CN101348757A - Preparation of low deuterium spirit - Google Patents

Preparation of low deuterium spirit Download PDF

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Publication number
CN101348757A
CN101348757A CNA2008100403793A CN200810040379A CN101348757A CN 101348757 A CN101348757 A CN 101348757A CN A2008100403793 A CNA2008100403793 A CN A2008100403793A CN 200810040379 A CN200810040379 A CN 200810040379A CN 101348757 A CN101348757 A CN 101348757A
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China
Prior art keywords
water
tower
deuterium
heavy
low deuterium
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Pending
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CNA2008100403793A
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Chinese (zh)
Inventor
丛峰松
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Shanghai Chitian Ddwater Biological Engineering Co Ltd
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Shanghai Chitian Ddwater Biological Engineering Co Ltd
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Priority to CNA2008100403793A priority Critical patent/CN101348757A/en
Publication of CN101348757A publication Critical patent/CN101348757A/en
Pending legal-status Critical Current

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Abstract

The invention relates to the technical field of the white spirit preparation, in particular to a method for preparing low deuterium white spirit, comprising the following: (1) a step of blending materials; (2) a step of baking to enclose materials; (3) a step of stewing and pasting; (4) a step of ventilating to cool dregs; (5) a step of adding seriflux; (6) a step of stirring evenly to put into a cellar and of saccharifying to ferment; (7) a step of taking out of the cellar to distill; (8) a step of adjusting flavor and blending; and (9) a step of canning the finished product. The method is characterized in that in the processes of baking to enclose materials, adding seriflux and/or adjusting flavor and blending, low deuterium water is used and the low deuterium water with the content of the deuterium between 0 and 135ppm is taken as a raw material for the production processing. Compared with the prior art, the method has the advantages: 1. the product not only keeps the style of the prior white spirit but also has mellow quality and soft mouthfeel; and 2. the content of the deuterium in the white spirit body is low, and the white spirit has the physiological functions of improving the human immunity, delaying senility, reducing the blood fat, and reducing the liver injury, and the like.

Description

A kind of preparation method of low deuterium spirit
[technical field]
The present invention relates to the liquor preparing technical field, specifically a kind of preparation method of low deuterium spirit.
[background technology]
People are the wine base with liquor for many years, by adding (or wine soaks) natural nutrient substance, make health promoting wine, but the market share are limited, with liquor comparison major cause be exactly that health promoting wine has changed former liquor flavor characteristics.
China white wine and water in close relations, people pay close attention to always and how to have adopted water to make to add oar degree of falling to improve the taste and the quality of wine for a long time, increase the added value of wine.
" deuterium " is a kind of poisonous element.Water is no matter the content of deuterium how much, all is deleterious to life entity.The content of deuterium is high more, and is just big more to the murder by poisoning of life entity.Because without any defensive ability/resistance ability, in a single day deuterium enters and be difficult to metabolism behind the life entity and go out viable organism, and in vivo accumulative action is arranged to deuterium, heredity, metabolism and the enzyme system etc. of human body there is detrimentally affect.Just because of contain " deuterium poison " in nature water and the life entity, cancer, diabetes and other chronic diseases so the mankind just constantly derive, so that health risk are nibbled life, make the people could not be long-lived!
Hungary, Romania are two countries that research and develop low deuterium-oxide in the world the earliest, find that low deuterium-oxide has positive effect aspect prevention and the treatment cancer.Japan has also carried out broad research to low deuterium-oxide, finds to drink low deuterium-oxide and can improve health NK cytoactive value greatly and can reduce the health blood glucose value.The scientist of state-run scientific center of the Russian Federation and US National Aeronautics and Space Administration (NASA) jet propulsion laboratory may launch research in the potential using value of manned space flight medical science at low deuterium-oxide, and the low deuterium-oxide of discovery can be resisted cosmic radiation DNA is caused damage.Shanghai Communications University launches research to low deuterium-oxide biological effect mechanism, finds that low deuterium-oxide is delaying senility and preventing aspect such as cardiovascular and cerebrovascular diseases that effect is arranged.
[summary of the invention]
The objective of the invention is to overcome the deficiencies in the prior art, a kind of preparation method of low deuterium spirit is provided
For realizing the present invention, the preparation method of low deuterium spirit comprises (1) batching; (2) heat training shelving; (3) boiling gelatinization; (4) the cool slag that ventilates; (5) addition water; (6) mix into the cellar for storing things diastatic fermentation thoroughly; (7) go out the cellar for storing things distillation; (8) blending is blent, (9) canned finished product, and it is characterized in that heat training shelving, addition water and/or blending are blent carries out heat with low deuterium-oxide and trains shelving, does water for syrup addition or blending water, and the low deuterium-oxide that with the deuterium content is 0-135ppm is that production processes raw material.
Described canned finished product liquor adopts low deuterium-oxide to add slurry and blends.
It is the isotope exchange reactions that utilize between hydrogen sulfide and the water that described low deuterium-oxide adopts the two warm exchange processes of hydrogen sulfide, adopt the mode of cold tower and thermal tower multi-stage cascade serial connection to realize separating of heavy hydrogen and tritium, liquid starting material water enters from cold top of tower, flows through hot and cold exchange column from top to bottom; Gas material hydrogen sulfide adds between cold and hot tower, and in cold and hot tower circulating from bottom to top, in exchange column, form convection current with liquid material, heavy constituent are shifted and are concentrated in liquid phase to liquid phase by chemical exchange in the cold tower, and the concentration of heavy constituent reaches maximum value in cold tower bottom liquid phase; The liquid material that has concentrated heavy constituent when flowing through thermal tower again with up gas generation chemical exchange, heavy constituent are shifted to gas phase again, the liquid phase material of discharging from thermal tower enters and promptly gets the finished product that reduced heavy hydrogen content after degassing tower removes hydrogen sulfide, when pressure 2~2.2MPa, the best operating condition T 1=303~308K of cold tower, the best operating condition T 2=403~413K of thermal tower.
Described low deuterium-oxide adopts the two warm exchange processes of hydrogen sulfide to be substituted by rectification method, rectification method is to utilize the molecule volatility of heavy hydrogen and hydrogen different and carry out isolating method, the separation factor of rectifying equals the ratio of the pure vapour pressure of separated two components, and increase with the reduction of temperature and the minimizing of molecular weight, liquid starting material water at first enters vaporizer, in vaporizer, be heated and gasify, in rectifying tower, because heavy water is different with the volatility of light-water, charging heavy water/the liquid of light-water steam in uphill process and on the column plate carries out mass transfer exchange and the thermal exchange between vapour-liquid, promptly the heavy water of Shang Shenging/light-water steam is the heavy water on contained heavy water and the heat transferred column plate/light-water mixture, and make it to rise to the last layer column plate again after the gasification, simultaneously, steam is after condensation on the column plate, be back to down one deck column plate, like this, in the steam flow that rises, the content of heavy water is more and more lower, in rectifying, compound by regulating in stage number and the reflux ratio one or both, can generate the finished product of different heavy hydrogen concentration.
Deuterium content is lower than the concentration range of normal level in the ortho-water, between 0ppm-135ppm.
The present invention compared with prior art has following beneficial effect: 1. this product has not only kept the style of traditional liquor fully, and vinosity is pure and mild, and mouthfeel is submissive; 2, deuterium content is low in this liquor wine body, has the enhancing body immunity, delays senility, and blood fat reducing reduces physiological functions such as liver injury.
[specific embodiment]
Illustrate in greater detail the present invention below by embodiment.
Embodiment 1 directly adds slurry degree of falling with low deuterium-oxide
Get Luzhou Lao Jiao 52 base wine, add the low deuterium-oxide of 10 ± 5ppm, make the wine degree be reduced to 38 degree, deuterium content is 110 ± 5ppm in the wine body.
Effect: the low deuterium spirit that this method is produced, to drink in right amount for a long time and have the enhancing body immunity, physiological function such as delay senility.
Embodiment 2 directly adds slurry degree of falling with low deuterium-oxide
Get the basic wine of Beijing Red Star strong, colourless liquor distilled from sorghum 56 degree, add the low deuterium-oxide of 40 ± 5ppm, make the wine degree be reduced to 38 degree, deuterium content is 105 ± 5ppm in the wine body.
Effect: the low deuterium spirit that this method is produced, to drink in right amount for a long time and have the enhancing body immunity, physiological function such as delay senility.
Example 2 is used low deuterium-oxide in fermentation
1. selecting the red sorghum for use is main raw material; 2. add the low deuterium-oxide of 125 ± 5ppm and carry out heat training shelving; 3. boiling gelatinization; 4. cool slag ventilates; 5. hang down deuterium-oxide as addition water with 125 ± 5ppm; 6. mix into the cellar for storing things diastatic fermentation thoroughly; 7. go out the cellar for storing things distillation; 8, blend with the low deuterium-oxide blending of 125 ± 5ppm.Deuterium content is 105 ± 5ppm in the wine body
Effect: the low deuterium spirit that this method is produced, to drink in right amount for a long time and have the enhancing body immunity, physiological function such as delay senility.

Claims (5)

1, a kind of preparation method of low deuterium spirit comprises (1) batching; (2) heat training shelving; (3) boiling gelatinization; (4) the cool slag that ventilates; (5) addition water; (6) mix into the cellar for storing things diastatic fermentation thoroughly; (7) go out the cellar for storing things distillation; (8) blending is blent, (9) canned finished product, and it is characterized in that heat training shelving, addition water and/or blending are blent carries out heat with low deuterium-oxide and trains shelving, does water for syrup addition or blending water, and the low deuterium-oxide that with the deuterium content is 0-135ppm is that production processes raw material.
2, the preparation method of a kind of low deuterium spirit according to claim 1 is characterized in that described canned finished product liquor adopts low deuterium-oxide to add slurry and blends.
3, the preparation method of a kind of low deuterium spirit according to claim 1, it is characterized in that it is the isotope exchange reactions that utilize between hydrogen sulfide and the water that described low deuterium-oxide adopts the two warm exchange processes of hydrogen sulfide, adopt the mode of cold tower and thermal tower multi-stage cascade serial connection to realize separating of heavy hydrogen and tritium, liquid starting material water enters from cold top of tower, flows through hot and cold exchange column from top to bottom; Gas material hydrogen sulfide adds between cold and hot tower, and in cold and hot tower circulating from bottom to top, in exchange column, form convection current with liquid material, heavy constituent are shifted and are concentrated in liquid phase to liquid phase by chemical exchange in the cold tower, and the concentration of heavy constituent reaches maximum value in cold tower bottom liquid phase; The liquid material that has concentrated heavy constituent when flowing through thermal tower again with up gas generation chemical exchange, heavy constituent are shifted to gas phase again, the liquid phase material of discharging from thermal tower enters and promptly gets the finished product that reduced heavy hydrogen content after degassing tower removes hydrogen sulfide, when pressure 2~2.2MPa, best operating condition T1=303~the 308K of cold tower, the best operating condition T2=403~413K of thermal tower.
4, the preparation method of a kind of low deuterium spirit according to claim 1, it is characterized in that described low deuterium-oxide adopts the two warm exchange processes of hydrogen sulfide to be substituted by rectification method, rectification method is to utilize the molecule volatility of heavy hydrogen and hydrogen different and carry out isolating method, the separation factor of rectifying equals the ratio of the pure vapour pressure of separated two components, and increase with the reduction of temperature and the minimizing of molecular weight, liquid starting material water at first enters vaporizer, in vaporizer, be heated and gasify, in rectifying tower, because heavy water is different with the volatility of light-water, charging heavy water/the liquid of light-water steam in uphill process and on the column plate carries out mass transfer exchange and the thermal exchange between vapour-liquid, promptly the heavy water of Shang Shenging/light-water steam is the heavy water on contained heavy water and the heat transferred column plate/light-water mixture, and make it to rise to the last layer column plate again after the gasification, simultaneously, steam is after condensation on the column plate, be back to down one deck column plate, like this, in the steam flow that rises, the content of heavy water is more and more lower, in rectifying, compound by regulating in stage number and the reflux ratio one or both, can generate the finished product of different heavy hydrogen concentration.
5, the preparation method of a kind of low deuterium spirit according to claim 1 is characterized in that deuterium content is lower than the concentration range of normal level in the ortho-water, between 0ppm-135ppm.
CNA2008100403793A 2008-07-09 2008-07-09 Preparation of low deuterium spirit Pending CN101348757A (en)

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Application Number Priority Date Filing Date Title
CNA2008100403793A CN101348757A (en) 2008-07-09 2008-07-09 Preparation of low deuterium spirit

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CN101348757A true CN101348757A (en) 2009-01-21

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102776093A (en) * 2012-07-16 2012-11-14 泸州品创科技有限公司 Preparation process of deuterium-depleted water Daqu
CN102776094A (en) * 2012-07-16 2012-11-14 泸州品创科技有限公司 Deuterium-depleted water white spirit and production method thereof
CN111018011A (en) * 2019-11-20 2020-04-17 四川新火炬化工有限责任公司 Production process of deuterium-removed drinking water
CN111500398A (en) * 2020-06-23 2020-08-07 四川大学 Preparation method of deuterium-depleted water-brewed Hakka rice wine
CN115141706A (en) * 2022-06-27 2022-10-04 上海信悉智能技术有限公司 Fruity low-deuterium wine and preparation method thereof

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102776093A (en) * 2012-07-16 2012-11-14 泸州品创科技有限公司 Preparation process of deuterium-depleted water Daqu
CN102776094A (en) * 2012-07-16 2012-11-14 泸州品创科技有限公司 Deuterium-depleted water white spirit and production method thereof
CN102776093B (en) * 2012-07-16 2013-12-11 泸州品创科技有限公司 Preparation process of deuterium-depleted water Daqu
CN111018011A (en) * 2019-11-20 2020-04-17 四川新火炬化工有限责任公司 Production process of deuterium-removed drinking water
CN111500398A (en) * 2020-06-23 2020-08-07 四川大学 Preparation method of deuterium-depleted water-brewed Hakka rice wine
CN115141706A (en) * 2022-06-27 2022-10-04 上海信悉智能技术有限公司 Fruity low-deuterium wine and preparation method thereof

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Open date: 20090121