CN101559943B - Graphite purifying device - Google Patents
Graphite purifying device Download PDFInfo
- Publication number
- CN101559943B CN101559943B CN2009100430954A CN200910043095A CN101559943B CN 101559943 B CN101559943 B CN 101559943B CN 2009100430954 A CN2009100430954 A CN 2009100430954A CN 200910043095 A CN200910043095 A CN 200910043095A CN 101559943 B CN101559943 B CN 101559943B
- Authority
- CN
- China
- Prior art keywords
- charging basket
- links
- treatment solution
- pipe
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Images
Landscapes
- Carbon And Carbon Compounds (AREA)
Abstract
The invention relates to a graphite purifying device which is characterized by comprising a charging basket (5), a reaction barrel (6), a wash bucket (7) and a dewatering machine (10) that are sequentially connected with each other; wherein, the charging basket (5), the reaction barrel (6) and the wash bucket (7) are internally provided with stirring machines (4); the top of the charging basket (5) is provided with a raw material feeding pipe (3), a treating liquid inlet and a waste gas outlet (2), a discharge hole of the charging basket (5) is connected with a feeding hole of the reaction barrel (6), and a treating liquid feeding pipe (1) is connected with the charging basket (5) through the treating liquid inlet; a discharge hole of the reaction barrel (6) is connected with a feeding hole of the wash bucket (7), and a liquid outlet of the reaction barrel (6) is connected with a treating liquid recycling bin (11); a discharge hole of the wash bucket (7) is connected with a feeding hole of the dewatering machine (10), the wash bucket (7) is provided with a clear water inlet and waste water discharge hole, and the dewatering machine (10) is connected with a discharge pipe through the discharge hole. The device has the advantages of simple structure, less equipment failure, corrosion prevention, ideal processing effect and little environmental pollution.
Description
Technical field
The present invention relates to a kind of graphite purifying device.
Background technology
The purified graphite of occurring in nature does not have, and wherein often contains SiO
2, Al
2O
3, FeO, CaO, P
2O
5, impurity such as CuO.These impurity often occur with mineral forms such as quartz, pyrite, carbonate.In addition, also have water, CO
2, H
2, CH
4, N
2Deng gaseous impurities.Graphite must carry out purification processes when carrying out industrial application.The at present domestic chemical equipment for purifying of graphite satisfactory for result of also not finding.
Summary of the invention
The object of the present invention is to provide a kind of simple in structure, less investment, running cost graphite purifying device low, satisfactory for result.
To achieve these goals, technical scheme of the present invention is following design:
A kind of graphite purifying device comprises banded charging basket, reaction container, cleaning barrels and water extracter successively, and stirrer all is installed in charging basket, reaction container and the cleaning barrels; The top of charging basket is equipped with raw material and goes into pipe, treatment solution inlet and waste gas outlet, and the discharge port of charging basket links to each other with the opening for feed of reaction container, and treatment solution is gone into pipe and linked to each other with charging basket by the treatment solution inlet; The discharge port of reaction container links to each other with the opening for feed of cleaning barrels, and the liquid outlet of reaction container links to each other with the treatment solution recycling bin; The discharge port of cleaning barrels links to each other with the opening for feed of water extracter, and clear water inlet and waste water discharge opening are installed on the cleaning barrels, and water extracter links to each other with discharge nozzle by discharge port.
Described graphite purifying device, the discharge nozzle of treatment solution recycling bin goes into pipe and connects with charging basket to link to each other with the treatment solution of charging basket.
Described graphite purifying device, the waste water discharge opening of cleaning barrels links to each other with the water-in of waste water treater, the rising pipe of waste water treater and clear water pipe and connect after, link to each other with the clear water of cleaning barrels inlet again.
Described graphite purifying device, water extracter are centrifuge.
Described graphite purifying device, the wadding that position that whole device contacts with material or components and parts are made or had poly-third vinyl material to make by poly-third vinyl material.
Useful benefit of the present invention is as follows:
1, facility investment is few, and is simple in structure, do not have the parts that run up, and running cost is cheap, and equipment failure is few.Be poly-third vinyl material of erosion resistance with the contacted position of graphite material in the device, can effectively prevent the corrosives etching mechanism equipment that produces in material, the reaction process.
2, ideal processing effect is surveyed factually, and the graphite of content 70% just ore deposit can obtain the smart graphite of precision more than 95% after this device is handled, improve the value of product greatly.
3, the useless treatment solution that produces in the production process, waste water etc. all pass through recovery, and recycling had both helped reducing environmental pollution, helped again reducing production costs.
Description of drawings
Fig. 1 is the structural representation of graphite purifying device,
Fig. 2 is the frame principle figure of graphite purifying device.
Wherein, description of reference numerals is as follows:
1, treatment solution is gone into pipe 2, waste gas outlet 3, raw material and is gone into pipe 4, stirrer
5, charging basket 6, reaction container 7, cleaning barrels 8, rising pipe
9, waste water treater 10, water extracter 11, treatment solution recycling bin 12, discharge nozzle
13, clear water pipe
Embodiment
A kind of graphite purifying device, its structure as shown in Figure 1.Comprise banded charging basket 5, reaction container 6, cleaning barrels 7 and water extracter 10 successively.In charging basket 5, reaction container 6 and the cleaning barrels 7 stirrer 4 is installed all.The top of charging basket 5 is equipped with raw material and goes into pipe 3, treatment solution inlet and waste gas outlet 2, and the discharge port of charging basket 5 links to each other with the opening for feed of reaction container 6, and treatment solution is gone into pipe 1 and linked to each other with charging basket 5 by the treatment solution inlet.The discharge port of reaction container 6 links to each other with the opening for feed of cleaning barrels 7, and the liquid outlet of reaction container 6 links to each other with treatment solution recycling bin 11.The discharge port of cleaning barrels 7 links to each other with the opening for feed of water extracter 10, and clear water inlet and waste water discharge opening are installed on the cleaning barrels 7, and water extracter 10 links to each other with discharge nozzle by discharge port.The discharge nozzle 12 of treatment solution recycling bin 11 goes into pipe 1 and connects with charging basket 5 to link to each other with the treatment solution of charging basket 5.The waste water discharge opening of cleaning barrels 7 links to each other with the water-in of waste water treater 9, and the rising pipe 8 of waste water treater 9 is with clear water pipe 13 and after connecing, and the water-in with cleaning barrels 7 links to each other again.Water extracter 10 is a centrifuge.The wadding that position that whole device contacts with material or components and parts are made or had poly-third vinyl material to make by poly-third vinyl material.
According to Fig. 2, graphite purifying device of the present invention, the natural micro crystal graphite that is used to purify, purification process is as follows:
1, natural micro crystal graphite raw material and treatment solution are inserted in the charging basket 5, start stirrer 4, treatment solution and graphite are mixed, the gas that treatment solution and graphite impurities reaction generate is discharged through waste gas outlet 2.
2, the material that mixes is transferred to reaction container 6, makes impurity and the abundant stirring reaction under 60-80 ℃ of condition of the chemical substance in the treatment solution in the graphite.Treatment solution enters in the treatment solution recycling bin 11, and material is transferred in the cleaning barrels 7.If the active chemical that contains in the treatment solution reaches requirement, can recycling.
3, shift material abundant stirring and washing in cleaning barrels 7 of coming from reaction container 6, impurity is fully separated with graphite, impure waste water enters in the waste water treater 9, and pure graphite enters water extracter 10.Behind the treated removal impurity of waste water, can recycling.
4, the graphite that contains certain moisture carries out centrifugation in water extracter 10, and after the removal most of moisture, graphite is drying again, obtains the pure graphite of finished product.
Claims (5)
1. a graphite purifying device is characterized in that: comprise banded charging basket (5), reaction container (6), cleaning barrels (7) and water extracter (10) successively, in charging basket (5), reaction container (6) and the cleaning barrels (7) stirrer (4) is installed all; The top of charging basket (5) is equipped with raw material and goes into pipe (3), treatment solution inlet and waste gas outlet (2), the discharge port of charging basket (5) links to each other with the opening for feed of reaction container (6), treatment solution is gone into pipe (1) and linked to each other with charging basket (5) by the treatment solution inlet: the discharge port of reaction container (6) links to each other with the opening for feed of cleaning barrels (7), and the liquid outlet of reaction container (6) links to each other with treatment solution recycling bin (11); The discharge port of cleaning barrels (7) links to each other with the opening for feed of water extracter (10), and clear water inlet and waste water discharge opening are installed on the cleaning barrels (7), and water extracter (10) links to each other with discharge nozzle by discharge port.
2. graphite purifying device according to claim 1 is characterized in that: the discharge nozzle (12) of treatment solution recycling bin (11) goes into pipe (1) and connects with charging basket (5) to link to each other with the treatment solution of charging basket (5).
3. graphite purifying device according to claim 1, it is characterized in that: the waste water discharge opening of cleaning barrels (7) links to each other with the water-in of waste water treater (9), the rising pipe (8) of waste water treater (9) links to each other with the clear water inlet of cleaning barrels (7) with clear water pipe (13) and after connecing again.
4. graphite purifying device according to claim 1 is characterized in that: water extracter (10) is a centrifuge.
5. graphite purifying device according to claim 1 is characterized in that: the wadding that position that whole device contacts with material or components and parts are made or had poly-third vinyl material to make by poly-third vinyl material.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009100430954A CN101559943B (en) | 2009-04-10 | 2009-04-10 | Graphite purifying device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009100430954A CN101559943B (en) | 2009-04-10 | 2009-04-10 | Graphite purifying device |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101559943A CN101559943A (en) | 2009-10-21 |
| CN101559943B true CN101559943B (en) | 2011-02-16 |
Family
ID=41218949
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2009100430954A Expired - Fee Related CN101559943B (en) | 2009-04-10 | 2009-04-10 | Graphite purifying device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101559943B (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1051154A (en) * | 1990-11-05 | 1991-05-08 | 鞍山市精制石墨厂 | The method of making refined grahite with dilute alkaline solution |
| US20060062716A1 (en) * | 2002-03-01 | 2006-03-23 | Hydro-Quebec | Method for the surface purification of a graphite containing impurities using a dilute aqueous solution of nh4f and h2so4 |
| CN101367517A (en) * | 2008-09-24 | 2009-02-18 | 青岛恒胜石墨有限公司 | Method for preparing high pure graphite with steam heating |
-
2009
- 2009-04-10 CN CN2009100430954A patent/CN101559943B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1051154A (en) * | 1990-11-05 | 1991-05-08 | 鞍山市精制石墨厂 | The method of making refined grahite with dilute alkaline solution |
| US20060062716A1 (en) * | 2002-03-01 | 2006-03-23 | Hydro-Quebec | Method for the surface purification of a graphite containing impurities using a dilute aqueous solution of nh4f and h2so4 |
| CN101367517A (en) * | 2008-09-24 | 2009-02-18 | 青岛恒胜石墨有限公司 | Method for preparing high pure graphite with steam heating |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101559943A (en) | 2009-10-21 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104003554B (en) | A kind of spent acid refining plant and technique | |
| CN105274359B (en) | Method for extracting and separating valuable metals from secondary lead smelting slag | |
| US20120298562A1 (en) | Ash processing and metals recovery systems and methods | |
| CN112047547A (en) | Continuous washing energy-saving treatment device and process for waste incineration fly ash or fly ash after hydrochloric acid washing | |
| CN109264898A (en) | A kind of flying dust multistage dechlorination and water lotion decalcification softening process and its system | |
| CN203333413U (en) | System for comprehensively utilizing wastewater generated during production of polyvinyl chloride (PVC) production by calcium carbide method | |
| CN213887551U (en) | Continuous washing energy-saving treatment device for waste incineration fly ash or fly ash after hydrochloric acid washing | |
| CN101559943B (en) | Graphite purifying device | |
| CN201313874Y (en) | Waste acrylic acid and acrylic ester recovery device | |
| CN102153127B (en) | Method for preparing gypsum by removing sulfate radicals from mineral salts with waste distillation liquid from ammonia alkali factory | |
| CN104003910A (en) | Method for extracting m-phthalic acid-5-sodium sulfonate from ternary-monomer industrial waste water | |
| CN115155279B (en) | Flue gas deacidification coupling fly ash treatment method | |
| CN106430713A (en) | Wet desulphurization wastewater zero-discharge treatment device | |
| CN113860315B (en) | Method for purifying waste obtained by extracting copper from organic silicon waste residue slurry | |
| CN209721798U (en) | A kind of device recycling magnesium in high magnesium desulfurization wastewater | |
| CN211098293U (en) | Equipment of wet process deacidification | |
| CN112125439A (en) | System for removing fluorine ions in wastewater for coal gas production | |
| CN112875784A (en) | Process water resource utilization process for membrane coal gasifier | |
| CN105600979A (en) | Method and apparatus for pretreatment of chlorinated resin polymerization mother liquor | |
| CN112624283A (en) | Method for preparing water purifying agent by using dust-collecting slag | |
| CN216397501U (en) | Miscellaneous salt processing apparatus | |
| KR20080064516A (en) | Removal method and system for copper | |
| CN110790440A (en) | High COD high salt effluent disposal system | |
| CN109179756A (en) | A kind for the treatment of process purifying SS from hydrometallurgy cobalt copper solution | |
| CN215102439U (en) | Sulfuric acid production wastewater treatment system |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20110216 Termination date: 20150410 |
|
| EXPY | Termination of patent right or utility model |