CN101337682A - Ammonium sulfide solution and processing process thereof - Google Patents

Ammonium sulfide solution and processing process thereof Download PDF

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Publication number
CN101337682A
CN101337682A CNA2008101287338A CN200810128733A CN101337682A CN 101337682 A CN101337682 A CN 101337682A CN A2008101287338 A CNA2008101287338 A CN A2008101287338A CN 200810128733 A CN200810128733 A CN 200810128733A CN 101337682 A CN101337682 A CN 101337682A
Authority
CN
China
Prior art keywords
ammonium sulfide
sulfide solution
solution
ammonium
ammoniacal liquor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CNA2008101287338A
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Chinese (zh)
Inventor
张洪来
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
TIANJIN DAGANG YIZHONG CHEMICAL FACTORY
Original Assignee
TIANJIN DAGANG YIZHONG CHEMICAL FACTORY
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by TIANJIN DAGANG YIZHONG CHEMICAL FACTORY filed Critical TIANJIN DAGANG YIZHONG CHEMICAL FACTORY
Priority to CNA2008101287338A priority Critical patent/CN101337682A/en
Publication of CN101337682A publication Critical patent/CN101337682A/en
Pending legal-status Critical Current

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Abstract

The invention relates to the chemical engineering field, in particular to an ammonium sulfide solution and a production process thereof. The content of ammonium sulfide in the ammonium sulfide solution is 10 percent to 45 percent. The ammonium sulfide solution and the production process have the advantages of strong stability and unchanged concentration and is deposit-free, and the color of the ammonium sulfide solution cannot be changed within a year.

Description

A kind of ammonium sulfide solution and complete processing thereof
Technical field
The present invention designs chemical field, and a kind of ammonium sulfide solution and complete processing thereof specifically are provided.
Background technology
Ammonium sulfide solution under the prior art generally just adopts hydrogen sulfide and ammonia chemical combination and blends, but its concentration of the ammonium sulfide solution that this mode obtains is lower, it is very easily variable color and reduce concentration under long-term situation of placing, thereby influence its normal use, make troubles for manufacturer and user.
Summary of the invention
The present invention be directed to above deficiency, a kind of ammonium sulfide solution and complete processing thereof are provided, its product stability is strong, nondiscoloration in a year, and sediment-free and concentration are constant.
The technical solution adopted for the present invention to solve the technical problems is:
A kind of ammonium sulfide solution, the content of ammonium sulfide is 10%-45% in the described ammonium sulfide solution.
A kind of complete processing of ammonium sulfide solution may further comprise the steps:
A, sodium sulphite and sulfuric acid are reacted the formation hydrogen sulfide;
B, will liquefied ammonia filter the back and form ammoniacal liquor with the water reaction;
C, the hydrogen sulfide that generates dashed described ammoniacal liquor after filtering converts, towards the time of converting be 56-200 hour, thereby form described ammonium sulfide solution.
A kind of ammonium sulfide solution of the present invention and production technique thereof, its product is stable, stores the look that can remain unchanged for a long time in the lucifuge bucket, and concentration is kept stable, sediment-free.
Whole process using reagent standard in the production technique of the present invention, thus the stability and the security of product greatly increased.
Embodiment
Below in conjunction with specific embodiment a kind of ammonium sulfide solution of the present invention and complete processing thereof are further described.
A kind of ammonium sulfide solution, the content of ammonium sulfide can be 10%, 15%, 20%, 25%, 30%, 35%, 40%, 45% in the described ammonium sulfide solution.
The complete processing of above-mentioned a kind of ammonium sulfide solution may further comprise the steps:
A, sodium sulphite and sulfuric acid are reacted the formation hydrogen sulfide;
B, will liquefied ammonia filter the back and form ammoniacal liquor with the water reaction;
C, the hydrogen sulfide that generates dashed described ammoniacal liquor after filtering converts, towards the time of converting be 56-200 hour, thereby form described ammonium sulfide solution.
A kind of ammonium sulfide solution of the present invention, the height of its content determines that according to the time it is high more towards the time concentration of converting of a specified duration more.
Above-described embodiment, the present invention embodiment a kind of more preferably just, the common variation that those skilled in the art carries out in the technical solution of the present invention scope and replacing all should be included in protection scope of the present invention.

Claims (2)

1, a kind of ammonium sulfide solution is characterized in that, the content of ammonium sulfide is 10%-45% in the described ammonium sulfide solution.
2, a kind of complete processing of ammonium sulfide solution is characterized in that, may further comprise the steps:
A, sodium sulphite and sulfuric acid are reacted the formation hydrogen sulfide;
B, will liquefied ammonia filter the back and form ammoniacal liquor with the water reaction;
C, the hydrogen sulfide that generates dashed described ammoniacal liquor after filtering converts, towards the time of converting be 56-200 hour, thereby form described ammonium sulfide solution.
CNA2008101287338A 2008-06-20 2008-06-20 Ammonium sulfide solution and processing process thereof Pending CN101337682A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CNA2008101287338A CN101337682A (en) 2008-06-20 2008-06-20 Ammonium sulfide solution and processing process thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CNA2008101287338A CN101337682A (en) 2008-06-20 2008-06-20 Ammonium sulfide solution and processing process thereof

Publications (1)

Publication Number Publication Date
CN101337682A true CN101337682A (en) 2009-01-07

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CNA2008101287338A Pending CN101337682A (en) 2008-06-20 2008-06-20 Ammonium sulfide solution and processing process thereof

Country Status (1)

Country Link
CN (1) CN101337682A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102745646A (en) * 2012-06-05 2012-10-24 新疆天业(集团)有限公司 Method for replenishing sulfureted hydrogen during CO transformation production process

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102745646A (en) * 2012-06-05 2012-10-24 新疆天业(集团)有限公司 Method for replenishing sulfureted hydrogen during CO transformation production process

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Open date: 20090107