CN101391073B - Da huoluo capsule preparation method - Google Patents
Da huoluo capsule preparation method Download PDFInfo
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- CN101391073B CN101391073B CN2008101718201A CN200810171820A CN101391073B CN 101391073 B CN101391073 B CN 101391073B CN 2008101718201 A CN2008101718201 A CN 2008101718201A CN 200810171820 A CN200810171820 A CN 200810171820A CN 101391073 B CN101391073 B CN 101391073B
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- fine powder
- moschus
- sanguis draxonis
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Abstract
The invention belongs to the technical field of traditional Chinese medicine, in particular to a preparation method for da huoluo capsules. The da huoluo capsules have the following medicinal compositions: red ginseng, rhizome of largehead atractylodes, liquorice roots, prepared rhizome of adhesive rehmannia, radix-polygoni multiflori, tortoise shells (prepared with vinegar), frankincense preparata, myrrh preparata, dragon blood, red peony roots, cassia barks, anemones raddeanae rhizome, musk, borneol, benzoin, Chinese eaglewood, costustoot, clove, nutgrass galingale rhizome, rhinoceros horn, combined spicebush roots, green tangerine peels, radic aconite kusnezoffii preparata, Chinese ephedra, asarum, incised notopterygium, divaricate saposhnikovia root, agkistrodon, zaocys, tiger bones, colophony, rhizome drynariae (scalded and dehaired), tall gas tcmlibodia tubers, pedate pinalliaJackinthepulpit rhizome (preparata), scorpio, bombyx batryticatus, lumbricus, roots of lobed kudzuvine, cardamom, pogostemon cablin (Blanco) benth, male fern rhizome, cow-bezoar, radix et rhizomarhei, rhizoma coptidis, baical skullcap roots, figwort roots and clematis roots. Through the implementation of the invention, the stability of the compositions in the medicine can be improved, the loss of effective compositions in the medicine is reduced, and the yield and the medicinal quality controllability are improved.
Description
[technical field]
The invention belongs to the traditional Chinese medicine technology technical field, be specifically related to a kind of preparation method of Da huoluo capsule.
[background technology]
Da huoluo capsule derives from Tongrentang's classics recipe DAHUOLUO WAN, and this medicine is used for wind-expelling pain-stopping, dehumidifying eliminating phlegm, relaxing muscles and tendons and activating QI and blood in the collateral.Be used for the hemiplegia that cerebral infarction causes, walking disorder and chest arthralgia precordial pain syndrome that the pain that rheumatism arthromyodynia (rheumatic arthritis) causes, spasm of muscles and vessels lumbago and skelalgia and traumatic injury cause.
Equally, the function of Da huoluo capsule cures mainly and is wind-expelling pain-stopping, dehumidifying eliminating phlegm, relaxing muscles and tendons and activating QI and blood in the collateral.Be used for the paralysis that the apoplexy syncope due to accumulation of phlegm causes, the arthralgia pain that withers enough, spasm of muscles and vessels, lumbago and skelalgia and traumatic injury, walking disorder, the diseases such as the thoracic obstruction.
The basis prescription of table 1 Da huoluo capsule
Radix Ginseng Rubra 10g Rhizoma Atractylodis Macrocephalae 3.3g Radix Glycyrrhizae 6.7g
Radix Rehmanniae Preparata 6.7g Radix Angelicae Sinensis 5.0g Radix Polygoni Multiflori 6.7g
Carapax Et Plastrum Testudinis (vinegar system) 2.3g Olibanum (system) 3.3g Myrrha (processed) 3.3g
Sanguis Draxonis 2.3g Radix Paeoniae Rubra 3.3g Cortex Cinnamomi 6.7g
Rhizoma Anemones Raddeanae 6.7g Moschus 1.7g Borneolum Syntheticum 0.5g
Benzoinum 3.3g Lignum Aquilariae Resinatum 6.7g Radix Aucklandiae 6.7g
Flos Caryophylli 3.3g Rhizoma Cyperi 3.3g Cornu rhinocerotis 1.7g
Radix Linderae 6.7g Pericarpium Citri Reticulatae Viride 3.3g Radix Aconiti Kusnezoffii Preparata 6.7g
Herba Ephedrae 6.7g Herba Asari 3.3g Rhizoma Et Radix Notopterygii 3.3g
Radix Saposhnikoviae 8.3g Agkistrodon 6.7g Zaocys 6.7g
Os Tigris 5.0g Colophonium 1.7g Rhizoma Drynariae (boiling hot, unhairing) 3.3g
Rhizoma Gastrodiae 6.7g Rhizoma Arisaematis (system) 3.3g Scorpio 6.7g
Bombyx Batryticatus 3.3g Pheretima 1.7g Radix Puerariae 5.0g
Fructus Amomi Rotundus 3.3g Herba Pogostemonis 6.7g Rhizoma Osmundae 6.7g
Calculus Bovis 0.5g Radix Et Rhizoma Rhei 6.7g Rhizoma Coptidis 6.7g
Radix Scutellariae 3.3g Radix Scrophulariae 3.3g Radix Clematidis 6.7g
[summary of the invention]
The object of the present invention is to provide a kind of preparation method of Da huoluo capsule.
The prescription of Da huoluo capsule of the present invention is:
Radix Ginseng Rubra 10g Rhizoma Atractylodis Macrocephalae 3.3g Radix Glycyrrhizae 6.7g
Radix Rehmanniae Preparata 6.7g Radix Angelicae Sinensis 5.0g Radix Polygoni Multiflori 6.7g
Carapax Et Plastrum Testudinis (vinegar system) 2.3g Olibanum (system) 3.3g Myrrha (processed) 3.3g
Sanguis Draxonis 2.3g Radix Paeoniae Rubra 3.3g Cortex Cinnamomi 6.7g
Rhizoma Anemones Raddeanae 6.7g Moschus 1.7g Borneolum Syntheticum 0.5g
Benzoinum 3.3g Lignum Aquilariae Resinatum 6.7g Radix Aucklandiae 6.7g
Flos Caryophylli 3.3g Rhizoma Cyperi 3.3g Cornu rhinocerotis 1.7g
Radix Linderae 6.7g Pericarpium Citri Reticulatae Viride 3.3g Radix Aconiti Kusnezoffii Preparata 6.7g
Herba Ephedrae 6.7g Herba Asari 3.3g Rhizoma Et Radix Notopterygii 3.3g
Radix Saposhnikoviae 8.3g Agkistrodon 6.7g Zaocys 6.7g
Os Tigris 5.0g Colophonium 1.7g Rhizoma Drynariae (boiling hot, unhairing) 3.3g
Rhizoma Gastrodiae 6.7g Rhizoma Arisaematis (system) 3.3g Scorpio 6.7g
Bombyx Batryticatus 3.3g Pheretima 1.7g Radix Puerariae 5.0g
Fructus Amomi Rotundus 3.3g Herba Pogostemonis 6.7g Rhizoma Osmundae 6.7g
Calculus Bovis 0.5g Radix Et Rhizoma Rhei 6.7g Rhizoma Coptidis 6.7g
Radix Scutellariae 3.3g Radix Scrophulariae 3.3g Radix Clematidis 6.7g
Particularly, preparation method of the present invention is: above 48 herbal medicines, except get Sanguis Draxonis, Rhizoma Arisaematis (system) mixed powder is broken into fine powder, outside Moschus, Borneolum Syntheticum, Calculus Bovis, the Pulvis Cornus Bubali Concentratus, all the other medicines are ground into fine powder and Calculus Bovis, Pulvis Cornus Bubali Concentratus facing-up, sieve, mixing; Get the 233g fine powder, add 150 milliliters of (g/ml) refined honey and 80% alcohol mixeding liquids, make soft material, cross 12 mesh sieves, cold drying 2-6 hour, 16 mesh sieve granulate, the suspension spray with Moschus and Borneolum Syntheticum and ethanol adds in addition, fling to ethanol, make 1000 of capsules, and get final product.
The preparation method of above-mentioned Da huoluo capsule, Moschus wherein and Borneolum Syntheticum porphyrize are made suspension with 25 milliliters of 30-95% ethanol grindings, and spray is added in the above-mentioned granule mixing.
The preparation method of above-mentioned Da huoluo capsule, Sanguis Draxonis wherein, Rhizoma Arisaematis (system) carry out superfine grinding, and grinding particle size is the 10-200 micron.
The preparation method of above-mentioned Da huoluo capsule, Radix Ginseng Rubra wherein, the Rhizoma Atractylodis Macrocephalae, Radix Glycyrrhizae, Radix Rehmanniae Preparata, Radix Angelicae Sinensis, Radix Polygoni Multiflori, Carapax Et Plastrum Testudinis (vinegar system), Olibanum (system), Myrrha (processed), Sanguis Draxonis, Radix Paeoniae Rubra, Cortex Cinnamomi, Rhizoma Anemones Raddeanae, Benzoinum, Lignum Aquilariae Resinatum, the Radix Aucklandiae, Flos Caryophylli, Rhizoma Cyperi, the Radix Linderae, Pericarpium Citri Reticulatae Viride, Radix Aconiti Kusnezoffii Preparata, Herba Ephedrae, Herba Asari, Rhizoma Et Radix Notopterygii, Radix Saposhnikoviae, Agkistrodon, Zaocys, Os Tigris, Colophonium, Rhizoma Drynariae (scalds, unhairing), Rhizoma Gastrodiae, Rhizoma Arisaematis (system), Scorpio, Bombyx Batryticatus, Pheretima, Radix Puerariae, Fructus Amomi Rotundus, Herba Pogostemonis, Rhizoma Osmundae, Radix Et Rhizoma Rhei, Rhizoma Coptidis, Radix Scutellariae, Radix Scrophulariae, Radix Clematidis carries out superfine grinding, and grinding particle size is the 10-200 micron.
The preparation method of above-mentioned Da huoluo capsule, the temperature of its cold drying are 55-60 degree centigrade.
The preparation method of above-mentioned Da huoluo capsule, the oven dry grain thickness is 0.5 centimetre during its cold drying.
The preparation method of above-mentioned Da huoluo capsule during its cold drying, was stirred once every 1 hour.
The preparation method of above-mentioned Da huoluo capsule, wherein concentration of alcohol is 50-95%, described refined honey concentration is 15-23%, the time 2-5 of described drying hour.
The preparation method of above-mentioned Da huoluo capsule, preferably wherein concentration of alcohol is 60-95%, described refined honey concentration is 15-25%, the time 2-5 of described drying hour.Above-mentioned preparation method, more preferably concentration of alcohol is 80%, described refined honey concentration is 15%, the 3 hours time of described drying; In the above-mentioned preparation method, but also preferred alcohol concentration is 95%, and described refined honey concentration is 15%, the 3 hours time of described drying; Above-mentioned preparation method, but also preferred alcohol concentration is 60%.Described refined honey concentration is 15%, the 3 hours time of described drying.
In the above-mentioned preparation method, described Os Tigris, Calculus Bovis, Cornu rhinocerotis, Moschus production change Os pardi, artificial Calculus Bovis, Pulvis Cornus Bubali Concentratus, artificial Moschus into according to the Ministry of Public Health relevant document and feed intake.
[specific embodiment]
Following embodiment further describes the present invention, but described embodiment only is used for explanation the present invention rather than restriction the present invention.Following examples are according to following prescription proportioning, and wherein Os Tigris, Calculus Bovis, Cornu rhinocerotis, Moschus production change Os pardi, artificial Calculus Bovis, Pulvis Cornus Bubali Concentratus, artificial Moschus into according to the Ministry of Public Health relevant document and feed intake.
Radix Ginseng Rubra 10g Rhizoma Atractylodis Macrocephalae 3.3g Radix Glycyrrhizae 6.7g
Radix Rehmanniae Preparata 6.7g Radix Angelicae Sinensis 5.0g Radix Polygoni Multiflori 6.7g
Carapax Et Plastrum Testudinis (vinegar system) 2.3g Olibanum (system) 3.3g Myrrha (processed) 3.3g
Sanguis Draxonis 2.3g Radix Paeoniae Rubra 3.3g Cortex Cinnamomi 6.7g
Rhizoma Anemones Raddeanae 6.7g Moschus 1.7g Borneolum Syntheticum 0.5g
Benzoinum 3.3g Lignum Aquilariae Resinatum 6.7g Radix Aucklandiae 6.7g
Flos Caryophylli 3.3g Rhizoma Cyperi 3.3g Cornu rhinocerotis 1.7g
Radix Linderae 6.7g Pericarpium Citri Reticulatae Viride 3.3g Radix Aconiti Kusnezoffii Preparata 6.7g
Herba Ephedrae 6.7g Herba Asari 3.3g Rhizoma Et Radix Notopterygii 3.3g
Radix Saposhnikoviae 8.3g Agkistrodon 6.7g Zaocys 6.7g
Os Tigris 5.0g Colophonium 1.7g Rhizoma Drynariae (boiling hot, unhairing) 3.3g
Rhizoma Gastrodiae 6.7g Rhizoma Arisaematis (system) 3.3g Scorpio 6.7g
Bombyx Batryticatus 3.3g Pheretima 1.7g Radix Puerariae 5.0g
Fructus Amomi Rotundus 3.3g Herba Pogostemonis 6.7g Rhizoma Osmundae 6.7g
Calculus Bovis 0.5g Radix Et Rhizoma Rhei 6.7g Rhizoma Coptidis 6.7g
Radix Scutellariae 3.3g Radix Scrophulariae 3.3g Radix Clematidis 6.7g
Embodiment 1
More than 48 herbal medicines, Sanguis Draxonis wherein, Rhizoma Arisaematis (system), Radix Ginseng Rubra, the Rhizoma Atractylodis Macrocephalae, Radix Glycyrrhizae, Radix Rehmanniae Preparata, Radix Angelicae Sinensis, Radix Polygoni Multiflori, Carapax Et Plastrum Testudinis (vinegar system), Olibanum (system), Myrrha (processed), Sanguis Draxonis, Radix Paeoniae Rubra, Cortex Cinnamomi, Rhizoma Anemones Raddeanae, Benzoinum, Lignum Aquilariae Resinatum, the Radix Aucklandiae, Flos Caryophylli, Rhizoma Cyperi, the Radix Linderae, Pericarpium Citri Reticulatae Viride, Radix Aconiti Kusnezoffii Preparata, Herba Ephedrae, Herba Asari, Rhizoma Et Radix Notopterygii, Radix Saposhnikoviae, Agkistrodon, Zaocys, Os Tigris, Colophonium, Rhizoma Drynariae (scalds, unhairing), Rhizoma Gastrodiae, Rhizoma Arisaematis (system), Scorpio, Bombyx Batryticatus, Pheretima, Radix Puerariae, Fructus Amomi Rotundus, Herba Pogostemonis, Rhizoma Osmundae, Radix Et Rhizoma Rhei, Rhizoma Coptidis, Radix Scutellariae, Radix Scrophulariae, Radix Clematidis carries out superfine grinding, and grinding particle size is the 10-200 micron; Except get Sanguis Draxonis, Rhizoma Arisaematis (system) mixed powder is broken into fine powder (putting in addition), outside Moschus, Borneolum Syntheticum, Calculus Bovis, the Pulvis Cornus Bubali Concentratus, all the other medicines are ground into fine powder and Calculus Bovis, Pulvis Cornus Bubali Concentratus facing-up, sieve, mixing.Get the 233g fine powder, 150 milliliters of 80% alcohol mixeding liquids of adding 15% (g/ml) refined honey are made soft material, cross 12 mesh sieves, cold drying 2 hours, 16 mesh sieve granulate are in addition with Moschus and Borneolum Syntheticum porphyrize, make suspension with 25 milliliter of 60% ethanol grinding, spray is added in the above-mentioned granule, and mixing is flung to ethanol, make 1000 of capsules, and get final product.
Embodiment 2
More than 48 herbal medicines, Sanguis Draxonis wherein, Rhizoma Arisaematis (system), Radix Ginseng Rubra, the Rhizoma Atractylodis Macrocephalae, Radix Glycyrrhizae, Radix Rehmanniae Preparata, Radix Angelicae Sinensis, Radix Polygoni Multiflori, Carapax Et Plastrum Testudinis (vinegar system), Olibanum (system), Myrrha (processed), Sanguis Draxonis, Radix Paeoniae Rubra, Cortex Cinnamomi, Rhizoma Anemones Raddeanae, Benzoinum, Lignum Aquilariae Resinatum, the Radix Aucklandiae, Flos Caryophylli, Rhizoma Cyperi, the Radix Linderae, Pericarpium Citri Reticulatae Viride, Radix Aconiti Kusnezoffii Preparata, Herba Ephedrae, Herba Asari, Rhizoma Et Radix Notopterygii, Radix Saposhnikoviae, Agkistrodon, Zaocys, Os Tigris, Colophonium, Rhizoma Drynariae (scalds, unhairing), Rhizoma Gastrodiae, Rhizoma Arisaematis (system), Scorpio, Bombyx Batryticatus, Pheretima, Radix Puerariae, Fructus Amomi Rotundus, Herba Pogostemonis, Rhizoma Osmundae, Radix Et Rhizoma Rhei, Rhizoma Coptidis, Radix Scutellariae, Radix Scrophulariae, Radix Clematidis carries out superfine grinding, and grinding particle size is the 10-200 micron; Except get Sanguis Draxonis, Rhizoma Arisaematis (system) mixed powder is broken into fine powder (putting in addition), outside Moschus, Borneolum Syntheticum, Calculus Bovis, the Pulvis Cornus Bubali Concentratus, all the other medicines are ground into fine powder and Calculus Bovis, Pulvis Cornus Bubali Concentratus facing-up, sieve, mixing.Get the 233g fine powder, 150 milliliters of 80% alcohol mixeding liquids of adding 20% (g/ml) refined honey are made soft material, cross 12 mesh sieves, low temperature 55-60 degree centigrade drying 3 hours, 16 mesh sieve granulate are in addition with Moschus and Borneolum Syntheticum porphyrize, make suspension with 25 milliliter of 60% ethanol grinding, spray is added in the above-mentioned granule, and mixing is flung to ethanol, make 1000 of capsules, and get final product.
Embodiment 3
More than 48 herbal medicines, Sanguis Draxonis wherein, Rhizoma Arisaematis (system), Radix Ginseng Rubra, the Rhizoma Atractylodis Macrocephalae, Radix Glycyrrhizae, Radix Rehmanniae Preparata, Radix Angelicae Sinensis, Radix Polygoni Multiflori, Carapax Et Plastrum Testudinis (vinegar system), Olibanum (system), Myrrha (processed), Sanguis Draxonis, Radix Paeoniae Rubra, Cortex Cinnamomi, Rhizoma Anemones Raddeanae, Benzoinum, Lignum Aquilariae Resinatum, the Radix Aucklandiae, Flos Caryophylli, Rhizoma Cyperi, the Radix Linderae, Pericarpium Citri Reticulatae Viride, Radix Aconiti Kusnezoffii Preparata, Herba Ephedrae, Herba Asari, Rhizoma Et Radix Notopterygii, Radix Saposhnikoviae, Agkistrodon, Zaocys, Os Tigris, Colophonium, Rhizoma Drynariae (scalds, unhairing), Rhizoma Gastrodiae, Rhizoma Arisaematis (system), Scorpio, Bombyx Batryticatus, Pheretima, Radix Puerariae, Fructus Amomi Rotundus, Herba Pogostemonis, Rhizoma Osmundae, Radix Et Rhizoma Rhei, Rhizoma Coptidis, Radix Scutellariae, Radix Scrophulariae, Radix Clematidis carries out superfine grinding, and grinding particle size is the 10-200 micron; Except get Sanguis Draxonis, Rhizoma Arisaematis (system) mixed powder is broken into fine powder (putting in addition), outside Moschus, Borneolum Syntheticum, Calculus Bovis, the Pulvis Cornus Bubali Concentratus, all the other medicines are ground into fine powder and Calculus Bovis, Pulvis Cornus Bubali Concentratus facing-up, sieve, mixing.Get the 233g fine powder, 150 milliliters of 80% alcohol mixeding liquids of adding 25% (g/ml) refined honey are made soft material, cross 12 mesh sieves, low temperature 55-60 degree centigrade drying 5 hours, 16 mesh sieve granulate are in addition with Moschus and Borneolum Syntheticum porphyrize, make suspension with 25 milliliter of 60% ethanol grinding, spray is added in the above-mentioned granule, and mixing is flung to ethanol, make 1000 of capsules, and get final product.
Embodiment 4
More than 48 herbal medicines, Sanguis Draxonis wherein, Rhizoma Arisaematis (system), Radix Ginseng Rubra, the Rhizoma Atractylodis Macrocephalae, Radix Glycyrrhizae, Radix Rehmanniae Preparata, Radix Angelicae Sinensis, Radix Polygoni Multiflori, Carapax Et Plastrum Testudinis (vinegar system), Olibanum (system), Myrrha (processed), Sanguis Draxonis, Radix Paeoniae Rubra, Cortex Cinnamomi, Rhizoma Anemones Raddeanae, Benzoinum, Lignum Aquilariae Resinatum, the Radix Aucklandiae, Flos Caryophylli, Rhizoma Cyperi, the Radix Linderae, Pericarpium Citri Reticulatae Viride, Radix Aconiti Kusnezoffii Preparata, Herba Ephedrae, Herba Asari, Rhizoma Et Radix Notopterygii, Radix Saposhnikoviae, Agkistrodon, Zaocys, Os Tigris, Colophonium, Rhizoma Drynariae (scalds, unhairing), Rhizoma Gastrodiae, Rhizoma Arisaematis (system), Scorpio, Bombyx Batryticatus, Pheretima, Radix Puerariae, Fructus Amomi Rotundus, Herba Pogostemonis, Rhizoma Osmundae, Radix Et Rhizoma Rhei, Rhizoma Coptidis, Radix Scutellariae, Radix Scrophulariae, Radix Clematidis carries out superfine grinding, and grinding particle size is the 10-200 micron; Except get Sanguis Draxonis, Rhizoma Arisaematis (system) mixed powder is broken into fine powder (putting in addition), outside Moschus, Borneolum Syntheticum, Calculus Bovis, the Pulvis Cornus Bubali Concentratus, all the other medicines are ground into fine powder and Calculus Bovis, Pulvis Cornus Bubali Concentratus facing-up, sieve, mixing.Get the 233g fine powder, 150 milliliters of 80% alcohol mixeding liquids of adding 15% (g/ml) refined honey are made soft material, cross 12 mesh sieves, cold drying 3 hours, 16 mesh sieve granulate are in addition with Moschus and Borneolum Syntheticum porphyrize, make suspension with 25 milliliter of 80% ethanol grinding, spray is added in the above-mentioned granule, and mixing is flung to ethanol, make 1000 of capsules, and get final product.
Embodiment 5
More than 48 herbal medicines, Sanguis Draxonis wherein, Rhizoma Arisaematis (system), Radix Ginseng Rubra, the Rhizoma Atractylodis Macrocephalae, Radix Glycyrrhizae, Radix Rehmanniae Preparata, Radix Angelicae Sinensis, Radix Polygoni Multiflori, Carapax Et Plastrum Testudinis (vinegar system), Olibanum (system), Myrrha (processed), Sanguis Draxonis, Radix Paeoniae Rubra, Cortex Cinnamomi, Rhizoma Anemones Raddeanae, Benzoinum, Lignum Aquilariae Resinatum, the Radix Aucklandiae, Flos Caryophylli, Rhizoma Cyperi, the Radix Linderae, Pericarpium Citri Reticulatae Viride, Radix Aconiti Kusnezoffii Preparata, Herba Ephedrae, Herba Asari, Rhizoma Et Radix Notopterygii, Radix Saposhnikoviae, Agkistrodon, Zaocys, Os Tigris, Colophonium, Rhizoma Drynariae (scalds, unhairing), Rhizoma Gastrodiae, Rhizoma Arisaematis (system), Scorpio, Bombyx Batryticatus, Pheretima, Radix Puerariae, Fructus Amomi Rotundus, Herba Pogostemonis, Rhizoma Osmundae, Radix Et Rhizoma Rhei, Rhizoma Coptidis, Radix Scutellariae, Radix Scrophulariae, Radix Clematidis carries out superfine grinding, and grinding particle size is the 10-200 micron; Except get Sanguis Draxonis, Rhizoma Arisaematis (system) mixed powder is broken into fine powder (putting in addition), outside Moschus, Borneolum Syntheticum, Calculus Bovis, the Pulvis Cornus Bubali Concentratus, all the other medicines are ground into fine powder and Calculus Bovis, Pulvis Cornus Bubali Concentratus facing-up, sieve, mixing.Get the 233g fine powder, 150 milliliters of 80% alcohol mixeding liquids of adding 20% (g/ml) refined honey are made soft material, cross 12 mesh sieves, low temperature 55-60 degree centigrade drying 5 hours, 16 mesh sieve granulate are in addition with Moschus and Borneolum Syntheticum porphyrize, make suspension with 25 milliliter of 80% ethanol grinding, spray is added in the above-mentioned granule, and mixing is flung to ethanol, make 1000 of capsules, and get final product.
Embodiment 6
More than 48 herbal medicines, Sanguis Draxonis wherein, Rhizoma Arisaematis (system), Radix Ginseng Rubra, the Rhizoma Atractylodis Macrocephalae, Radix Glycyrrhizae, Radix Rehmanniae Preparata, Radix Angelicae Sinensis, Radix Polygoni Multiflori, Carapax Et Plastrum Testudinis (vinegar system), Olibanum (system), Myrrha (processed), Sanguis Draxonis, Radix Paeoniae Rubra, Cortex Cinnamomi, Rhizoma Anemones Raddeanae, Benzoinum, Lignum Aquilariae Resinatum, the Radix Aucklandiae, Flos Caryophylli, Rhizoma Cyperi, the Radix Linderae, Pericarpium Citri Reticulatae Viride, Radix Aconiti Kusnezoffii Preparata, Herba Ephedrae, Herba Asari, Rhizoma Et Radix Notopterygii, Radix Saposhnikoviae, Agkistrodon, Zaocys, Os Tigris, Colophonium, Rhizoma Drynariae (scalds, unhairing), Rhizoma Gastrodiae, Rhizoma Arisaematis (system), Scorpio, Bombyx Batryticatus, Pheretima, Radix Puerariae, Fructus Amomi Rotundus, Herba Pogostemonis, Rhizoma Osmundae, Radix Et Rhizoma Rhei, Rhizoma Coptidis, Radix Scutellariae, Radix Scrophulariae, Radix Clematidis carries out superfine grinding, and grinding particle size is the 10-200 micron; Except get Sanguis Draxonis, Rhizoma Arisaematis (system) mixed powder is broken into fine powder (putting in addition), outside Moschus, Borneolum Syntheticum, Calculus Bovis, the Pulvis Cornus Bubali Concentratus, all the other medicines are ground into fine powder and Calculus Bovis, Pulvis Cornus Bubali Concentratus facing-up, sieve, mixing.Get the 233g fine powder, 150 milliliters of 80% alcohol mixeding liquids of adding 25% (g/ml) refined honey are made soft material, cross 12 mesh sieves, low temperature 55-60 degree centigrade drying 2 hours, 16 mesh sieve granulate are in addition with Moschus and Borneolum Syntheticum porphyrize, make suspension with 25 milliliter of 80% ethanol grinding, spray is added in the above-mentioned granule, and mixing is flung to ethanol, make 1000 of capsules, and get final product.
Embodiment 7
More than 48 herbal medicines, Sanguis Draxonis wherein, Rhizoma Arisaematis (system), Radix Ginseng Rubra, the Rhizoma Atractylodis Macrocephalae, Radix Glycyrrhizae, Radix Rehmanniae Preparata, Radix Angelicae Sinensis, Radix Polygoni Multiflori, Carapax Et Plastrum Testudinis (vinegar system), Olibanum (system), Myrrha (processed), Sanguis Draxonis, Radix Paeoniae Rubra, Cortex Cinnamomi, Rhizoma Anemones Raddeanae, Benzoinum, Lignum Aquilariae Resinatum, the Radix Aucklandiae, Flos Caryophylli, Rhizoma Cyperi, the Radix Linderae, Pericarpium Citri Reticulatae Viride, Radix Aconiti Kusnezoffii Preparata, Herba Ephedrae, Herba Asari, Rhizoma Et Radix Notopterygii, Radix Saposhnikoviae, Agkistrodon, Zaocys, Os Tigris, Colophonium, Rhizoma Drynariae (scalds, unhairing), Rhizoma Gastrodiae, Rhizoma Arisaematis (system), Scorpio, Bombyx Batryticatus, Pheretima, Radix Puerariae, Fructus Amomi Rotundus, Herba Pogostemonis, Rhizoma Osmundae, Radix Et Rhizoma Rhei, Rhizoma Coptidis, Radix Scutellariae, Radix Scrophulariae, Radix Clematidis carries out superfine grinding, and grinding particle size is the 10-200 micron; Except get Sanguis Draxonis, Rhizoma Arisaematis (system) mixed powder is broken into fine powder (putting in addition), outside Moschus, Borneolum Syntheticum, Calculus Bovis, the Pulvis Cornus Bubali Concentratus, all the other medicines are ground into fine powder and Calculus Bovis, Pulvis Cornus Bubali Concentratus facing-up, sieve, mixing.Get the 233g fine powder, 150 milliliters of 80% alcohol mixeding liquids of adding 15% (g/ml) refined honey are made soft material, cross 12 mesh sieves, cold drying 5 hours, 16 mesh sieve granulate are in addition with Moschus and Borneolum Syntheticum porphyrize, make suspension with 25 milliliter of 95% ethanol grinding, spray is added in the above-mentioned granule, and mixing is flung to ethanol, make 1000 of capsules, and get final product.
Embodiment 8
More than 48 herbal medicines, Sanguis Draxonis wherein, Rhizoma Arisaematis (system), Radix Ginseng Rubra, the Rhizoma Atractylodis Macrocephalae, Radix Glycyrrhizae, Radix Rehmanniae Preparata, Radix Angelicae Sinensis, Radix Polygoni Multiflori, Carapax Et Plastrum Testudinis (vinegar system), Olibanum (system), Myrrha (processed), Sanguis Draxonis, Radix Paeoniae Rubra, Cortex Cinnamomi, Rhizoma Anemones Raddeanae, Benzoinum, Lignum Aquilariae Resinatum, the Radix Aucklandiae, Flos Caryophylli, Rhizoma Cyperi, the Radix Linderae, Pericarpium Citri Reticulatae Viride, Radix Aconiti Kusnezoffii Preparata, Herba Ephedrae, Herba Asari, Rhizoma Et Radix Notopterygii, Radix Saposhnikoviae, Agkistrodon, Zaocys, Os Tigris, Colophonium, Rhizoma Drynariae (scalds, unhairing), Rhizoma Gastrodiae, Rhizoma Arisaematis (system), Scorpio, Bombyx Batryticatus, Pheretima, Radix Puerariae, Fructus Amomi Rotundus, Herba Pogostemonis, Rhizoma Osmundae, Radix Et Rhizoma Rhei, Rhizoma Coptidis, Radix Scutellariae, Radix Scrophulariae, Radix Clematidis carries out superfine grinding, and grinding particle size is the 10-200 micron; Except get Sanguis Draxonis, Rhizoma Arisaematis (system) mixed powder is broken into fine powder (putting in addition), outside Moschus, Borneolum Syntheticum, Calculus Bovis, the Pulvis Cornus Bubali Concentratus, all the other medicines are ground into fine powder and Calculus Bovis, Pulvis Cornus Bubali Concentratus facing-up, sieve, mixing.Get the 233g fine powder, 150 milliliters of 80% alcohol mixeding liquids of adding 20% (g/ml) refined honey are made soft material, cross 12 mesh sieves, low temperature 55-60 degree centigrade drying 2 hours, 16 mesh sieve granulate are in addition with Moschus and Borneolum Syntheticum porphyrize, make suspension with 25 milliliter of 95% ethanol grinding, spray is added in the above-mentioned granule, and mixing is flung to ethanol, make 1000 of capsules, and get final product.
Embodiment 9
More than 48 herbal medicines, Sanguis Draxonis wherein, Rhizoma Arisaematis (system), Radix Ginseng Rubra, the Rhizoma Atractylodis Macrocephalae, Radix Glycyrrhizae, Radix Rehmanniae Preparata, Radix Angelicae Sinensis, Radix Polygoni Multiflori, Carapax Et Plastrum Testudinis (vinegar system), Olibanum (system), Myrrha (processed), Sanguis Draxonis, Radix Paeoniae Rubra, Cortex Cinnamomi, Rhizoma Anemones Raddeanae, Benzoinum, Lignum Aquilariae Resinatum, the Radix Aucklandiae, Flos Caryophylli, Rhizoma Cyperi, the Radix Linderae, Pericarpium Citri Reticulatae Viride, Radix Aconiti Kusnezoffii Preparata, Herba Ephedrae, Herba Asari, Rhizoma Et Radix Notopterygii, Radix Saposhnikoviae, Agkistrodon, Zaocys, Os Tigris, Colophonium, Rhizoma Drynariae (scalds, unhairing), Rhizoma Gastrodiae, Rhizoma Arisaematis (system), Scorpio, Bombyx Batryticatus, Pheretima, Radix Puerariae, Fructus Amomi Rotundus, Herba Pogostemonis, Rhizoma Osmundae, Radix Et Rhizoma Rhei, Rhizoma Coptidis, Radix Scutellariae, Radix Scrophulariae, Radix Clematidis carries out superfine grinding, and grinding particle size is the 10-200 micron; Except get Sanguis Draxonis, Rhizoma Arisaematis (system) mixed powder is broken into fine powder (putting in addition), outside Moschus, Borneolum Syntheticum, Calculus Bovis, the Pulvis Cornus Bubali Concentratus, all the other medicines are ground into fine powder and Calculus Bovis, Pulvis Cornus Bubali Concentratus facing-up, sieve, mixing.Get the 233g fine powder, 150 milliliters of 80% alcohol mixeding liquids of adding 25% (g/ml) refined honey are made soft material, cross 12 mesh sieves, low temperature 55-60 degree centigrade drying 3 hours, 16 mesh sieve granulate are in addition with Moschus and Borneolum Syntheticum porphyrize, make suspension with 25 milliliter of 80% ethanol grinding, spray is added in the above-mentioned granule, and mixing is flung to ethanol, make 1000 of capsules, and get final product.
Embodiment 10
More than 48 herbal medicines, Sanguis Draxonis wherein, Rhizoma Arisaematis (system), Radix Ginseng Rubra, the Rhizoma Atractylodis Macrocephalae, Radix Glycyrrhizae, Radix Rehmanniae Preparata, Radix Angelicae Sinensis, Radix Polygoni Multiflori, Carapax Et Plastrum Testudinis (vinegar system), Olibanum (system), Myrrha (processed), Sanguis Draxonis, Radix Paeoniae Rubra, Cortex Cinnamomi, Rhizoma Anemones Raddeanae, Benzoinum, Lignum Aquilariae Resinatum, the Radix Aucklandiae, Flos Caryophylli, Rhizoma Cyperi, the Radix Linderae, Pericarpium Citri Reticulatae Viride, Radix Aconiti Kusnezoffii Preparata, Herba Ephedrae, Herba Asari, Rhizoma Et Radix Notopterygii, Radix Saposhnikoviae, Agkistrodon, Zaocys, Os Tigris, Colophonium, Rhizoma Drynariae (scalds, unhairing), Rhizoma Gastrodiae, Rhizoma Arisaematis (system), Scorpio, Bombyx Batryticatus, Pheretima, Radix Puerariae, Fructus Amomi Rotundus, Herba Pogostemonis, Rhizoma Osmundae, Radix Et Rhizoma Rhei, Rhizoma Coptidis, Radix Scutellariae, Radix Scrophulariae, Radix Clematidis carries out superfine grinding, and grinding particle size is the 10-200 micron; Except get Sanguis Draxonis, Rhizoma Arisaematis (system) mixed powder is broken into fine powder (putting in addition), outside Moschus, Borneolum Syntheticum, Calculus Bovis, the Pulvis Cornus Bubali Concentratus, all the other medicines are ground into fine powder and Calculus Bovis, Pulvis Cornus Bubali Concentratus facing-up, sieve, mixing.Get the 233g fine powder, 150 milliliters of 80% alcohol mixeding liquids of adding 15% (g/ml) refined honey are made soft material, cross 12 mesh sieves, cold drying 5 hours, 16 mesh sieve granulate are in addition with Moschus and Borneolum Syntheticum porphyrize, make suspension with 25 milliliter of 55% ethanol grinding, spray is added in the above-mentioned granule, and mixing is flung to ethanol, make 1000 of capsules, and get final product.
Embodiment 11
More than 48 herbal medicines, Sanguis Draxonis wherein, Rhizoma Arisaematis (system), Radix Ginseng Rubra, the Rhizoma Atractylodis Macrocephalae, Radix Glycyrrhizae, Radix Rehmanniae Preparata, Radix Angelicae Sinensis, Radix Polygoni Multiflori, Carapax Et Plastrum Testudinis (vinegar system), Olibanum (system), Myrrha (processed), Sanguis Draxonis, Radix Paeoniae Rubra, Cortex Cinnamomi, Rhizoma Anemones Raddeanae, Benzoinum, Lignum Aquilariae Resinatum, the Radix Aucklandiae, Flos Caryophylli, Rhizoma Cyperi, the Radix Linderae, Pericarpium Citri Reticulatae Viride, Radix Aconiti Kusnezoffii Preparata, Herba Ephedrae, Herba Asari, Rhizoma Et Radix Notopterygii, Radix Saposhnikoviae, Agkistrodon, Zaocys, Os Tigris, Colophonium, Rhizoma Drynariae (scalds, unhairing), Rhizoma Gastrodiae, Rhizoma Arisaematis (system), Scorpio, Bombyx Batryticatus, Pheretima, Radix Puerariae, Fructus Amomi Rotundus, Herba Pogostemonis, Rhizoma Osmundae, Radix Et Rhizoma Rhei, Rhizoma Coptidis, Radix Scutellariae, Radix Scrophulariae, Radix Clematidis carries out superfine grinding, and grinding particle size is the 10-200 micron; Except get Sanguis Draxonis, Rhizoma Arisaematis (system) mixed powder is broken into fine powder (putting in addition), outside Moschus, Borneolum Syntheticum, Calculus Bovis, the Pulvis Cornus Bubali Concentratus, all the other medicines are ground into fine powder and Calculus Bovis, Pulvis Cornus Bubali Concentratus facing-up, sieve, mixing.Get the 233g fine powder, 150 milliliters of 80% alcohol mixeding liquids of adding 20% (g/ml) refined honey are made soft material, cross 12 mesh sieves, low temperature 55-60 degree centigrade drying 6 hours, 16 mesh sieve granulate are in addition with Moschus and Borneolum Syntheticum porphyrize, make suspension with 25 milliliter of 50% ethanol grinding, spray is added in the above-mentioned granule, and mixing is flung to ethanol, make 1000 of capsules, and get final product.
Embodiment 12
More than 48 herbal medicines, Sanguis Draxonis wherein, Rhizoma Arisaematis (system), Radix Ginseng Rubra, the Rhizoma Atractylodis Macrocephalae, Radix Glycyrrhizae, Radix Rehmanniae Preparata, Radix Angelicae Sinensis, Radix Polygoni Multiflori, Carapax Et Plastrum Testudinis (vinegar system), Olibanum (system), Myrrha (processed), Sanguis Draxonis, Radix Paeoniae Rubra, Cortex Cinnamomi, Rhizoma Anemones Raddeanae, Benzoinum, Lignum Aquilariae Resinatum, the Radix Aucklandiae, Flos Caryophylli, Rhizoma Cyperi, the Radix Linderae, Pericarpium Citri Reticulatae Viride, Radix Aconiti Kusnezoffii Preparata, Herba Ephedrae, Herba Asari, Rhizoma Et Radix Notopterygii, Radix Saposhnikoviae, Agkistrodon, Zaocys, Os Tigris, Colophonium, Rhizoma Drynariae (scalds, unhairing), Rhizoma Gastrodiae, Rhizoma Arisaematis (system), Scorpio, Bombyx Batryticatus, Pheretima, Radix Puerariae, Fructus Amomi Rotundus, Herba Pogostemonis, Rhizoma Osmundae, Radix Et Rhizoma Rhei, Rhizoma Coptidis, Radix Scutellariae, Radix Scrophulariae, Radix Clematidis carries out superfine grinding, and grinding particle size is the 10-200 micron; Except get Sanguis Draxonis, Rhizoma Arisaematis (system) mixed powder is broken into fine powder (putting in addition), outside Moschus, Borneolum Syntheticum, Calculus Bovis, the Pulvis Cornus Bubali Concentratus, all the other medicines are ground into fine powder and Calculus Bovis, Pulvis Cornus Bubali Concentratus facing-up, sieve, mixing.Get the 233g fine powder, 150 milliliters of 80% alcohol mixeding liquids of adding 25% (g/ml) refined honey are made soft material, cross 12 mesh sieves, low temperature 55-60 degree centigrade drying 3 hours, 16 mesh sieve granulate are in addition with Moschus and Borneolum Syntheticum porphyrize, make suspension with 20 milliliter of 50% ethanol grinding, spray is added in the above-mentioned granule, and mixing is flung to ethanol, make 1000 of capsules, and get final product.
Embodiment 13
More than 48 herbal medicines, Sanguis Draxonis wherein, Rhizoma Arisaematis (system), Radix Ginseng Rubra, the Rhizoma Atractylodis Macrocephalae, Radix Glycyrrhizae, Radix Rehmanniae Preparata, Radix Angelicae Sinensis, Radix Polygoni Multiflori, Carapax Et Plastrum Testudinis (vinegar system), Olibanum (system), Myrrha (processed), Sanguis Draxonis, Radix Paeoniae Rubra, Cortex Cinnamomi, Rhizoma Anemones Raddeanae, Benzoinum, Lignum Aquilariae Resinatum, the Radix Aucklandiae, Flos Caryophylli, Rhizoma Cyperi, the Radix Linderae, Pericarpium Citri Reticulatae Viride, Radix Aconiti Kusnezoffii Preparata, Herba Ephedrae, Herba Asari, Rhizoma Et Radix Notopterygii, Radix Saposhnikoviae, Agkistrodon, Zaocys, Os Tigris, Colophonium, Rhizoma Drynariae (scalds, unhairing), Rhizoma Gastrodiae, Rhizoma Arisaematis (system), Scorpio, Bombyx Batryticatus, Pheretima, Radix Puerariae, Fructus Amomi Rotundus, Herba Pogostemonis, Rhizoma Osmundae, Radix Et Rhizoma Rhei, Rhizoma Coptidis, Radix Scutellariae, Radix Scrophulariae, Radix Clematidis carries out superfine grinding, and grinding particle size is the 10-200 micron; Except get Sanguis Draxonis, Rhizoma Arisaematis (system) mixed powder is broken into fine powder (putting in addition), outside Moschus, Borneolum Syntheticum, Calculus Bovis, the Pulvis Cornus Bubali Concentratus, all the other medicines are ground into fine powder and Calculus Bovis, Pulvis Cornus Bubali Concentratus facing-up, sieve, mixing.Get the 233g fine powder, 150 milliliters of 80% alcohol mixeding liquids of adding 15% (g/ml) refined honey are made soft material, cross 12 mesh sieves, cold drying 2.5 hours, 16 mesh sieve granulate are in addition with Moschus and Borneolum Syntheticum porphyrize, make suspension with 25 milliliter of 60% ethanol grinding, spray is added in the above-mentioned granule, and mixing is flung to ethanol, make 1000 of capsules, and get final product.
Embodiment 14
More than 48 herbal medicines, Sanguis Draxonis wherein, Rhizoma Arisaematis (system), Radix Ginseng Rubra, the Rhizoma Atractylodis Macrocephalae, Radix Glycyrrhizae, Radix Rehmanniae Preparata, Radix Angelicae Sinensis, Radix Polygoni Multiflori, Carapax Et Plastrum Testudinis (vinegar system), Olibanum (system), Myrrha (processed), Sanguis Draxonis, Radix Paeoniae Rubra, Cortex Cinnamomi, Rhizoma Anemones Raddeanae, Benzoinum, Lignum Aquilariae Resinatum, the Radix Aucklandiae, Flos Caryophylli, Rhizoma Cyperi, the Radix Linderae, Pericarpium Citri Reticulatae Viride, Radix Aconiti Kusnezoffii Preparata, Herba Ephedrae, Herba Asari, Rhizoma Et Radix Notopterygii, Radix Saposhnikoviae, Agkistrodon, Zaocys, Os Tigris, Colophonium, Rhizoma Drynariae (scalds, unhairing), Rhizoma Gastrodiae, Rhizoma Arisaematis (system), Scorpio, Bombyx Batryticatus, Pheretima, Radix Puerariae, Fructus Amomi Rotundus, Herba Pogostemonis, Rhizoma Osmundae, Radix Et Rhizoma Rhei, Rhizoma Coptidis, Radix Scutellariae, Radix Scrophulariae, Radix Clematidis carries out superfine grinding, and grinding particle size is the 10-200 micron; Except get Sanguis Draxonis, Rhizoma Arisaematis (system) mixed powder is broken into fine powder (putting in addition), outside Moschus, Borneolum Syntheticum, Calculus Bovis, the Pulvis Cornus Bubali Concentratus, all the other medicines are ground into fine powder and Calculus Bovis, Pulvis Cornus Bubali Concentratus facing-up, sieve, mixing.Get the 233g fine powder, 150 milliliters of 80% alcohol mixeding liquids of adding 20% (g/ml) refined honey are made soft material, cross 12 mesh sieves, low temperature 55-60 degree centigrade drying 3 hours, 16 mesh sieve granulate are in addition with Moschus and Borneolum Syntheticum porphyrize, make suspension with 25 milliliter of 75% ethanol grinding, spray is added in the above-mentioned granule, and mixing is flung to ethanol, make 1000 of capsules, and get final product.
Embodiment 15
More than 48 herbal medicines, Sanguis Draxonis wherein, Rhizoma Arisaematis (system), Radix Ginseng Rubra, the Rhizoma Atractylodis Macrocephalae, Radix Glycyrrhizae, Radix Rehmanniae Preparata, Radix Angelicae Sinensis, Radix Polygoni Multiflori, Carapax Et Plastrum Testudinis (vinegar system), Olibanum (system), Myrrha (processed), Sanguis Draxonis, Radix Paeoniae Rubra, Cortex Cinnamomi, Rhizoma Anemones Raddeanae, Benzoinum, Lignum Aquilariae Resinatum, the Radix Aucklandiae, Flos Caryophylli, Rhizoma Cyperi, the Radix Linderae, Pericarpium Citri Reticulatae Viride, Radix Aconiti Kusnezoffii Preparata, Herba Ephedrae, Herba Asari, Rhizoma Et Radix Notopterygii, Radix Saposhnikoviae, Agkistrodon, Zaocys, Os Tigris, Colophonium, Rhizoma Drynariae (scalds, unhairing), Rhizoma Gastrodiae, Rhizoma Arisaematis (system), Scorpio, Bombyx Batryticatus, Pheretima, Radix Puerariae, Fructus Amomi Rotundus, Herba Pogostemonis, Rhizoma Osmundae, Radix Et Rhizoma Rhei, Rhizoma Coptidis, Radix Scutellariae, Radix Scrophulariae, Radix Clematidis carries out superfine grinding, and grinding particle size is the 10-200 micron; Except get Sanguis Draxonis, Rhizoma Arisaematis (system) mixed powder is broken into fine powder (putting in addition), outside Moschus, Borneolum Syntheticum, Calculus Bovis, the Pulvis Cornus Bubali Concentratus, all the other medicines are ground into fine powder and Calculus Bovis, Pulvis Cornus Bubali Concentratus facing-up, sieve, mixing.Get the 233g fine powder, 150 milliliters of 80% alcohol mixeding liquids of adding 15% (g/ml) refined honey are made soft material, cross 12 mesh sieves, low temperature 55-60 degree centigrade drying 4 hours, 16 mesh sieve granulate are in addition with Moschus and Borneolum Syntheticum porphyrize, make suspension with 25 milliliter of 60% ethanol grinding, spray is added in the above-mentioned granule, and mixing is flung to ethanol, make 1000 of capsules, and get final product.
Embodiment 16
More than 48 herbal medicines, Sanguis Draxonis wherein, Rhizoma Arisaematis (system), Radix Ginseng Rubra, the Rhizoma Atractylodis Macrocephalae, Radix Glycyrrhizae, Radix Rehmanniae Preparata, Radix Angelicae Sinensis, Radix Polygoni Multiflori, Carapax Et Plastrum Testudinis (vinegar system), Olibanum (system), Myrrha (processed), Sanguis Draxonis, Radix Paeoniae Rubra, Cortex Cinnamomi, Rhizoma Anemones Raddeanae, Benzoinum, Lignum Aquilariae Resinatum, the Radix Aucklandiae, Flos Caryophylli, Rhizoma Cyperi, the Radix Linderae, Pericarpium Citri Reticulatae Viride, Radix Aconiti Kusnezoffii Preparata, Herba Ephedrae, Herba Asari, Rhizoma Et Radix Notopterygii, Radix Saposhnikoviae, Agkistrodon, Zaocys, Os Tigris, Colophonium, Rhizoma Drynariae (scalds, unhairing), Rhizoma Gastrodiae, Rhizoma Arisaematis (system), Scorpio, Bombyx Batryticatus, Pheretima, Radix Puerariae, Fructus Amomi Rotundus, Herba Pogostemonis, Rhizoma Osmundae, Radix Et Rhizoma Rhei, Rhizoma Coptidis, Radix Scutellariae, Radix Scrophulariae, Radix Clematidis carries out superfine grinding, and grinding particle size is the 10-200 micron; Except get Sanguis Draxonis, Rhizoma Arisaematis (system) mixed powder is broken into fine powder (putting in addition), outside Moschus, Borneolum Syntheticum, Calculus Bovis, the Pulvis Cornus Bubali Concentratus, all the other medicines are ground into fine powder and Calculus Bovis, Pulvis Cornus Bubali Concentratus facing-up, sieve, mixing.Get the 233g fine powder, 150 milliliters of 80% alcohol mixeding liquids of adding 30% (g/ml) refined honey are made soft material, cross 12 mesh sieves, cold drying 5 hours, 16 mesh sieve granulate are in addition with Moschus and Borneolum Syntheticum porphyrize, make suspension with 25 milliliter of 80% ethanol grinding, spray is added in the above-mentioned granule, and mixing is flung to ethanol, make 1000 of capsules, and get final product.
Embodiment 17
More than 48 herbal medicines, Sanguis Draxonis wherein, Rhizoma Arisaematis (system), Radix Ginseng Rubra, the Rhizoma Atractylodis Macrocephalae, Radix Glycyrrhizae, Radix Rehmanniae Preparata, Radix Angelicae Sinensis, Radix Polygoni Multiflori, Carapax Et Plastrum Testudinis (vinegar system), Olibanum (system), Myrrha (processed), Sanguis Draxonis, Radix Paeoniae Rubra, Cortex Cinnamomi, Rhizoma Anemones Raddeanae, Benzoinum, Lignum Aquilariae Resinatum, the Radix Aucklandiae, Flos Caryophylli, Rhizoma Cyperi, the Radix Linderae, Pericarpium Citri Reticulatae Viride, Radix Aconiti Kusnezoffii Preparata, Herba Ephedrae, Herba Asari, Rhizoma Et Radix Notopterygii, Radix Saposhnikoviae, Agkistrodon, Zaocys, Os Tigris, Colophonium, Rhizoma Drynariae (scalds, unhairing), Rhizoma Gastrodiae, Rhizoma Arisaematis (system), Scorpio, Bombyx Batryticatus, Pheretima, Radix Puerariae, Fructus Amomi Rotundus, Herba Pogostemonis, Rhizoma Osmundae, Radix Et Rhizoma Rhei, Rhizoma Coptidis, Radix Scutellariae, Radix Scrophulariae, Radix Clematidis carries out superfine grinding, and grinding particle size is the 10-200 micron; Except get Sanguis Draxonis, Rhizoma Arisaematis (system) mixed powder is broken into fine powder (putting in addition), outside Moschus, Borneolum Syntheticum, Calculus Bovis, the Pulvis Cornus Bubali Concentratus, all the other medicines are ground into fine powder and Calculus Bovis, Pulvis Cornus Bubali Concentratus facing-up, sieve, mixing.Get the 233g fine powder, 150 milliliters of 80% alcohol mixeding liquids of adding 20% (g/ml) refined honey are made soft material, cross 12 mesh sieves, low temperature 55-60 degree centigrade drying 2 hours, 16 mesh sieve granulate are in addition with Moschus and Borneolum Syntheticum porphyrize, make suspension with 25 milliliters of dehydrated alcohol grindings, spray is added in the above-mentioned granule, and mixing is flung to ethanol, make 1000 of capsules, and get final product.
Embodiment 18
More than 48 herbal medicines, Sanguis Draxonis wherein, Rhizoma Arisaematis (system), Radix Ginseng Rubra, the Rhizoma Atractylodis Macrocephalae, Radix Glycyrrhizae, Radix Rehmanniae Preparata, Radix Angelicae Sinensis, Radix Polygoni Multiflori, Carapax Et Plastrum Testudinis (vinegar system), Olibanum (system), Myrrha (processed), Sanguis Draxonis, Radix Paeoniae Rubra, Cortex Cinnamomi, Rhizoma Anemones Raddeanae, Benzoinum, Lignum Aquilariae Resinatum, the Radix Aucklandiae, Flos Caryophylli, Rhizoma Cyperi, the Radix Linderae, Pericarpium Citri Reticulatae Viride, Radix Aconiti Kusnezoffii Preparata, Herba Ephedrae, Herba Asari, Rhizoma Et Radix Notopterygii, Radix Saposhnikoviae, Agkistrodon, Zaocys, Os Tigris, Colophonium, Rhizoma Drynariae (scalds, unhairing), Rhizoma Gastrodiae, Rhizoma Arisaematis (system), Scorpio, Bombyx Batryticatus, Pheretima, Radix Puerariae, Fructus Amomi Rotundus, Herba Pogostemonis, Rhizoma Osmundae, Radix Et Rhizoma Rhei, Rhizoma Coptidis, Radix Scutellariae, Radix Scrophulariae, Radix Clematidis carries out superfine grinding, and grinding particle size is the 10-200 micron; Except get Sanguis Draxonis, Rhizoma Arisaematis (system) mixed powder is broken into fine powder (putting in addition), outside Moschus, Borneolum Syntheticum, Calculus Bovis, the Pulvis Cornus Bubali Concentratus, all the other medicines are ground into fine powder and Calculus Bovis, Pulvis Cornus Bubali Concentratus facing-up, sieve, mixing.Get the 233g fine powder, 150 milliliters of 80% alcohol mixeding liquids of adding 10% (g/ml) refined honey are made soft material, cross 12 mesh sieves, low temperature 55-60 degree centigrade drying 3 hours, 16 mesh sieve granulate are in addition with Moschus and Borneolum Syntheticum porphyrize, make suspension with 25 milliliter of 85% ethanol grinding, spray is added in the above-mentioned granule, and mixing is flung to ethanol, make 1000 of capsules, and get final product.
Embodiment 19
More than 48 herbal medicines, Sanguis Draxonis wherein, Rhizoma Arisaematis (system), Radix Ginseng Rubra, the Rhizoma Atractylodis Macrocephalae, Radix Glycyrrhizae, Radix Rehmanniae Preparata, Radix Angelicae Sinensis, Radix Polygoni Multiflori, Carapax Et Plastrum Testudinis (vinegar system), Olibanum (system), Myrrha (processed), Sanguis Draxonis, Radix Paeoniae Rubra, Cortex Cinnamomi, Rhizoma Anemones Raddeanae, Benzoinum, Lignum Aquilariae Resinatum, the Radix Aucklandiae, Flos Caryophylli, Rhizoma Cyperi, the Radix Linderae, Pericarpium Citri Reticulatae Viride, Radix Aconiti Kusnezoffii Preparata, Herba Ephedrae, Herba Asari, Rhizoma Et Radix Notopterygii, Radix Saposhnikoviae, Agkistrodon, Zaocys, Os Tigris, Colophonium, Rhizoma Drynariae (scalds, unhairing), Rhizoma Gastrodiae, Rhizoma Arisaematis (system), Scorpio, Bombyx Batryticatus, Pheretima, Radix Puerariae, Fructus Amomi Rotundus, Herba Pogostemonis, Rhizoma Osmundae, Radix Et Rhizoma Rhei, Rhizoma Coptidis, Radix Scutellariae, Radix Scrophulariae, Radix Clematidis carries out superfine grinding, and grinding particle size is the 10-200 micron; Except get Sanguis Draxonis, Rhizoma Arisaematis (system) mixed powder is broken into fine powder (putting in addition), outside Moschus, Borneolum Syntheticum, Calculus Bovis, the Pulvis Cornus Bubali Concentratus, all the other medicines are ground into fine powder and Calculus Bovis, Pulvis Cornus Bubali Concentratus facing-up, sieve, mixing.Get the 233g fine powder, 150 milliliters of 80% alcohol mixeding liquids of adding 18% (g/ml) refined honey are made soft material, cross 12 mesh sieves, cold drying 2 hours, 16 mesh sieve granulate are in addition with Moschus and Borneolum Syntheticum porphyrize, make suspension with 25 milliliter of 95% ethanol grinding, spray is added in the above-mentioned granule, and mixing is flung to ethanol, make 1000 of capsules, and get final product.
Embodiment 20
More than 48 herbal medicines, Sanguis Draxonis wherein, Rhizoma Arisaematis (system), Radix Ginseng Rubra, the Rhizoma Atractylodis Macrocephalae, Radix Glycyrrhizae, Radix Rehmanniae Preparata, Radix Angelicae Sinensis, Radix Polygoni Multiflori, Carapax Et Plastrum Testudinis (vinegar system), Olibanum (system), Myrrha (processed), Sanguis Draxonis, Radix Paeoniae Rubra, Cortex Cinnamomi, Rhizoma Anemones Raddeanae, Benzoinum, Lignum Aquilariae Resinatum, the Radix Aucklandiae, Flos Caryophylli, Rhizoma Cyperi, the Radix Linderae, Pericarpium Citri Reticulatae Viride, Radix Aconiti Kusnezoffii Preparata, Herba Ephedrae, Herba Asari, Rhizoma Et Radix Notopterygii, Radix Saposhnikoviae, Agkistrodon, Zaocys, Os Tigris, Colophonium, Rhizoma Drynariae (scalds, unhairing), Rhizoma Gastrodiae, Rhizoma Arisaematis (system), Scorpio, Bombyx Batryticatus, Pheretima, Radix Puerariae, Fructus Amomi Rotundus, Herba Pogostemonis, Rhizoma Osmundae, Radix Et Rhizoma Rhei, Rhizoma Coptidis, Radix Scutellariae, Radix Scrophulariae, Radix Clematidis carries out superfine grinding, and grinding particle size is the 10-200 micron; Except get Sanguis Draxonis, Rhizoma Arisaematis (system) mixed powder is broken into fine powder (putting in addition), outside Moschus, Borneolum Syntheticum, Calculus Bovis, the Pulvis Cornus Bubali Concentratus, all the other medicines are ground into fine powder and Calculus Bovis, Pulvis Cornus Bubali Concentratus facing-up, sieve, mixing.Get the 233g fine powder, 150 milliliters of 80% alcohol mixeding liquids of adding 16% (g/ml) refined honey are made soft material, cross 12 mesh sieves, low temperature 55-60 degree centigrade drying 2 hours, 16 mesh sieve granulate are in addition with Moschus and Borneolum Syntheticum porphyrize, make suspension with 25 milliliter of 85% ethanol grinding, spray is added in the above-mentioned granule, and mixing is flung to ethanol, make 1000 of capsules, and get final product.
Embodiment 21
More than 48 herbal medicines, Sanguis Draxonis wherein, Rhizoma Arisaematis (system), Radix Ginseng Rubra, the Rhizoma Atractylodis Macrocephalae, Radix Glycyrrhizae, Radix Rehmanniae Preparata, Radix Angelicae Sinensis, Radix Polygoni Multiflori, Carapax Et Plastrum Testudinis (vinegar system), Olibanum (system), Myrrha (processed), Sanguis Draxonis, Radix Paeoniae Rubra, Cortex Cinnamomi, Rhizoma Anemones Raddeanae, Benzoinum, Lignum Aquilariae Resinatum, the Radix Aucklandiae, Flos Caryophylli, Rhizoma Cyperi, the Radix Linderae, Pericarpium Citri Reticulatae Viride, Radix Aconiti Kusnezoffii Preparata, Herba Ephedrae, Herba Asari, Rhizoma Et Radix Notopterygii, Radix Saposhnikoviae, Agkistrodon, Zaocys, Os Tigris, Colophonium, Rhizoma Drynariae (scalds, unhairing), Rhizoma Gastrodiae, Rhizoma Arisaematis (system), Scorpio, Bombyx Batryticatus, Pheretima, Radix Puerariae, Fructus Amomi Rotundus, Herba Pogostemonis, Rhizoma Osmundae, Radix Et Rhizoma Rhei, Rhizoma Coptidis, Radix Scutellariae, Radix Scrophulariae, Radix Clematidis carries out superfine grinding, and grinding particle size is the 10-200 micron; Except get Sanguis Draxonis, Rhizoma Arisaematis (system) mixed powder is broken into fine powder (putting in addition), outside Moschus, Borneolum Syntheticum, Calculus Bovis, the Pulvis Cornus Bubali Concentratus, all the other medicines are ground into fine powder and Calculus Bovis, Pulvis Cornus Bubali Concentratus facing-up, sieve, mixing.Get the 233g fine powder, 150 milliliters of 80% alcohol mixeding liquids of adding 22% (g/ml) refined honey are made soft material, cross 12 mesh sieves, low temperature 55-60 degree centigrade drying 3 hours, 16 mesh sieve granulate are in addition with Moschus and Borneolum Syntheticum porphyrize, make suspension with 25 milliliter of 75% ethanol grinding, spray is added in the above-mentioned granule, and mixing is flung to ethanol, make 1000 of capsules, and get final product.
Embodiment 22
More than 48 herbal medicines, Sanguis Draxonis wherein, Rhizoma Arisaematis (system), Radix Ginseng Rubra, the Rhizoma Atractylodis Macrocephalae, Radix Glycyrrhizae, Radix Rehmanniae Preparata, Radix Angelicae Sinensis, Radix Polygoni Multiflori, Carapax Et Plastrum Testudinis (vinegar system), Olibanum (system), Myrrha (processed), Sanguis Draxonis, Radix Paeoniae Rubra, Cortex Cinnamomi, Rhizoma Anemones Raddeanae, Benzoinum, Lignum Aquilariae Resinatum, the Radix Aucklandiae, Flos Caryophylli, Rhizoma Cyperi, the Radix Linderae, Pericarpium Citri Reticulatae Viride, Radix Aconiti Kusnezoffii Preparata, Herba Ephedrae, Herba Asari, Rhizoma Et Radix Notopterygii, Radix Saposhnikoviae, Agkistrodon, Zaocys, Os Tigris, Colophonium, Rhizoma Drynariae (scalds, unhairing), Rhizoma Gastrodiae, Rhizoma Arisaematis (system), Scorpio, Bombyx Batryticatus, Pheretima, Radix Puerariae, Fructus Amomi Rotundus, Herba Pogostemonis, Rhizoma Osmundae, Radix Et Rhizoma Rhei, Rhizoma Coptidis, Radix Scutellariae, Radix Scrophulariae, Radix Clematidis carries out superfine grinding, and grinding particle size is the 10-200 micron; Except get Sanguis Draxonis, Rhizoma Arisaematis (system) mixed powder is broken into fine powder (putting in addition), outside Moschus, Borneolum Syntheticum, Calculus Bovis, the Pulvis Cornus Bubali Concentratus, all the other medicines are ground into fine powder and Calculus Bovis, Pulvis Cornus Bubali Concentratus facing-up, sieve, mixing.Get the 233g fine powder, 150 milliliters of 80% alcohol mixeding liquids of adding 14% (g/ml) refined honey are made soft material, cross 12 mesh sieves, cold drying 3 hours, 16 mesh sieve granulate are in addition with Moschus and Borneolum Syntheticum porphyrize, make suspension with 25 milliliter of 65% ethanol grinding, spray is added in the above-mentioned granule, and mixing is flung to ethanol, make 1000 of capsules, and get final product.
Embodiment 23
More than 48 herbal medicines, Sanguis Draxonis wherein, Rhizoma Arisaematis (system), Radix Ginseng Rubra, the Rhizoma Atractylodis Macrocephalae, Radix Glycyrrhizae, Radix Rehmanniae Preparata, Radix Angelicae Sinensis, Radix Polygoni Multiflori, Carapax Et Plastrum Testudinis (vinegar system), Olibanum (system), Myrrha (processed), Sanguis Draxonis, Radix Paeoniae Rubra, Cortex Cinnamomi, Rhizoma Anemones Raddeanae, Benzoinum, Lignum Aquilariae Resinatum, the Radix Aucklandiae, Flos Caryophylli, Rhizoma Cyperi, the Radix Linderae, Pericarpium Citri Reticulatae Viride, Radix Aconiti Kusnezoffii Preparata, Herba Ephedrae, Herba Asari, Rhizoma Et Radix Notopterygii, Radix Saposhnikoviae, Agkistrodon, Zaocys, Os Tigris, Colophonium, Rhizoma Drynariae (scalds, unhairing), Rhizoma Gastrodiae, Rhizoma Arisaematis (system), Scorpio, Bombyx Batryticatus, Pheretima, Radix Puerariae, Fructus Amomi Rotundus, Herba Pogostemonis, Rhizoma Osmundae, Radix Et Rhizoma Rhei, Rhizoma Coptidis, Radix Scutellariae, Radix Scrophulariae, Radix Clematidis carries out superfine grinding, and grinding particle size is the 10-200 micron; Except get Sanguis Draxonis, Rhizoma Arisaematis (system) mixed powder is broken into fine powder (putting in addition), outside Moschus, Borneolum Syntheticum, Calculus Bovis, the Pulvis Cornus Bubali Concentratus, all the other medicines are ground into fine powder and Calculus Bovis, Pulvis Cornus Bubali Concentratus facing-up, sieve, mixing.Get the 233g fine powder, 150 milliliters of 80% alcohol mixeding liquids of adding 15% (g/ml) refined honey are made soft material, cross 12 mesh sieves, low temperature 55-60 degree centigrade drying 4 hours, 16 mesh sieve granulate are in addition with Moschus and Borneolum Syntheticum porphyrize, make suspension with 25 milliliter of 50% ethanol grinding, spray is added in the above-mentioned granule, and mixing is flung to ethanol, make 1000 of capsules, and get final product.
Embodiment 24
More than 48 herbal medicines, Sanguis Draxonis wherein, Rhizoma Arisaematis (system), Radix Ginseng Rubra, the Rhizoma Atractylodis Macrocephalae, Radix Glycyrrhizae, Radix Rehmanniae Preparata, Radix Angelicae Sinensis, Radix Polygoni Multiflori, Carapax Et Plastrum Testudinis (vinegar system), Olibanum (system), Myrrha (processed), Sanguis Draxonis, Radix Paeoniae Rubra, Cortex Cinnamomi, Rhizoma Anemones Raddeanae, Benzoinum, Lignum Aquilariae Resinatum, the Radix Aucklandiae, Flos Caryophylli, Rhizoma Cyperi, the Radix Linderae, Pericarpium Citri Reticulatae Viride, Radix Aconiti Kusnezoffii Preparata, Herba Ephedrae, Herba Asari, Rhizoma Et Radix Notopterygii, Radix Saposhnikoviae, Agkistrodon, Zaocys, Os Tigris, Colophonium, Rhizoma Drynariae (scalds, unhairing), Rhizoma Gastrodiae, Rhizoma Arisaematis (system), Scorpio, Bombyx Batryticatus, Pheretima, Radix Puerariae, Fructus Amomi Rotundus, Herba Pogostemonis, Rhizoma Osmundae, Radix Et Rhizoma Rhei, Rhizoma Coptidis, Radix Scutellariae, Radix Scrophulariae, Radix Clematidis carries out superfine grinding, and grinding particle size is the 10-200 micron; Except get Sanguis Draxonis, Rhizoma Arisaematis (system) mixed powder is broken into fine powder (putting in addition), outside Moschus, Borneolum Syntheticum, Calculus Bovis, the Pulvis Cornus Bubali Concentratus, all the other medicines are ground into fine powder and Calculus Bovis, Pulvis Cornus Bubali Concentratus facing-up, sieve, mixing.Get the 233g fine powder, 150 milliliters of 80% alcohol mixeding liquids of adding 15% (g/ml) refined honey are made soft material, cross 12 mesh sieves, low temperature 55-60 degree centigrade drying 5.5 hours, 16 mesh sieve granulate are in addition with Moschus and Borneolum Syntheticum porphyrize, make suspension with 20 milliliter of 50% ethanol grinding, spray is added in the above-mentioned granule, and mixing is flung to ethanol, make 1000 of capsules, and get final product.
The optimization Test of experimental example-preparation method of the present invention
More than 48 flavor medicines according to " the various kinds of 95 editions one of Chinese pharmacopoeia concoct a lower regulation and " the medicinal material processing general rule regulation of 95 editions one appendix II D of Chinese pharmacopoeia is concocted.Show that through test of many times the average flour extraction after the pulverizing medicinal materials is 90.45%.
Table 2 medical material flour extraction statistical table
Sanguis Draxonis, flour extraction after Rhizoma Arisaematis is pulverized:
Table 3 Sanguis Draxonis and Rhizoma Arisaematis flour extraction statistical table
The many prescriptions of we's flavour of a drug are large, wherein contain animal drugs, plant amedica, valuable medicinal etc., through test of many times, adopt the Orthogonal Experiment and Design effective component extracting to be difficult to prove effective, for fear of the loss of effective ingredient at extraction, concentration process, affect the treatment, granulate filling capsule technique so in preparation process, determine former powder.
According to the characteristics that the former powder of this capsule is granulated, through the test of many times checking, this Traditional Chinese medicine capsule material contains the medical material of volatile ingredient, and baking temperature is 55-60 degree centigrade, and the oven dry grain thickness is 0.5 centimetre, stirs once every one hour.
The present invention selectes concentration of alcohol, refined honey concentration and drying time as the factor level analysis of granulate quality:
Table 4 factor level table
Table 5L
9(3
3) orthogonal test table
The relevant explanation of table 5:
1. granule qualification rate: greater than 90% being 100 minutes, every decline 1% was detained 2 minutes.
2. moisture content: take 5% as 100 minutes, every rising or descend 0.1% was detained 1 minute.
3. content weight: 20 capsules are average, and 0.25 gram is 100 minutes, and every rising or 0.0 gram that descends were detained 10 minutes.
4. can know from table 5 that refined honey is dense has a significant effect to processing quality, for pelletization control, refined honey in the pelletization is controlled, and 10 batches of moisture determinations are as follows
5. refined honey concentration refers to that 100 milliliter of 80 ethanol adds the grams of refined honey.
6. be in order to guarantee capsule fill specification homogeneous and Moschus to half finished particle control, Borneolum Syntheticum is uniformly dispersed, qualified granule refer to by 16 mesh sieves can not be by 65 mesh sieves particle weight in the ratio of granule total amount, the granule qualification rate should be controlled at more than 90%.
In order to ensure moisture content of finished products in prescribed limit, avoid drying once again the loss that causes Moschus and Borneolum Syntheticum, it is 5% more suitable to determine that half-finished pellet moisture is controlled at.
8. factorial analysis, table 5 can find out that optimum process condition is A
2B
1C
2, namely concentration of alcohol 80%, refined honey 15%, dry 3 hours.Influence factor's size is that refined honey concentration is most important, and take second place drying time, and concentration of alcohol again.
Claims (1)
1. the granulation drying means of a Da huoluo capsule, wherein said Da huoluo capsule prescription be,
Wherein the Rhizoma Drynariae method for making is for scalding unhairing processed, it is characterized in that, employing following methods preparation: above 48 herbal medicines, get Sanguis Draxonis, Rhizoma Arisaematis (system) and mix that to carry out grinding particle size be that 10-200 micron micropowder is broken into fine powder, Moschus, Borneolum Syntheticum, Calculus Bovis, Pulvis Cornus Bubali Concentratus, all the other medicines carry out superfine grinding, and grinding particle size is the 10-200 micron, with Calculus Bovis, Pulvis Cornus Bubali Concentratus facing-up, sieve, mixing; Get the 233g fine powder, add 150 milliliters of 15%g/ml refined honey and 80% alcohol mixeding liquids, make soft material, cross 12 mesh sieves, drying is made suspension with Moschus and Borneolum Syntheticum with 25 milliliter of 60% ethanol grinding in addition, spray is added in the above-mentioned granule, and mixing is flung to ethanol, make 1000 of capsules, and get final product, it is characterized in that described drying process is: 55-60 degree centigrade cold drying 2-6 hour, stirred once every 1 hour, 16 mesh sieve granulate, wherein drying grain thickness is 0.5 centimetre.
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