CN101560350A - Water-base adhesion force enhancing primer for ultraviolet light polymerization and production method thereof - Google Patents
Water-base adhesion force enhancing primer for ultraviolet light polymerization and production method thereof Download PDFInfo
- Publication number
- CN101560350A CN101560350A CNA2008100363052A CN200810036305A CN101560350A CN 101560350 A CN101560350 A CN 101560350A CN A2008100363052 A CNA2008100363052 A CN A2008100363052A CN 200810036305 A CN200810036305 A CN 200810036305A CN 101560350 A CN101560350 A CN 101560350A
- Authority
- CN
- China
- Prior art keywords
- water
- ultraviolet light
- light polymerization
- sticking power
- priming paint
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000006116 polymerization reaction Methods 0.000 title claims abstract description 20
- 238000004519 manufacturing process Methods 0.000 title abstract description 8
- 230000002708 enhancing effect Effects 0.000 title abstract 3
- 239000011347 resin Substances 0.000 claims abstract description 26
- 229920005989 resin Polymers 0.000 claims abstract description 26
- 239000000463 material Substances 0.000 claims abstract description 25
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 24
- -1 acrylic ester Chemical class 0.000 claims abstract description 10
- 230000001476 alcoholic effect Effects 0.000 claims abstract description 8
- 239000002904 solvent Substances 0.000 claims abstract description 8
- 229920001577 copolymer Polymers 0.000 claims abstract description 5
- 239000012948 isocyanate Substances 0.000 claims abstract description 4
- 229920000728 polyester Polymers 0.000 claims abstract description 4
- 229920002635 polyurethane Polymers 0.000 claims abstract description 3
- 239000004814 polyurethane Substances 0.000 claims abstract description 3
- 239000002562 thickening agent Substances 0.000 claims abstract description 3
- 239000003973 paint Substances 0.000 claims description 18
- 230000037452 priming Effects 0.000 claims description 18
- 239000013530 defoamer Substances 0.000 claims description 10
- 230000008719 thickening Effects 0.000 claims description 10
- 239000003795 chemical substances by application Substances 0.000 claims description 9
- 239000000080 wetting agent Substances 0.000 claims description 9
- 230000003750 conditioning effect Effects 0.000 claims description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 7
- 238000003756 stirring Methods 0.000 claims description 7
- CBTVGIZVANVGBH-UHFFFAOYSA-N aminomethyl propanol Chemical group CC(C)(N)CO CBTVGIZVANVGBH-UHFFFAOYSA-N 0.000 claims description 6
- 230000000855 fungicidal effect Effects 0.000 claims description 6
- 239000003755 preservative agent Substances 0.000 claims description 6
- 230000002335 preservative effect Effects 0.000 claims description 6
- 239000004721 Polyphenylene oxide Substances 0.000 claims description 5
- 229920000570 polyether Polymers 0.000 claims description 5
- 239000000839 emulsion Substances 0.000 claims description 4
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims description 3
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 3
- 239000006185 dispersion Substances 0.000 claims description 3
- ZXEKIIBDNHEJCQ-UHFFFAOYSA-N isobutanol Chemical compound CC(C)CO ZXEKIIBDNHEJCQ-UHFFFAOYSA-N 0.000 claims description 3
- 229940058020 2-amino-2-methyl-1-propanol Drugs 0.000 claims description 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 2
- 238000013019 agitation Methods 0.000 claims description 2
- 238000007334 copolymerization reaction Methods 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 claims description 2
- 239000011248 coating agent Substances 0.000 abstract description 11
- 238000000576 coating method Methods 0.000 abstract description 11
- 230000007613 environmental effect Effects 0.000 abstract description 2
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 abstract 2
- 239000004816 latex Substances 0.000 abstract 1
- 229920000126 latex Polymers 0.000 abstract 1
- 238000000034 method Methods 0.000 description 8
- 238000007761 roller coating Methods 0.000 description 5
- 238000010276 construction Methods 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 239000002245 particle Substances 0.000 description 3
- 241000237502 Ostreidae Species 0.000 description 2
- 239000012467 final product Substances 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 235000020636 oyster Nutrition 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 238000009736 wetting Methods 0.000 description 2
- CFKMVGJGLGKFKI-UHFFFAOYSA-N 4-chloro-m-cresol Chemical compound CC1=CC(O)=CC=C1Cl CFKMVGJGLGKFKI-UHFFFAOYSA-N 0.000 description 1
- JOYRKODLDBILNP-UHFFFAOYSA-N Ethyl urethane Chemical compound CCOC(N)=O JOYRKODLDBILNP-UHFFFAOYSA-N 0.000 description 1
- 244000137852 Petrea volubilis Species 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- MGIYRDNGCNKGJU-UHFFFAOYSA-N isothiazolinone Chemical compound O=C1C=CSN1 MGIYRDNGCNKGJU-UHFFFAOYSA-N 0.000 description 1
- 239000004922 lacquer Substances 0.000 description 1
- 239000010985 leather Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 125000002347 octyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 238000000016 photochemical curing Methods 0.000 description 1
- 238000003847 radiation curing Methods 0.000 description 1
- 238000007790 scraping Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Abstract
The invention provides a water-base adhesion force enhancing primer for ultraviolet light polymerization and a production method thereof. The primer comprises the following components by the weight percent: 55-56 of water-base resin A, 35-40 of water-base resin B, 2-5 of alcoholic solvent, 1-2 of water and 0.1-0.3 of thickening agent, wherein the water-base resin A is a copolymer of styrene and acrylic ester; and the water-base resin B is a polyurethane latex or a dispersoid of polyester acrylic ester and aliphatic isocyanate. The water-base adhesion force enhancing primer for ultraviolet light polymerization has the advantages of environmental protection and less smell, can be directly diluted by water, can greatly improve the adhesion force of an ultraviolet light polymerization coating and a base material and has lower cost.
Description
Technical field
The present invention relates to a kind of water-based sticking power and strengthen priming paint, refer in particular to a kind of aqueous priming paint and production method thereof of improving sticking power between harder sheet material of quality and ultraviolet curable coating when being used for ultraviolet light polymerization (UV) application.
Background technology
Ultraviolet light polymerization (UV) is coated with to be contained in and has obtained development faster in recent years, especially in dull and stereotyped furniture and timber floor production, owing to its hardness height, repainting hours weak point, production efficiency advantages of higher develop rapidly.But in UV application production process, the sticking power problem becomes a resistance of its fast development, particularly when the roller coating of timber floor is produced, owing to timber floor is very hard with the general quality of timber, the timber kapillary is less, some timber has reasons such as grease, make its sticking power when the UV application relatively poor, as draw 2 * 2mm lattice with blade, but white spotted finiss when scraping resitant coatings with blade big area release coating or with coin then (coating disengaging timber), this problem hamper the widespread use of UV lacquer in the application of floor for a long time always.Do more existing reports in aspect such as hide finishes at employing aqueous photo-curing resin, the patent No. of announcing as on February 25th, 2004 is the photo curable aqueous coating agent of CN1477168A, a kind of exactly oil polish finishing agent that is used for timber, leather, paper, its during to woodwork coating sticking power do not have remarkable improvement.
Summary of the invention
The purpose of this invention is to provide a kind of water-based sticking power that is used for ultraviolet light polymerization and strengthen priming paint and production method thereof, to overcome the above-mentioned defective that prior art exists.
The said water-based sticking power that is used for ultraviolet light polymerization of the present invention strengthens priming paint, comprises following components in weight percentage:
Water-base resin A 55%～60%;
Water-base resin B 35%～40%
Alcoholic solvent 2%～5%;
Water 1%～2%
Thickening material 0.1%～0.3%
Said water-base resin A is a copolymer in cinnamic acrylic ester, and technical requirements is: weight contains 30～32% admittedly, pH value 7～9, and particle diameter≤0.5um can adopt the UCAR of U.S. UCAR company
TMR-64;
Emulsion or dispersion that said water-base resin B is the water-based radiation curing, it mainly acts on is the sticking power that improves between workability and aqueous coating and solvent-borne type ultraviolet curable coating, its main component is the polyaminoester emulsion or the dispersion of polyester type acrylate and aliphatic isocyanates, can adopt the UV LS2348 as BAYER company;
Said alcoholic solvent is the monohydroxy-alcohol of C2～C3, more than one in preferred alcohol, Virahol or the isopropylcarbinol;
Said thickening material is one or both in the association type polyurethane thickener, and its chemical composition is roughly association type urethane, can adopt the PUR40 of German bright icepro company;
Preferably, also comprise the defoamer of gross weight 0.1%～0.2%, the preferred polysiloxane-polyether copolymer of defoamer, the trade mark that can adopt TEGO company is the product of TEGO810;
Preferably, also comprise the base material wetting agent of gross weight 0.1%～0.2%, the preferred polysiloxane-polyether copolymerization of base material wetting agent, the trade mark that can adopt TEGO company is the product of TEGO270;
Said defoamer and base material wetting agent are polysiloxane-polyether copolymer, and still, difference wherein is that the former wetting ability is poor, and latter's wetting ability will be got well.
Preferred according to the present invention, also comprise the pH value conditioning agent of gross weight 0.1%～0.2%, pH value conditioning agent is a 2-amino-2-methyl-1-propanol, the trade mark of preferred U.S. Mykrolis Corp is the product of AMP-95.
Preferred according to the present invention, also comprise the fungicidal preservative of gross weight 0.1%～0.2%, major ingredient is the octyl group isothiazolinone, as the PARMETOL N20 of German Shu Mei company.
Making method of the present invention comprises the steps:
(1) at first water-base resin A and water-base resin B are mixed, under agitation add defoamer and alcoholic solvent, dispersed with stirring then;
(2) add thickening material, base material wetting agent, fungicidal preservative, pH value conditioning agent and water then, dispersed with stirring adds the thickening material adjustment and promptly obtains product for viscosity to 75～85KU/25 ℃.
Using method of the present invention can be wiping, also can be roller coating.
Use when of the present invention, note following item:
1. must select for use suitable sand paper to the sheet material sanded before the construction, to obtain fine and smooth surface.
2. this aqueous priming paint must be fully dry, just can carry out the next procedure construction, otherwise the not good problem of sticking power also can occur.When adopting the construction of wiping method, generally under 25 ℃, 75% humidity, can carry out the construction of next procedure in 3 hours, at low temperature below 10 ℃ and under high humidity such as the condition of relative humidity more than 75%, but proper extension time of drying; During the ultraviolet light polymerization roller coating, can suitably adjust temperature of oven and storing time.
The water-based sticking power that is used for ultraviolet light polymerization of the present invention strengthens priming paint, and following advantage is arranged: environmental protection, and very little flavor, direct dilute with water can improve the sticking power of ultraviolet curable coating and base material greatly, and cost is lower.
Embodiment
Embodiment 1
Raw-material weight per-cent is as follows:
Water-base resin A 60%
Water-base resin B 35%
Ethanol 3.0%
Water 1.2%
Thickening material PUR40 0.3%
Base material wetting agent TEGO270 0.2%
Defoamer TEGO810 0.1%
PH value conditioning agent AMP-95 0.1%
Fungicidal preservative K-20 0.1%
100％
Water-base resin A is a copolymer in cinnamic acrylic ester, and weight contains 30% admittedly, pH value 7, particle diameter≤0.5um;
Water-base resin B is the polyaminoester emulsion of polyester type acrylate and aliphatic isocyanates;
Concrete making processes is: (1) adds in the cylinder dispersed with stirring with water-base resin A and water-base resin B; (2) will add behind defoamer TEGO810 and the ethanol mixing, dispersed with stirring, and add PUR40, disperseed 5 minutes; (3) adding successively, TEGO270, AMP-95 and K-20 then, dispersed with stirring 5 minutes adds PUR40 and adjusts viscosity and get final product to 75KU/ ℃.
Detected result is as follows:
Solid content: 32% GB/T 1725-79 (second method)
Outward appearance: oyster white semi-fluid GB 1727-79
The sticking power of UV coating and base material behind this priming paint of roller coating :≤1 grade.
Embodiment 2
Raw-material weight per-cent is as follows:
Water-base resin A 55%
Water-base resin B 39%
The mixture of Virahol and isopropylcarbinol (1: 1, weight ratio) 4.2%
Water 1.0%
Thickening material PUR40 0.1%
Base material wetting agent TEGO270 0.1%
Defoamer TEGO810 0.2%
PH value conditioning agent AMP-95 0.2%
Fungicidal preservative K-20 0.2%
100％。
Water-base resin A is a copolymer in cinnamic acrylic ester, and weight contains 31% admittedly, pH value 9, particle diameter≤0.5um.
The preparation method is with embodiment 1, adjusts viscosity and gets final product to 85KU/ ℃.
Detected result is as follows:
Solid content: 33% GB/T 1725-79 (second method)
Outward appearance: oyster white semi-fluid GB 1727-79
The sticking power of UV coating and base material behind this priming paint of roller coating :≤1 grade.
Claims (9)
1. the water-based sticking power that is used for ultraviolet light polymerization strengthens priming paint, it is characterized in that, comprises following components in weight percentage:
Water-base resin A 55%～60%;
Water-base resin B 35%～40%
Alcoholic solvent 2%～5%;
Water 1%～2%
Thickening material 0.1%～0.3%;
Said water-base resin A is a copolymer in cinnamic acrylic ester;
Polyaminoester emulsion or dispersion that said water-base resin B is polyester type acrylate and aliphatic isocyanates.
2. the water-based sticking power that is used for ultraviolet light polymerization according to claim 1 strengthens priming paint, it is characterized in that said alcoholic solvent is the monohydroxy-alcohol of C2～C3.
3. the water-based sticking power that is used for ultraviolet light polymerization according to claim 2 strengthens priming paint, it is characterized in that said alcoholic solvent is more than one in ethanol, Virahol or the isopropylcarbinol.
4. the water-based sticking power that is used for ultraviolet light polymerization according to claim 1 strengthens priming paint, it is characterized in that said thickening material is one or both in the association type polyurethane thickener.
5. strengthen priming paint according to each described water-based sticking power that is used for ultraviolet light polymerization of claim 1～4, it is characterized in that also comprise the defoamer of gross weight 0.1%～0.2%, defoamer is that the trade mark is the polysiloxane-polyether copolymer of TEGO810.
6. strengthen priming paint according to each described water-based sticking power that is used for ultraviolet light polymerization of claim 1～4, it is characterized in that also comprise the base material wetting agent of gross weight 0.1%～0.2%, the base material wetting agent is that the trade mark is the polysiloxane-polyether copolymerization of TEGO270.
7. strengthen priming paint according to each described water-based sticking power that is used for ultraviolet light polymerization of claim 1～4, it is characterized in that also comprise the pH value conditioning agent of gross weight 0.1%～0.2%, pH value conditioning agent is a 2-amino-2-methyl-1-propanol.
8. strengthen priming paint according to each described water-based sticking power that is used for ultraviolet light polymerization of claim 1～4, it is characterized in that, also comprise the fungicidal preservative of gross weight 0.1%～0.2%.
9. strengthen the preparation method of priming paint according to each described water-based sticking power that is used for ultraviolet light polymerization of claim 1～8, it is characterized in that, comprise the steps:
(1) at first water-base resin A and water-base resin B are mixed, under agitation add defoamer and alcoholic solvent, dispersed with stirring then;
(2) add thickening material, base material wetting agent, fungicidal preservative, pH value conditioning agent and water then, dispersed with stirring adds the thickening material adjustment and promptly obtains product for viscosity to 75～85KU/25 ℃.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200810036305 CN101560350B (en) | 2008-04-18 | 2008-04-18 | Water-base adhesion force enhancing primer for ultraviolet light curing and production method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200810036305 CN101560350B (en) | 2008-04-18 | 2008-04-18 | Water-base adhesion force enhancing primer for ultraviolet light curing and production method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101560350A true CN101560350A (en) | 2009-10-21 |
| CN101560350B CN101560350B (en) | 2012-09-05 |
Family
ID=41219341
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200810036305 Active CN101560350B (en) | 2008-04-18 | 2008-04-18 | Water-base adhesion force enhancing primer for ultraviolet light curing and production method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101560350B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102888161A (en) * | 2012-10-23 | 2013-01-23 | 上海维凯化学品有限公司 | Environment-friendly water-based high-adhesion PET (polyethylene terephthalate) precoat coating composition as well as preparation method and application |
| CN107532843A (en) * | 2015-05-11 | 2018-01-02 | 松下知识产权经营株式会社 | Home appliance |
| CN109278368A (en) * | 2018-07-20 | 2019-01-29 | 无锡和烁丰新材料有限公司 | A kind of structure and its production technology of the blank synthetic paper of two-sided writing |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AU528378B2 (en) * | 1978-09-13 | 1983-04-28 | Rock, J.D. And Garnett, J.L. | Radiation cured coating for leather |
| CN1208402C (en) * | 2001-07-13 | 2005-06-29 | 大连路明发光科技股份有限公司 | Luminous water paint and its preparing process |
| CN100448939C (en) * | 2004-12-20 | 2009-01-07 | 比亚迪股份有限公司 | Coating material solidified by ultraviolet light and prepartion method |
-
2008
- 2008-04-18 CN CN 200810036305 patent/CN101560350B/en active Active
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102888161A (en) * | 2012-10-23 | 2013-01-23 | 上海维凯化学品有限公司 | Environment-friendly water-based high-adhesion PET (polyethylene terephthalate) precoat coating composition as well as preparation method and application |
| CN102888161B (en) * | 2012-10-23 | 2016-08-03 | 上海维凯光电新材料有限公司 | Environment-friendly water-based high adhesion force PET precoated shet coating composition and preparation, purposes |
| CN107532843A (en) * | 2015-05-11 | 2018-01-02 | 松下知识产权经营株式会社 | Home appliance |
| CN109278368A (en) * | 2018-07-20 | 2019-01-29 | 无锡和烁丰新材料有限公司 | A kind of structure and its production technology of the blank synthetic paper of two-sided writing |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101560350B (en) | 2012-09-05 |
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| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C56 | Change in the name or address of the patentee |
Owner name: SHANGHAI ZHANCHEN PAINT CO., LTD. Free format text: FORMER NAME: SHANGHAI FUCHEN CHEMICAL CO. LTD. |
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| CP03 | Change of name, title or address |
Address after: 8555 No. 201700 Shanghai city Qingpu District Songze Avenue Patentee after: SHANGHAI ZHANCHEN PAINT Co.,Ltd. Patentee after: ZHANCHEN PAINT GROUP Co.,Ltd. Patentee after: Beijing Zhanchen Chemical Co.,Ltd. Address before: 201700 Shanghai City Industrial Park, No. 8555 Qingpu Songze Avenue Patentee before: Shanghai Vision Chemical Co.,Ltd. Patentee before: ZHANCHEN PAINT GROUP Co.,Ltd. Patentee before: Beijing Zhanchen Chemical Co.,Ltd. |
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| CP01 | Change in the name or title of a patent holder |
Address after: 8555 No. 201700 Shanghai city Qingpu District Songze Avenue Patentee after: SHANGHAI ZHANCHEN PAINT Co.,Ltd. Patentee after: China Zhanchen New Materials Group Co.,Ltd. Patentee after: BEIJING ZHANCHEN NEW MATERIAL Co.,Ltd. Address before: 8555 No. 201700 Shanghai city Qingpu District Songze Avenue Patentee before: SHANGHAI ZHANCHEN PAINT Co.,Ltd. Patentee before: ZHANCHEN PAINT GROUP Co.,Ltd. Patentee before: Beijing Zhanchen Chemical Co.,Ltd. |
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| CP01 | Change in the name or title of a patent holder |
Address after: 8555 No. 201700 Shanghai city Qingpu District Songze Avenue Co-patentee after: China Zhanchen New Materials Group Co.,Ltd. Patentee after: SHANGHAI ZHANCHEN PAINT Co.,Ltd. Co-patentee after: Beijing zhanchen Intelligent Property Management Co.,Ltd. Address before: 8555 No. 201700 Shanghai city Qingpu District Songze Avenue Co-patentee before: China Zhanchen New Materials Group Co.,Ltd. Patentee before: SHANGHAI ZHANCHEN PAINT Co.,Ltd. Co-patentee before: BEIJING ZHANCHEN NEW MATERIAL Co.,Ltd. |
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Effective date of registration: 20200706 Address after: 8555 No. 201700 Shanghai city Qingpu District Songze Avenue Co-patentee after: Zhuhai zhanchen New Material Co.,Ltd. Patentee after: SHANGHAI ZHANCHEN PAINT Co.,Ltd. Address before: 8555 No. 201700 Shanghai city Qingpu District Songze Avenue Co-patentee before: China Zhanchen New Materials Group Co.,Ltd. Patentee before: SHANGHAI ZHANCHEN PAINT Co.,Ltd. Co-patentee before: Beijing zhanchen Intelligent Property Management Co.,Ltd. |