CN101491243A - 室内空气病毒致病菌克星的制备方法 - Google Patents
室内空气病毒致病菌克星的制备方法 Download PDFInfo
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Abstract
公开一种室内空气病毒致病菌克星的制备方法，由薄荷醇、百里香酚、连翘油、柴胡油制成的室内空气病毒致病菌克星，对流脑、流感病毒、手足口病、禽流感、军团菌、肺炎菌、丙型肝炎病毒、甲型肝炎病毒、白色葡萄球菌、金黄色葡萄球菌、肺炎克雷伯、白色念珠菌、伤寒病毒、大肠杆菌、霍乱病毒、传染病菌病毒、有害细菌病毒杀灭率达76－99.％。主要应用于居室、学校、医院、宾馆、空调、汽车、公共场所等防治流感、上呼吸道感染等病症具有明显的效果。该品具有突出的实质性特点，具有广阔的应用前景。
Description
技术领域：
本发明涉及一种杀病毒杀菌挥发性固体物消毒剂，尤其涉及一种纯植物杀菌油提取合成的自然挥发性固体物，应用于居室、学校、医院、宾馆、空调、汽车、公共场所等的室内空气病毒致病菌克星的制备方法。
背景技术：
目前，国内外空气杀菌剂种类多，但不是由纯植物杀菌油提取合成的自然挥发性固体物。有的杀菌效果好但毒性也大，不能持续性杀菌；有的晶体挥发杀菌效果好成本高，投资设备多，生产工艺复杂；有的需要发热片加热熏蒸杀菌使用不安全、没有自然升华挥发功能、不能持续性杀菌，使用不便、费用高；臭氧、氯气杀菌的同时对人体也造成了极大的伤害，而且杀菌时人必须离现场，不能持续性杀菌，还有刺激性、腐蚀性、对环境造成二次污染；有的烟雾杀菌非常麻烦不能持续性杀菌，杀菌时人必须离开现场；有的毒性相对较小但是根本没有杀菌效果或者效果不明显等技术缺点。
发明内容：
本发明的目的是为了克服上述技术不足，而提供一种纯植物杀菌油提取合成的自然挥发性固体物，能持续性杀菌杀病毒，杀菌杀病毒效果好，无毒性、无刺激性、无腐蚀性、对环境无二次污染、使用方便灵活及费用低的室内空气病毒致病菌克星的制备方法。
本发明解决其技术问题所采用的技术方案，这种室内空气病毒致病菌克星的制备方法，主要由下述重量配比的原料组合制成：薄荷醇10-40克、柏木醇10-20克、百里香酚10-40克、丁香酚10-20克、连翘油1-5克、柴胡油1-5克。
本发明所述的这种室内空气病毒致病菌克星的制备方法的生产方法，先制备原料如下：
1、薄荷醇的制备方法
含量低的薄荷醇16.3g加入50ml乙腈，加温至30℃溶解。将该溶液冷却至5℃，过滤、蒸馏析出的结晶，从而得到薄荷醇11.8g(收率72％)纯度为99.6％。
2、百里香酚的制备方法：
百里香油、40％氢氧化纳→搅拌→加热水→稀释→分层分离→酚钠水溶液→酚钠水稀盐酸酸化分解→水液分层分离→分离出粗酚→粗酚→干燥→粗酚加乙醇减压蒸馏→结晶过滤→乙醇重结晶→干燥→百里香酚。
3、柏木醇制备方法：
柏木油→减压蒸馏→粗脑→乙醇重结晶→柏木醇。
本发明所述的这种室内空气病毒致病菌克星的制备方法的生产方法，其特征是薄荷醇40克、柏木醇20克、百里香酚40克合并于一体→加热熔解→冷却结晶→结晶料粉碎→粉碎料中加入丁香酚20克、连翘油5克、柴胡油5克加热熔解→熔解后充分搅拌混合→溶解液流入聚丙烯塑料盒→冷却结晶→成品室内空气病毒致病菌克星。
室内空气病毒致病菌克星经毒理学测定，小白鼠经口LD50为6266.8毫克公斤，hMLS试验属阳性，慢性毒性实验证明没有致癌，致畸，致突变等现象，故对人畜无毒。
本发明的有益效果是：
本发明突破了纯植物杀菌油提取合成的自然挥发性杀菌固体物，对流脑、流感病毒、手足口病、禽流感、军团菌、肺炎菌、丙型肝炎病毒、甲型肝炎病毒、白色葡萄球菌、金黄色葡萄球菌、肺炎克雷伯、白色念珠菌、伤寒病毒、大肠杆菌、霍乱病毒、传染病菌病毒、有害细菌病毒杀灭率达76-99.9％的关键技术。解决了对病原微生物有明显的抑制及杀灭作用的难题。解决了应用于防治流感、上呼吸道感染等病症具有明显的效果。实现了使用时将室内空气病毒致病菌克星药盒利用电机风轮微风装置或空调风吹入室内空气病毒致病菌克星转变为升华气体1-3纳米悬浮在室内空气中达到杀灭有害病菌、病毒，预防疾病的传播和病毒交叉感染，减少患病机率，从而达到净化室内空气的目的。该品与其它室内空气杀菌产品相比，具有突出的实质性特点和显著进步，能产生积极效果和效益、具有广阔的应用前景。
具体实施方式：
下面实施例对本发明作进一步描述。
实施例1：
这种室内空气病毒致病菌克星的制备方法，主要由下述重量配比的原料组合制成：
薄荷醇40克、柏木醇20克、百里香酚40克合并于一体→加热熔解→冷却结晶→结晶料粉碎→粉碎料中加入丁香酚20克、连翘油5克、柴胡油5克加热熔解→熔解后充分搅拌混合→溶解液流入聚丙烯塑料盒→冷却结晶→成品室内空气病毒致病菌克星。
实施例2：
取实施例1所制的室内空气病毒致病菌克星2盒，放入交通车空调出风口试验结果如下；
| 室内空气病毒致病菌克星 | 空气杀菌率(30、60、100分钟) |
| 200克/盒 | 96.24％ |
| 150克/盒 | 85.56％ |
| 100克/盒 | 76.68％ |
本发明的杀菌效果实验：
1、方法：室内空气病毒致病菌克星一盒插入空调出风口，在39立方房间内，观察不同时间升华挥发杀菌效果。
结果：
对自然菌的杀灭效果，在约为39立方米室内消毒前自然菌量为1196个/立方米，空调风消毒时间为30、60、100分钟时，对自燃菌的杀菌率分别为73.89％、93.32％、98.70％。
本发明的急性毒性试验：
2、材料和方法
测试样品：样品为淡黄棕色固体，具有香味，易挥发。实验动物：成年小鼠，雌雄各半。
方法：参照静态染毒法。室内空气病毒致病菌克星一盒利用电机风轮微风装置挥发，小鼠置于1立方米染毒柜内，吸入室内空气病毒致病菌克星升华气体72小时，取出后观察2周，记录中毒反应。
结果与讨论：
实验染毒半小时动物出现兴奋症状，活泼好动，尔后逐渐出现抑制症状，动物安静不动，呼吸加深，嗜睡，直至染毒36小时，取出。至24小时后动物恢复如常，再继续观察3周，未发生变化。故，测得小鼠吸入室内空气病毒致病菌克星升华气体72小时的急性毒性分级标准，被测样品属于基本无毒。
Claims (2)
1、一种室内空气病毒致病菌克星的制备方法，其特征是由下述重量配比的原料组合制成：薄荷醇10-40克、柏木醇10-20克、百里香酚10-40克、丁香酚10-20克、连翘油1-5克、柴胡油1-5克。
2、根据权利要求1所述的室内空气病毒致病菌克星的制备方法，其特征是薄荷醇40克、柏木醇20克、百里香酚40克合并于一体→加热熔解→冷却结晶→结晶料粉碎→粉碎料中加入丁香酚20克、连翘油5克、柴胡油5克加热熔解→熔解后充分搅拌混合→溶解液流入聚丙烯塑料盒→冷却结晶→成品室内空气病毒致病菌克星。
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2012104571A1 (en) * | 2011-02-02 | 2012-08-09 | GILHOLM, Stephen, Philip | Compositions of monoterpenoids for the treatment of influenza |
| CN105211123A (zh) * | 2014-06-10 | 2016-01-06 | 黄安宏 | 通过空气净化器消除空气污染的中草药消毒剂的制备方法 |
| CN111109302A (zh) * | 2020-02-22 | 2020-05-08 | 深圳超微颗粒产业有限责任公司 | 一种抗微生物气溶胶和染毒飞沫悬浮颗粒喷剂及其制备方法 |
| CN115052487A (zh) * | 2020-02-20 | 2022-09-13 | 帝斯曼知识产权资产管理有限公司 | 通过饲料预防病毒传播 |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1221175C (zh) * | 2002-10-08 | 2005-10-05 | 谢永军 | 空气杀菌消毒剂 |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2012104571A1 (en) * | 2011-02-02 | 2012-08-09 | GILHOLM, Stephen, Philip | Compositions of monoterpenoids for the treatment of influenza |
| CN105211123A (zh) * | 2014-06-10 | 2016-01-06 | 黄安宏 | 通过空气净化器消除空气污染的中草药消毒剂的制备方法 |
| CN115052487A (zh) * | 2020-02-20 | 2022-09-13 | 帝斯曼知识产权资产管理有限公司 | 通过饲料预防病毒传播 |
| CN111109302A (zh) * | 2020-02-22 | 2020-05-08 | 深圳超微颗粒产业有限责任公司 | 一种抗微生物气溶胶和染毒飞沫悬浮颗粒喷剂及其制备方法 |
| CN111109302B (zh) * | 2020-02-22 | 2021-04-06 | 深圳超微颗粒产业有限责任公司 | 一种抗微生物气溶胶和染毒飞沫悬浮颗粒喷剂及其制备方法 |
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| Publication number | Publication date |
|---|---|
| CN101491243B (zh) | 2012-04-25 |
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