Title |
|---|
| JP特开2007-29848A 2007.02.08 |
| 张淑玲等.复合乳化剂在乳化香精中的应用.《香料香精化妆品》.2004,(第6期),43-46. * |
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Owner name: YINGTAN HUABAO FLAVORS AND FRAGRANCES CO., LTD. Free format text: FORMER OWNER: WUXI FUHUA FLAVOR + FRAGRANCE CO., LTD. Effective date: 20140905 |
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Free format text: CORRECT: ADDRESS; FROM: 214112 WUXI, JIANGSU PROVINCE TO: 335200 YINGTAN, JIANGXI PROVINCE |
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Effective date of registration: 20140905 Address after: 335200 Yingtan Economic Development Zone, Jiangxi Province, Longgang area south of the Eagle Road, Yingtan fragrance fragrance Co., Ltd. Patentee after: Yingtan Huabao Flavours & Fragrances Co., Ltd. Address before: The new plum village in Jiangsu province 214112 Wuxi Xindu Road No. 17 room -2B Patentee before: Wuxi Fuhua Flavor & Fragrance Co., Ltd. |
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Address after: 335000 Yingtan economic and Technological Development Zone, Longgang District, South Wing Road, Jiangxi Patentee after: Yingtan Huabao flavors Co. Address before: 335200 Yingtan Economic Development Zone, Jiangxi Province, Longgang area south of the Eagle Road, Yingtan fragrance fragrance Co., Ltd. Patentee before: Yingtan Huabao Flavours & Fragrances Co., Ltd. |