CN101376570B - Treating compound special for high textile performance weft yarn and preparation thereof - Google Patents
Treating compound special for high textile performance weft yarn and preparation thereof Download PDFInfo
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- CN101376570B CN101376570B CN 200810156013 CN200810156013A CN101376570B CN 101376570 B CN101376570 B CN 101376570B CN 200810156013 CN200810156013 CN 200810156013 CN 200810156013 A CN200810156013 A CN 200810156013A CN 101376570 B CN101376570 B CN 101376570B
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Abstract
The invention discloses a special treating compound for weft yarn with high spinning performance, and a preparation method thereof. The special treating compound comprises a polyester emulsion, an epoxy emulsion, water-based epoxy, a lubricant, a coupling agent, glacial acetic acid and water in balancing amount, which are respectively subjected to the dispersion of the coupling agent, the dilution of the water-based epoxy, the dilution of the polyester emulsion, the dilution of the epoxy emulsion and the dilution of the lubricant, and then added into a preparation tank in sequence; and the residual water is added until the total amount is reached, and the stirring-up is carried out for 15 minutes. The treating compound endows the yarn with good convergence, ensures the smooth glass fiber drawing progress, and has excellent spinning performance; the abrasion of the fiber precursors is less during the spinning process; the wool yarn of the cloth cover is less, the compatibility with the back resin is good; the strength of the cloth cover is good; besides, the preparation process is simple, and the operation is easy.
Description
Technical field
The present invention relates to a kind for the treatment of compound, especially a kind of weft yarn sizing agent special and preparation method thereof with high textile performance.
Background technology
In the prior art, treating compound is vital production material in glass fiber wire-drawing, winding process, directly the quality quality to glass fibre plays a decisive role, if the quality for the treatment of compound can not get guaranteeing, weft yarn wool yarn in the process of weaving cotton cloth is many, the operation yield rate is low, the waste big, and intensity is also low.
Summary of the invention
The invention provides weft yarn sizing agent special of a kind of high textile performance and preparation method thereof.
In order to solve above technical problem, the weft yarn sizing agent special of a kind of high textile performance of the present invention comprises following component: press the 100Kg treating compound and calculate, polyester emulsion 4-5%, epoxy emulsion 2-2.5%, water-base epoxy 1-1.5%, lubricant 0.4-0.5%, coupling agent 0.3-0.5%, Glacial acetic acid 0.2%, all the other are water; The preparation of the weft yarn sizing agent special of high textile performance realizes by following preparation process:
A. the dispersing method of coupling agent: in the premix still, put into water as much as possible, add Glacial acetic acid and regulate its pH value 3.5-4, under stirring state, slowly add coupling agent and stir more than 30 minutes, treat the solution clarification, the no oil bloom shape in surface, promptly accuse hydrolysis and finish, survey the solution pH value this moment again, make it≤and 6, if excessive, but a little adds Glacial acetic acid;
B. the dilution of water-base epoxy: with about 3 times water dilution of its weight, after stirring, pour reactor into, stir;
C. the dilution of polyester emulsion: with about 3 times water dilution of polyester emulsion weight, after stirring, pour reactor into, stir;
D. the dilution of epoxy emulsion: with about 3 times water dilution of epoxy emulsion weight, after stirring, pour reactor into, stir;
E. the dilution of lubricant: the warm water of 60 ℃ about 10 of weight times dilution with lubricator, after stirring, pour reactor into, stir;
F. above-mentioned dilution is good A, B, C, D, E order add in the preparing tank successively;
G. the water that adds surplus stirs after 15 minutes to total amount, and is stand-by.
The invention has the advantages that: this treating compound can be given the good convergency of yarn and guarantee carrying out smoothly of glass fiber wire-drawing and have excellent textile performance, the precursor wearing and tearing are few in the weaving process, the cloth cover wool yarn is few and good with the consistency of road, back resin, and the cloth cover brute force is good; And preparation technology is simple, and is easy to operate.
Embodiment
Embodiment 1
The weft yarn sizing agent special of high textile performance is by polyester emulsion, epoxy emulsion, water-base epoxy, lubricant, coupling agent, Glacial acetic acid, water is formed, pressing the 100Kg treating compound calculates, the weight of its component is followed successively by: polyester emulsion 4.5kg, epoxy emulsion 2kg, water-base epoxy 1.2kg, lubricant 0.4kg, coupling agent 0.4kg, Glacial acetic acid 0.2%, all the other are water.
The preparation method of the weft yarn sizing agent special treating compound of described high textile performance, realize by following preparation process:
The dispersing method of A, coupling agent: in the premix still, put into water as much as possible, add Glacial acetic acid 0.2% and regulate its pH value 3.5-4, under stirring state, slowly add coupling agent 0.4kg and stir more than 30 minutes, treat the solution clarification, the no oil bloom shape in surface, promptly accuse hydrolysis and finish, survey the solution pH value this moment again, make it≤and 6, if excessive, but a little adds Glacial acetic acid;
The dilution of B, water-base epoxy: with about 3 times the water dilution of water-base epoxy 1.2kg, after stirring, pour reactor into, stir with its weight;
The dilution of C, polyester emulsion: with about 3 times the water dilution of polyester emulsion 4.5kg, after stirring, pour reactor into, stir with its weight;
The dilution of D, epoxy emulsion: with about 3 times the water dilution of epoxy emulsion 2kg, after stirring, pour reactor into, stir with its weight;
The dilution of E, lubricant: with about 10 times 60 ℃ the warm water dilution of lubricant 0.4kg, after stirring, pour reactor into, stir with its weight;
F, A, B, C, D, the E order that above-mentioned dilution is good add in the preparing tank successively;
The water of G, adding surplus stirs after 15 minutes to total amount, and is stand-by.
According to test, the weft yarn that makes reaches 0.45N/tex than brute force, and the grey cloth weft direction reaches 2000N/50mm than brute force, and last adhesive plaster weft direction reaches 3500N/50mm than brute force.
Embodiment 2
The weft yarn sizing agent special of high textile performance is by polyester emulsion, epoxy emulsion, water-base epoxy, lubricant, coupling agent, Glacial acetic acid, water is formed, pressing the 100Kg treating compound calculates, the weight of its component is followed successively by: polyester emulsion 4.8kg, epoxy emulsion 2.2kg, water-base epoxy 1.5kg, lubricant 0.5kg, coupling agent 0.45kg, Glacial acetic acid 0.2%, all the other are water.
The preparation method of the weft yarn sizing agent special treating compound of described high textile performance, realize by following preparation process:
The dispersing method of H, coupling agent: in the premix still, put into water as much as possible, add Glacial acetic acid 0.2% and regulate its pH value 3.5-4, under stirring state, slowly add coupling agent 0.45kg and stir more than 30 minutes, treat the solution clarification, the no oil bloom shape in surface, promptly accuse hydrolysis and finish, survey the solution pH value this moment again, make it≤and 6, if excessive, but a little adds Glacial acetic acid;
The dilution of I, water-base epoxy: with about 3 times the water dilution of water-base epoxy 1.5kg, after stirring, pour reactor into, stir with its weight;
The dilution of J, polyester emulsion: with about 3 times the water dilution of polyester emulsion 4.8kg, after stirring, pour reactor into, stir with its weight;
The dilution of K, epoxy emulsion: with about 3 times the water dilution of epoxy emulsion 2.2kg, after stirring, pour reactor into, stir with its weight;
The dilution of L, lubricant: with about 10 times 60 ℃ the warm water dilution of lubricant 0.5kg, after stirring, pour reactor into, stir with its weight;
M, A, B, C, D, the E order that above-mentioned dilution is good add in the preparing tank successively;
The water of N, adding surplus stirs after 15 minutes to total amount, and is stand-by.
According to test, the weft yarn that makes reaches 0.45N/tex than brute force, and the grey cloth weft direction reaches 2000N/50mm than brute force, and last adhesive plaster weft direction reaches 3500N/50mm than brute force.
Claims (2)
1. the weft yarn sizing agent special of a high textile performance, it is characterized in that: described treating compound comprises following component: press the 100Kg treating compound and calculate, polyester emulsion 4-5%, epoxy emulsion 2-2.5%, water-base epoxy 1-1.5%, lubricant 0.4-0.5%, coupling agent 0.3-0.5%, Glacial acetic acid 0.2%, all the other are water.
2. the preparation method of the weft yarn sizing agent special of high textile performance according to claim 1 is characterized in that: be to realize through following preparation process:
A. the dispersing method of coupling agent: in the premix still, put into water, add Glacial acetic acid and regulate the pH value 3.5-4 of solution in the premix still, under stirring state, slowly add coupling agent and stir more than 30 minutes, treat the solution clarification, the no oil bloom shape in surface, promptly accuse hydrolysis and finish, survey the pH value of solution value this moment again, make it≤and 6, if excessive, add Glacial acetic acid;
B. the dilution of water-base epoxy: 3 times water dilution of use epoxy weight, after stirring, pour reactor into, stir;
C. the dilution of polyester emulsion: with 3 times water dilution of polyester emulsion weight, after stirring, pour reactor into, stir;
D. the dilution of epoxy emulsion: with 3 times water dilution of epoxy emulsion weight, after stirring, pour reactor into, stir;
E. the dilution of lubricant: 60 ℃ of 10 of weight times warm water dilution with lubricator, after stirring, pour reactor into, stir;
F. above-mentioned dilution is good A, B, C, D, E order add in the preparing tank successively;
G. the water that adds surplus stirs after 15 minutes to total amount, and is stand-by.
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| Application Number | Priority Date | Filing Date | Title |
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| CN 200810156013 CN101376570B (en) | 2008-09-26 | 2008-09-26 | Treating compound special for high textile performance weft yarn and preparation thereof |
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| CN 200810156013 CN101376570B (en) | 2008-09-26 | 2008-09-26 | Treating compound special for high textile performance weft yarn and preparation thereof |
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| CN101376570A CN101376570A (en) | 2009-03-04 |
| CN101376570B true CN101376570B (en) | 2011-06-15 |
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Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102603212A (en) * | 2011-12-06 | 2012-07-25 | 巨石攀登电子基材有限公司 | Formula and production method of electronic grade glass fiber cloth treatment agent |
| CN103466966A (en) * | 2012-06-07 | 2013-12-25 | 天津市硅酸盐研究所 | Impregnating compound for enhancing quartz fiber tensile strength |
| CN104556739A (en) * | 2014-06-30 | 2015-04-29 | 江苏九鼎新材料股份有限公司 | Special alkali-free direct yarn wetting agent for grinding wheel reinforcing sheets and preparation method thereof |
| CN104440613B (en) * | 2014-09-30 | 2018-01-19 | 江苏九鼎新材料股份有限公司 | High-strength glass fibre strengthens emery wheel screen cloth and mesh sheet |
| CN108516703B (en) * | 2018-05-31 | 2021-03-30 | 九江鑫星玻纤材料有限公司 | Preparation method of glass fiber impregnating compound |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4933381A (en) * | 1987-08-27 | 1990-06-12 | Owens-Corning Fiberglas Corporation | Resin compatible size composition for small diameter glass fibers |
| CN1923740A (en) * | 2006-09-13 | 2007-03-07 | 中材科技股份有限公司 | Enhancement soakage agent for thin glass fiber bulked yarn |
| CN101092291A (en) * | 2007-06-12 | 2007-12-26 | 巨石集团有限公司 | High performance jetting treating compound for twistless roving |
| CN101100355A (en) * | 2007-06-12 | 2008-01-09 | 巨石集团有限公司 | Soaking agent capable of increasing glass fiber acid resistance |
-
2008
- 2008-09-26 CN CN 200810156013 patent/CN101376570B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4933381A (en) * | 1987-08-27 | 1990-06-12 | Owens-Corning Fiberglas Corporation | Resin compatible size composition for small diameter glass fibers |
| CN1923740A (en) * | 2006-09-13 | 2007-03-07 | 中材科技股份有限公司 | Enhancement soakage agent for thin glass fiber bulked yarn |
| CN101092291A (en) * | 2007-06-12 | 2007-12-26 | 巨石集团有限公司 | High performance jetting treating compound for twistless roving |
| CN101100355A (en) * | 2007-06-12 | 2008-01-09 | 巨石集团有限公司 | Soaking agent capable of increasing glass fiber acid resistance |
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