CN101353252B - Functional ceramic ornament, preparation and use thereof - Google Patents
Functional ceramic ornament, preparation and use thereof Download PDFInfo
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- CN101353252B CN101353252B CN 200710130793 CN200710130793A CN101353252B CN 101353252 B CN101353252 B CN 101353252B CN 200710130793 CN200710130793 CN 200710130793 CN 200710130793 A CN200710130793 A CN 200710130793A CN 101353252 B CN101353252 B CN 101353252B
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Abstract
The invention relates to a ceramic ornament with biological activation function. The ornament is made from 1-30wt% of ceramic powder material with the biological activation function and 70-99wt% of common silicon rubber particles. The ceramic ornament is characterized by activating amino acid molecules, improving the microcirculation of human body, having beautiful appearance as well as having a certain health care and beautifying effect on the human body. The invention also relates to a preparation method of the ceramic ornament and the application thereof.
Description
Technical field
The present invention relates to a kind of ceramic ornament, particularly a kind of functional ceramic ornament and its preparation method and application.
Background technology
General ceramic ornament only adopts ceramic material chain pendant or ornament, only in order to reach effect attractive in appearance.Along with the growing interest of people to beauty treatment and health care, people also no longer rest on the requirement of ceramic ornament has simple decoration functions, further has the beauty and health care function when gradually it being had decoration function and expresses expectation.Therefore, be necessary to provide a kind of new ceramic ornament to satisfy people's demand.The present invention proposes under above-mentioned background just.
Summary of the invention
The object of the present invention is to provide a kind of novel ceramic ornament with bioactivation function, make it to have the bioactivation function, can play to human body the effect of health and beauty.
The objective of the invention is to be achieved through the following technical solutions:
A kind of functional ceramic ornament is provided, is prepared from by the ceramic powder material with bioactivation function of 1～30% weight percent and the common silica gel particle of 70～99% weight percents.
Described ceramic powder material with bioactivation function is made by the raw material of following weight percent: far-infrared functional ceramic 20～45%, magneticsubstance 20～45%, rare-earth mineral material 2～10%, matrix material 5～30% and inorganic antibacterial material 1～3%.The particle diameter of all raw materials all is not less than 200 orders, is the commercially available prod.
Described far-infrared functional ceramic is one or more the mixture in iron tourmaline, dravite, iron dravite, elbaite, iron elbaite or the quartz; Described magneticsubstance is one or more the composition in ferrite, strontium ferrites or the neodymium iron boron; Described rare-earth mineral material is one or more the composition in quartz porphyry, marble porphyry, monazite, grouan, granite pegmatite, Cerium monophosphate ytterbium ore deposit or the Cerium monophosphate lanthanum ore deposit; Described matrix material is one or both the composition in wilkinite or the Suzhou soil; Described inorganic antibacterial material is any one in the inorganic antibacterial material of argentiferous or the inorganic antibacterial material that contains rare earth.
The weight percent of silver is 0.25～3.0% in the inorganic antibacterial material of described argentiferous; The described weight percent that contains the inorganic antibacterial material middle-weight rare earths of rare earth is 0.25～15.0%.
Described ceramic powder material meso-position radius (D50) with bioactivation function is 0.2～8.0 micron.Described ceramic powder material with bioactivation function is prepared by following steps:
(1) with the raw material ball mill mixing of above-mentioned weight percent, make the diameter of particle that obtains be not less than 325 orders;
(2) in the powder of step (1) preparation, evenly spray the clear water that accounts for powder weight 0.5～2.0%;
(3) with the powder moulding of pressing machine with step (2) preparation, make ceramic body;
(4) with the base substrate of step (3) preparation 850～1200 degrees centigrade of sintering 1.5～4 hours, make ceramic sintered bodies;
(5) ceramic sintered bodies of step (4) preparation is broken, pulverize, grind, make meso-position radius (D50) and be 0.2～8.0 micron the ceramic powder material with bioactivation function.
Described common silica gel particle is the commercially available prod.
The preparation method of described functional ceramic ornament may further comprise the steps:
(1) the common silica gel particle of described weight percent is mixed with the ceramic powder material with bioactivation function is placed in the encloses container;
(2) mixture in step (1) encloses container is heated to 100～200 degrees centigrade under 2～4 normal atmosphere, heated 1.5～3 hours, make it fully melt-blended;
(3) will extrude by the mixture of step (2) fusing by mould outlet, approximately after 2 hours, cooling forming gets final product under physical environment in heating in 100 degrees centigrade of water vapour.
The described encloses container of step (1) is heating kettle or pressure cooker.
The described mould outlet of step (3) is rope form or band shape.
The pressure of ratio, Heating temperature, heat-up time and pressurization by adjusting starting materials can be adjusted hardness and the toughness of ropy or the ribbon of final production.With ropy or the ribbon that this method is produced, additional cochain pendant or ornament can form bioactivation function porcelain particle ornaments.
The present invention also provides the application of described functional ceramic ornament aspect the body-care beauty treatment.
Described application is described functional ceramic ornament further to be processed into necklace, bracelet, bangle or bracelet wear in body local.
Compare with existing conventional ceramic ornaments, functional ceramic ornament of the present invention is owing to having adopted the ceramic powder material with bioactivation function, therefore have the activated amino acid molecule, improve microcirculatory characteristic, in attractive in appearance, can play certain health and beauty to human body.
The experiment of ornaments activated amino acid molecule of the present invention:
Functional ceramic ornament with the embodiment of the invention 1～3 preparation carries out the test of activated amino acid molecule.
Method: above-mentioned ornaments are placed testee's left hand third finger front and back contact 15 minutes, measure blood vessel, the blood parameters of nail fold microcirculation.
Result: the results are shown in Table 1 and Fig. 1～4, data can be found out from image and table: functional ceramic ornament of the present invention has significant activation to amino acid molecular, can play certain improvement effect to microcirculation, be mainly reflected in vasodilation, improve the aspects such as velocity of blood flow.
Table 1. functional ceramic ornament of the present invention acts on before and after testee's left hand third finger
Blood vessel, the blood parameters of (after 15 minutes) nail fold microcirculation test
| Input tap footpath (micron) | Output tap footpath (micron) | Flow velocity (little meter per second) | |
| Blank | 6.51 | 7.66 | 840 |
| Embodiment 1 | 9.39 | 12.94 | 858 |
| Embodiment 2 | 9.45 | 10.62 | 907 |
| Embodiment 3 | 9.38 | 12.95 | 858 |
Description of drawings
Fig. 1 is the image of the unknown nail folds in a garment of blank group testee left hand under micro-circle microscope.
Fig. 2 is that the functional ceramic ornament of embodiment 1 acts on testee's left hand its first folds in a garment image under micro-circle microscope after nameless 15 minutes.
Fig. 3 is that the functional ceramic ornament of embodiment 2 acts on testee's left hand its first folds in a garment image under micro-circle microscope after nameless 15 minutes.
Fig. 4 is that the functional ceramic ornament of embodiment 3 acts on testee's left hand its first folds in a garment image under micro-circle microscope after nameless 15 minutes.
Embodiment
Embodiment 1.
1. preparation functional ceramic powder material: with iron tourmaline powder 40 grams, ferrite powder 30 grams, quartz porphyry powder 8 grams, Suzhou soil powder 20 grams, argentiferous 0.5% silicate inorganic antibacterial material powder 2 grams, be placed in the ball mill ball milling 4 hours, mix, make diameter of particle reach 325 orders.In above-mentioned powder, evenly spray the clear water of 0.8 gram; With the powder moulding, make the ceramic plate base substrate of 50 millimeters of diameters, 6 millimeters of thickness with pressing machine; Base substrate 930 degrees centigrade of sintering 4 hours, is made ceramic sintered bodies; Ceramic sintered bodies is broken, pulverize, grind, make meso-position radius (D50) and be 3.4 microns functional ceramic powder material.
2. the ceramic powder material of above-mentioned steps 1 preparation is mixed with 9.9 kilograms of common silica gel and place heating kettle, under 2 normal atmosphere, heat to 110 degrees centigrade, heated 1.5 hours, make it fully melt-blended, then extrude by the rope form mould outlet, heating is approximately after 2 hours in 100 degrees centigrade of water vapour, cooling forming under physical environment.
3. the rope form ornaments with step 2 preparation further are equipped with pendant, make necklace and wear in order to neck.
Embodiment 2.
1. preparation functional ceramic powder material: with quartzy powder 22 grams, neodymium iron boron powder 45 grams, Cerium monophosphate ytterbium breeze body 3 grams, Suzhou soil powder 27 grams, argentiferous 0.5%, contain cerium 0.5% phosphate-based silicate inorganic antibacterial material powder 3 and restrain, be placed in the ball mill ball milling 4 hours, mix, make diameter of particle reach 325 orders.In above-mentioned powder, evenly spray the clear water of 0.8 gram; With the powder moulding, make the ceramic plate base substrate of 50 millimeters of diameters, 6 millimeters of thickness with pressing machine; Base substrate 1050 degrees centigrade of sintering 2.5 hours, is made ceramic sintered bodies; Ceramic sintered bodies is broken, pulverize, grind, make meso-position radius (D50) and be 1.93 microns functional ceramic powder material.
2. the ceramic powder material and 400 of above-mentioned steps 1 preparation being restrained common silica gel mixes and places pressure cooker, under 3 normal atmosphere, heat to 150 degrees centigrade, heated 1.5 hours, make it fully melt-blended, then extrude by banded mould outlet, heating is approximately after 2 hours in 100 degrees centigrade of water vapour, cooling forming under physical environment.
3. the banded ornaments of step 2 preparation are further interspersed floriation, make bracelet, wear in order to wrist.
Embodiment 3.
1. preparation functional ceramic powder material: with iron dravite powder 45 grams, ferrite powder 25 grams, Cerium monophosphate lanthanum breeze body 10 grams, Suzhou soil powder 18.5 grams, argentiferous 0.5%, contain cerium 0.25% phosphate-based inorganic antibacterial material powder 1.5 and restrain, be placed in the ball mill ball milling 4 hours, mix, make diameter of particle reach 325 orders.In above-mentioned powder, evenly spray the clear water of 1.2 grams; With the powder moulding, make the ceramic plate base substrate of 50 millimeters of diameters, 6 millimeters of thickness with pressing machine; Base substrate 850 degrees centigrade of sintering 4 hours, is made ceramic sintered bodies; Ceramic sintered bodies is broken, pulverize, grind, make meso-position radius (D50) and be 4.5 microns functional ceramic powder material.
2. the ceramic powder material and 250 of above-mentioned steps 1 preparation being restrained common silica gel mixes and places heating kettle, under 4 normal atmosphere, heat to 200 degrees centigrade, heated 3 hours, make it fully melt-blended, then extrude by banded mould outlet, heating is approximately after 2 hours in 100 degrees centigrade of water vapour, cooling forming under physical environment.
3. with the further boudle thing of banded ornaments of step 2 preparation, make bangle, wear in order to wrist.
Claims (7)
1. a functional ceramic ornament is characterized in that it is prepared from by the ceramic powder material with bioactivation function of 1～30% weight percent and the common silica gel particle of 70～99% weight percents; Described ceramic powder material with bioactivation function is made by the raw material of following weight percent: far-infrared functional ceramic 20～45%, magneticsubstance 20～45%, rare-earth mineral material 2～10%, matrix material 5～30% and inorganic antibacterial material 1～3%; Described far-infrared functional ceramic is one or both the mixture in iron dravite or the iron elbaite; Described magneticsubstance is one or more the composition in ferrite, strontium ferrites or the neodymium iron boron; Described matrix material is one or both the composition in wilkinite or the Suzhou soil; Described inorganic antibacterial material is Inorganic Antibacterial Material Carrying Silver; Described rare-earth mineral material is one or more the composition in quartz porphyry, marble porphyry, monazite, grouan, granite pegmatite, Cerium monophosphate ytterbium ore deposit or the Cerium monophosphate lanthanum ore deposit; The weight percent of silver is 0.25～3.0% in the described Inorganic Antibacterial Material Carrying Silver.
2. functional ceramic ornament claimed in claim 1, it is characterized in that: described ceramic powder material meso-position radius with bioactivation function is 0.2～8.0 micron.
3. the preparation method of functional ceramic ornament claimed in claim 1 may further comprise the steps:
(1) the common silica gel particle of described weight percent is mixed with the ceramic powder material with bioactivation function is placed in the encloses container;
(2) mixture in step (1) encloses container is heated to 100～200 degrees centigrade under 2～4 normal atmosphere, heated 1.5～3 hours, make it fully melt-blended;
(3) will extrude by the mixture of step (2) fusing by mould outlet, heating is after 2 hours in 100 degrees centigrade of water vapour, and cooling forming gets final product under physical environment.
4. the preparation method of functional ceramic ornament claimed in claim 3, it is characterized in that: the described encloses container of step (1) is heating kettle or pressure cooker.
5. the preparation method of functional ceramic ornament claimed in claim 3, it is characterized in that: the described mould outlet of step (3) is rope form or band shape.
6. the application of functional ceramic ornament claimed in claim 1 aspect the body-care beauty treatment.
7. the application of functional ceramic ornament claimed in claim 6 aspect the body-care beauty treatment is characterized in that: described functional ceramic ornament further is processed into necklace, bracelet, bangle or bracelet wears in body local.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200710130793 CN101353252B (en) | 2007-07-25 | 2007-07-25 | Functional ceramic ornament, preparation and use thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200710130793 CN101353252B (en) | 2007-07-25 | 2007-07-25 | Functional ceramic ornament, preparation and use thereof |
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| Publication Number | Publication Date |
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| CN101353252A CN101353252A (en) | 2009-01-28 |
| CN101353252B true CN101353252B (en) | 2013-02-20 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN 200710130793 Expired - Fee Related CN101353252B (en) | 2007-07-25 | 2007-07-25 | Functional ceramic ornament, preparation and use thereof |
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Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102241517B (en) * | 2011-04-07 | 2014-08-27 | 佛山市中国科学院上海硅酸盐研究所陶瓷研发中心 | Method for preparing functional building ceramic |
| CN106726628B (en) * | 2016-11-22 | 2020-02-14 | 惠州市申天地生物科技有限公司 | Anion far infrared nano multifunctional material |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1123650A (en) * | 1995-04-12 | 1996-06-05 | 任全利 | Health-care earphone for promoting memory and preventing noises |
| CN1392115A (en) * | 2002-08-13 | 2003-01-22 | 河北工业大学 | Multifunctinoal health ceramic material and its preparing method and use |
| CN1887784A (en) * | 2006-07-14 | 2007-01-03 | 河北工业大学 | Functional ceramic material and its prepn process |
-
2007
- 2007-07-25 CN CN 200710130793 patent/CN101353252B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1123650A (en) * | 1995-04-12 | 1996-06-05 | 任全利 | Health-care earphone for promoting memory and preventing noises |
| CN1392115A (en) * | 2002-08-13 | 2003-01-22 | 河北工业大学 | Multifunctinoal health ceramic material and its preparing method and use |
| CN1887784A (en) * | 2006-07-14 | 2007-01-03 | 河北工业大学 | Functional ceramic material and its prepn process |
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| CN101353252A (en) | 2009-01-28 |
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Owner name: BEIJING WUHUAN YONGSHENG TECHNOLOGY CO., LTD. Free format text: FORMER OWNER: BEIJING UNIFLY TECHNOLOGY CO., LTD. Effective date: 20131205 |
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Effective date of registration: 20131205 Address after: 100016, Beijing, Jiuxianqiao, Chaoyang District Road, No. 11, Three Gorges Merchants Building 220C Patentee after: BEIJING WUHUA YONGSHENG TECHNOLOGY CO., LTD. Address before: 100007 A710 room, No. 28 East Main Street, Dongcheng District, Beijing, Andingmen Patentee before: Beijing Unifly Technology Co., Ltd. |
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Granted publication date: 20130220 Termination date: 20160725 |